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GB718306A - Improvements in or relating to the manufacture of catalysts - Google Patents

Improvements in or relating to the manufacture of catalysts

Info

Publication number
GB718306A
GB718306A GB10687/52A GB1068752A GB718306A GB 718306 A GB718306 A GB 718306A GB 10687/52 A GB10687/52 A GB 10687/52A GB 1068752 A GB1068752 A GB 1068752A GB 718306 A GB718306 A GB 718306A
Authority
GB
United Kingdom
Prior art keywords
palladium
catalyst
solution
alumina
salt
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB10687/52A
Inventor
Cyril Alfred Morgan
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik LCL Ltd
Original Assignee
Laporte Chemicals Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to BE519537D priority Critical patent/BE519537A/xx
Priority to IT507231D priority patent/IT507231A/it
Priority to NL81271D priority patent/NL81271C/xx
Application filed by Laporte Chemicals Ltd filed Critical Laporte Chemicals Ltd
Priority to GB10687/52A priority patent/GB718306A/en
Priority to ES0208938A priority patent/ES208938A1/en
Priority to FR1085061D priority patent/FR1085061A/en
Publication of GB718306A publication Critical patent/GB718306A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C01B15/022—Preparation from organic compounds
    • C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/44—Palladium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)

Abstract

Palladium catalyst is prepared by adsorbing a palladium salt from solution on to an alumina carrier and treating with a water-soluble metal hydroxide or carbonate to form a hydrated palladium oxide or basic carbonate, which is thereafter reduced to metallic palladium. Activated gamma-alumina or gamma-alumina monohydrate of coarse or fine particle size is stirred for a short time with a solution of palladium chloride, nitrate, or acetate, the slurry is filtered and washed, the solid stirred with caustic soda solution and again filtered and washed; further treatments with palladium salt solutions may be given, using the filtrate from the first stage or solutions of higher concentration. The amount of acid in the palladium salt solution should be limited to that required for complete solution of the salt. The palladium content of the final catalyst is 0.01-10 per cent., varying with the particle size of the alumina. The catalyst is used in the hydrogenation stage of the cyclic process for the manufacture of hydrogen peroxide by autoxidation of anthraquinhydrones, for example as described in Specification 718,305; before use the catalyst is reduced with a mixture of hydrogen and nitrogen of increasing hydrogen content, or reduction may be effected in the hydrogenator. Regeneration of the catalyst may be carried out by thermal oxidation of the adsorbed organic matter, followed if necessary by reduction. Specification 508,081 also is referred to. The Provisional Specification refers also to the use of charcoal as the carrier.
GB10687/52A 1952-04-28 1952-04-28 Improvements in or relating to the manufacture of catalysts Expired GB718306A (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
BE519537D BE519537A (en) 1952-04-28
IT507231D IT507231A (en) 1952-04-28
NL81271D NL81271C (en) 1952-04-28
GB10687/52A GB718306A (en) 1952-04-28 1952-04-28 Improvements in or relating to the manufacture of catalysts
ES0208938A ES208938A1 (en) 1952-04-28 1953-04-23 Improvements in or relating to the manufacture of catalysts
FR1085061D FR1085061A (en) 1952-04-28 1953-04-28 Palladium catalyst and its preparation process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB10687/52A GB718306A (en) 1952-04-28 1952-04-28 Improvements in or relating to the manufacture of catalysts

Publications (1)

Publication Number Publication Date
GB718306A true GB718306A (en) 1954-11-10

Family

ID=9972435

Family Applications (1)

Application Number Title Priority Date Filing Date
GB10687/52A Expired GB718306A (en) 1952-04-28 1952-04-28 Improvements in or relating to the manufacture of catalysts

Country Status (6)

Country Link
BE (1) BE519537A (en)
ES (1) ES208938A1 (en)
FR (1) FR1085061A (en)
GB (1) GB718306A (en)
IT (1) IT507231A (en)
NL (1) NL81271C (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4376724A (en) * 1980-04-14 1983-03-15 Showa Denko Kabushiki Kaisha Rhodium catalyst and method for preparing the same
US5772977A (en) * 1994-12-14 1998-06-30 E. I. Du Pont De Nemours And Company Anthraquinone process
EP0878235A1 (en) * 1997-05-05 1998-11-18 Akzo Nobel N.V. Method of producing a catalyst by electroless deposition of the active metal on the support
US5853693A (en) * 1996-04-03 1998-12-29 Mitsubishi Gas Chemical Company, Inc. Hydrogenation catalyst for production of hydrogen peroxide, and method for preparation of same
US6207128B1 (en) 1997-05-05 2001-03-27 Akzo Nobel N.V. Method of producing a catalyst
EP1852392A1 (en) 2006-05-01 2007-11-07 Mitsubishi Gas Chemical Company, Inc. Method for activating hydrogenation catalyst and method for producing hydrogen peroxide including same
WO2016064443A1 (en) * 2014-10-22 2016-04-28 Chevron U.S.A. Inc. Process for preparing a spent catalyst for precious metals recovery

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4376724A (en) * 1980-04-14 1983-03-15 Showa Denko Kabushiki Kaisha Rhodium catalyst and method for preparing the same
US5772977A (en) * 1994-12-14 1998-06-30 E. I. Du Pont De Nemours And Company Anthraquinone process
US5853693A (en) * 1996-04-03 1998-12-29 Mitsubishi Gas Chemical Company, Inc. Hydrogenation catalyst for production of hydrogen peroxide, and method for preparation of same
US6126914A (en) * 1996-04-03 2000-10-03 Mitsubishi Gas Chemical Co., Inc. Hydrogenation catalyst for production of hydrogen peroxide, and method for preparation of same
EP0878235A1 (en) * 1997-05-05 1998-11-18 Akzo Nobel N.V. Method of producing a catalyst by electroless deposition of the active metal on the support
US6207128B1 (en) 1997-05-05 2001-03-27 Akzo Nobel N.V. Method of producing a catalyst
EP1852392A1 (en) 2006-05-01 2007-11-07 Mitsubishi Gas Chemical Company, Inc. Method for activating hydrogenation catalyst and method for producing hydrogen peroxide including same
WO2016064443A1 (en) * 2014-10-22 2016-04-28 Chevron U.S.A. Inc. Process for preparing a spent catalyst for precious metals recovery
US9580770B2 (en) 2014-10-22 2017-02-28 Chevron U.S.A. Inc. Process for preparing a spent catalyst for precious metals recovery

Also Published As

Publication number Publication date
NL81271C (en) 1900-01-01
ES208938A1 (en) 1954-06-16
FR1085061A (en) 1955-01-27
IT507231A (en) 1900-01-01
BE519537A (en) 1900-01-01

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