GB830813A - Production of triacetone dialcohol - Google Patents
Production of triacetone dialcoholInfo
- Publication number
- GB830813A GB830813A GB3717257A GB3717257A GB830813A GB 830813 A GB830813 A GB 830813A GB 3717257 A GB3717257 A GB 3717257A GB 3717257 A GB3717257 A GB 3717257A GB 830813 A GB830813 A GB 830813A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acetone
- triacetone
- dialcohol
- triacetone dialcohol
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 8
- SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Chemical compound CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 abstract 4
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000006386 neutralization reaction Methods 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/04—Saturated compounds containing keto groups bound to acyclic carbon atoms
- C07C49/17—Saturated compounds containing keto groups bound to acyclic carbon atoms containing hydroxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Triacetone dialcohol is prepared along with diacetone alcohol by mixing acetone with an alkali metal hydroxide in solution in a C1-4 alkanol at -30 DEG to +15 DEG C. Preferably 0.002 to 0.02 grams of alkali metal hydroxide are used per 100 ml. of acetone. The temperature preferably does not exceed 0 DEG C. Acetone containing up to 0.5% by volume of water may be used. The triacetone dialcohol may be recovered by, for example, neutralizing the alkali with acid, distilling the acetone at atmospheric pressure, filtering off the salt formed in the neutralization, and then removing diacetone alcohol at reduced pressure leaving the triacetone dialcohol as the residue.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3717257A GB830813A (en) | 1957-11-28 | 1957-11-28 | Production of triacetone dialcohol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3717257A GB830813A (en) | 1957-11-28 | 1957-11-28 | Production of triacetone dialcohol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB830813A true GB830813A (en) | 1960-03-23 |
Family
ID=10394358
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3717257A Expired GB830813A (en) | 1957-11-28 | 1957-11-28 | Production of triacetone dialcohol |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB830813A (en) |
-
1957
- 1957-11-28 GB GB3717257A patent/GB830813A/en not_active Expired
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