GB755635A - Improvements in the electrodeposition of iron - Google Patents
Improvements in the electrodeposition of ironInfo
- Publication number
- GB755635A GB755635A GB1298/54A GB129854A GB755635A GB 755635 A GB755635 A GB 755635A GB 1298/54 A GB1298/54 A GB 1298/54A GB 129854 A GB129854 A GB 129854A GB 755635 A GB755635 A GB 755635A
- Authority
- GB
- United Kingdom
- Prior art keywords
- iron
- electrolyte
- followed
- added
- anode
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical group [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title abstract 11
- 229910052742 iron Inorganic materials 0.000 title abstract 6
- 238000004070 electrodeposition Methods 0.000 title abstract 2
- 239000003792 electrolyte Substances 0.000 abstract 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- 239000000080 wetting agent Substances 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- 101100165798 Arabidopsis thaliana CYP86A1 gene Proteins 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 abstract 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 abstract 1
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 abstract 1
- 239000004141 Sodium laurylsulphate Substances 0.000 abstract 1
- 229910000831 Steel Inorganic materials 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000001913 cellulose Substances 0.000 abstract 1
- 229920002678 cellulose Polymers 0.000 abstract 1
- 229910052804 chromium Inorganic materials 0.000 abstract 1
- 239000011651 chromium Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000000866 electrolytic etching Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 239000008262 pumice Substances 0.000 abstract 1
- 239000010802 sludge Substances 0.000 abstract 1
- 235000019333 sodium laurylsulphate Nutrition 0.000 abstract 1
- 239000010959 steel Substances 0.000 abstract 1
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
- 229920006163 vinyl copolymer Polymers 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 239000002023 wood Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/20—Electroplating: Baths therefor from solutions of iron
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Electrolytic Production Of Metals (AREA)
Abstract
755,635. Electrodeposition of iron. INGENIEURSBUREAU LEMET CHROMIUM H. VAN DER HORST N.V., and HORST, H. VAN DER. Jan. 15, 1954 [Jan. 16, 1953], No. 1298/54. Class 41. Cathodically deposited iron is produced by using as electrolyte an acidic aqueous solution containing per litre 10 to 100 grams fluoborate calculated as BF 4 , not less than 6.5 grams chloride calculated as Cl, and ferrous iron radicals. Preferably the electrolyte is of pH 2 to 5, the temperature is 135‹ to 150‹ F., and the cathode current density is 30 to 70 amps/sq. ft., a ferrous anode-iron or steel-being used. Anode sludge is collected in a porous bag, preferably of vinyl copolymers. Ammonium and sulphate radicals may be included in the electrolyte if desired while a wetting agent such as sodium lauryl sulphate may also be added. The compound supplying the fluoborate radical should be dissolved in water first followed by the other ingredients, iron is added to precipitate impurities, followed by activated carbon and finely divided wood cellulose to absorb the impurities, and the solution is then filtered, the wetting agent if required being added after filtering. The surface to be plated especially if of iron or steel is first vapour-degreased if necessary and then cleaned with pumice, followed by electrolytic etching as anode in a strong sulphuric acid solution. The iron-plated cathode may be heated e.g. to 600‹ F. to improve its toughness and ductility.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US331725A US2745800A (en) | 1953-01-16 | 1953-01-16 | Electroplating with iron |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB755635A true GB755635A (en) | 1956-08-22 |
Family
ID=23295111
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1298/54A Expired GB755635A (en) | 1953-01-16 | 1954-01-15 | Improvements in the electrodeposition of iron |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US2745800A (en) |
| BE (1) | BE522608A (en) |
| CH (1) | CH327296A (en) |
| DE (1) | DE1048755B (en) |
| ES (1) | ES211670A1 (en) |
| FR (1) | FR1146512A (en) |
| GB (1) | GB755635A (en) |
| NL (2) | NL100872C (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE548025A (en) * | 1956-05-23 | |||
| US2986499A (en) * | 1958-01-17 | 1961-05-30 | Du Pont | Electropolishing steel |
| US3282809A (en) * | 1962-11-07 | 1966-11-01 | Clevite Corp | Iron coating for refractory metal |
| US3481638A (en) * | 1963-12-13 | 1969-12-02 | Dryden Hugh L | Method of forming ceramic-to-metal seal |
| US3415556A (en) * | 1963-12-13 | 1968-12-10 | Nasa | Ceramic-to-metal seal and method of making same |
| US3345212A (en) * | 1964-02-18 | 1967-10-03 | Esb Inc | Electrolytic process for preparing iron |
| US3477876A (en) * | 1966-06-13 | 1969-11-11 | Dow Chemical Co | Galvanic cell employing iron cathode and method of producing galvanic cathode having activated iron surface |
| US3753664A (en) * | 1971-11-24 | 1973-08-21 | Gen Motors Corp | Hard iron electroplating of soft substrates and resultant product |
| DE3422327A1 (en) * | 1984-06-15 | 1985-12-19 | Fürstlich Hohenzollernsche Hüttenverwaltung Laucherthal, 7480 Sigmaringen | Process for producing a sliding layer of white metal on lead bronze surfaces of steel/lead bronze babbitt bearings |
| CN115787013A (en) * | 2022-11-30 | 2023-03-14 | 扬州托新汽车零部件有限公司 | Electroplating process for easy collection of anode slime |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB154282A (en) * | 1919-08-06 | 1920-11-08 | Sherard Osborn Cowper Coles | Improved process for building up undersized parts of machinery |
| US1562710A (en) * | 1920-07-27 | 1925-11-24 | Madsenell Corp | Method of treating metallic objects and resulting products |
| US1516326A (en) * | 1921-10-12 | 1924-11-18 | Electrolytic Iron Inc | Manufacture of electrolytic iron |
| US1607960A (en) * | 1923-06-26 | 1926-11-23 | Madsenell Corp | Method and means for electrodepositing nickel metals and the resulting products |
| US1567625A (en) * | 1925-01-23 | 1925-12-29 | Joseph A Smith | Plated article and its manufacture |
| US1645927A (en) * | 1926-03-05 | 1927-10-18 | Metals Prot Corp | Chromium plating |
| US1780213A (en) * | 1926-10-07 | 1930-11-04 | Vincent M Vertucci | Method of preparing chromium-plated ferrous articles |
| US1862745A (en) * | 1928-12-12 | 1932-06-14 | Fuller | Process for electrodepositing iron |
| US1937068A (en) * | 1929-07-31 | 1933-11-28 | Ernst Kelsen | Method of depositing iron electrolytically |
| US1912430A (en) * | 1929-08-19 | 1933-06-06 | Richardson Co | Electrolytic process of producing ductile iron |
| US2092130A (en) * | 1936-05-19 | 1937-09-07 | Meaker Company | Anodic cleaning process |
| US2359224A (en) * | 1940-04-29 | 1944-09-26 | Knol Kornelis Swier | Electromagnetic device |
| US2304709A (en) * | 1940-10-31 | 1942-12-08 | Thomas Steel Company | Method of coating ferrous articles |
| US2420403A (en) * | 1943-02-25 | 1947-05-13 | Champion Paper & Fibre Co | Electrodeposition of iron |
| US2465747A (en) * | 1945-04-30 | 1949-03-29 | Rca Corp | Apparatus for electroplating metal |
| US2523160A (en) * | 1947-11-28 | 1950-09-19 | Allied Chem & Dye Corp | Electrodeposition of metals |
| US2580681A (en) * | 1948-08-24 | 1952-01-01 | Sulphide Ore Process Company I | Method of treating the electrolyte in the electrodeposition of iron |
-
0
- BE BE522608D patent/BE522608A/xx unknown
- NL NLAANVRAGE7410367,B patent/NL180512B/en unknown
- DE DENDAT1048755D patent/DE1048755B/de active Pending
- NL NL100872D patent/NL100872C/xx active
-
1953
- 1953-01-16 US US331725A patent/US2745800A/en not_active Expired - Lifetime
- 1953-08-28 FR FR1146512D patent/FR1146512A/en not_active Expired
- 1953-09-16 CH CH327296D patent/CH327296A/en unknown
- 1953-10-14 ES ES0211670A patent/ES211670A1/en not_active Expired
-
1954
- 1954-01-15 GB GB1298/54A patent/GB755635A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US2745800A (en) | 1956-05-15 |
| ES211670A1 (en) | 1954-02-16 |
| DE1048755B (en) | 1959-01-15 |
| BE522608A (en) | |
| NL100872C (en) | |
| CH327296A (en) | 1958-01-31 |
| NL180512B (en) | |
| FR1146512A (en) | 1957-11-13 |
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