GB526760A - A process for dyeing wool and improved dyestuff preparations for use therein - Google Patents
A process for dyeing wool and improved dyestuff preparations for use thereinInfo
- Publication number
- GB526760A GB526760A GB848339A GB848339A GB526760A GB 526760 A GB526760 A GB 526760A GB 848339 A GB848339 A GB 848339A GB 848339 A GB848339 A GB 848339A GB 526760 A GB526760 A GB 526760A
- Authority
- GB
- United Kingdom
- Prior art keywords
- wool
- minutes
- temperature
- lissolamine
- boil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 210000002268 wool Anatomy 0.000 title abstract 15
- 239000000975 dye Substances 0.000 title abstract 5
- 238000004043 dyeing Methods 0.000 title abstract 3
- 238000002360 preparation method Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 18
- 238000009835 boiling Methods 0.000 abstract 8
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 abstract 6
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 abstract 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
- 150000001875 compounds Chemical class 0.000 abstract 4
- 239000001117 sulphuric acid Substances 0.000 abstract 4
- 235000011149 sulphuric acid Nutrition 0.000 abstract 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 abstract 3
- 239000010446 mirabilite Substances 0.000 abstract 3
- KMUONIBRACKNSN-UHFFFAOYSA-N potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- YSVBPNGJESBVRM-UHFFFAOYSA-L disodium;4-[(1-oxido-4-sulfonaphthalen-2-yl)diazenyl]naphthalene-1-sulfonate Chemical compound [Na+].[Na+].C1=CC=C2C(N=NC3=C(C4=CC=CC=C4C(=C3)S([O-])(=O)=O)O)=CC=C(S([O-])(=O)=O)C2=C1 YSVBPNGJESBVRM-UHFFFAOYSA-L 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- LFYSWCFSJAZQJJ-UHFFFAOYSA-L 1-dodecylpyridin-1-ium;sulfate Chemical compound [O-]S([O-])(=O)=O.CCCCCCCCCCCC[N+]1=CC=CC=C1.CCCCCCCCCCCC[N+]1=CC=CC=C1 LFYSWCFSJAZQJJ-UHFFFAOYSA-L 0.000 abstract 1
- CXRFDZFCGOPDTD-UHFFFAOYSA-M Cetrimide Chemical compound [Br-].CCCCCCCCCCCCCC[N+](C)(C)C CXRFDZFCGOPDTD-UHFFFAOYSA-M 0.000 abstract 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- ILDSIMPXNFWKLH-KATARQTJSA-N Leu-Thr-Ser Chemical compound CC(C)C[C@H](N)C(=O)N[C@@H]([C@@H](C)O)C(=O)N[C@@H](CO)C(O)=O ILDSIMPXNFWKLH-KATARQTJSA-N 0.000 abstract 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 abstract 1
- 239000004234 Yellow 2G Substances 0.000 abstract 1
- 150000001450 anions Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 150000001768 cations Chemical class 0.000 abstract 1
- 239000003086 colorant Substances 0.000 abstract 1
- SVSHEAJPDAGGCC-UHFFFAOYSA-L disodium 7-hydroxy-8-[[4-[4-[[4-(4-methylphenyl)sulfonyloxyphenyl]diazenyl]phenyl]phenyl]diazenyl]naphthalene-1,3-disulfonate Chemical compound CC1=CC=C(C=C1)S(=O)(=O)OC2=CC=C(C=C2)N=NC3=CC=C(C=C3)C4=CC=C(C=C4)N=NC5=C(C=CC6=CC(=CC(=C65)S(=O)(=O)O)S(=O)(=O)[O-])[O-].[Na+].[Na+] SVSHEAJPDAGGCC-UHFFFAOYSA-L 0.000 abstract 1
- FBNCDTLHQPLASV-UHFFFAOYSA-L disodium;5-methyl-2-[[5-(4-methyl-2-sulfonatoanilino)-9,10-dioxoanthracen-1-yl]amino]benzenesulfonate Chemical compound [Na+].[Na+].[O-]S(=O)(=O)C1=CC(C)=CC=C1NC1=CC=CC2=C1C(=O)C1=CC=CC(NC=3C(=CC(C)=CC=3)S([O-])(=O)=O)=C1C2=O FBNCDTLHQPLASV-UHFFFAOYSA-L 0.000 abstract 1
- FPVGTPBMTFTMRT-NSKUCRDLSA-L fast yellow Chemical compound [Na+].[Na+].C1=C(S([O-])(=O)=O)C(N)=CC=C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 FPVGTPBMTFTMRT-NSKUCRDLSA-L 0.000 abstract 1
- 235000019233 fast yellow AB Nutrition 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 abstract 1
- AMMWFYKTZVIRFN-UHFFFAOYSA-N sodium 3-hydroxy-4-[(1-hydroxynaphthalen-2-yl)diazenyl]-7-nitronaphthalene-1-sulfonic acid Chemical compound [Na+].C1=CC=CC2=C(O)C(N=NC3=C4C=CC(=CC4=C(C=C3O)S(O)(=O)=O)[N+]([O-])=O)=CC=C21 AMMWFYKTZVIRFN-UHFFFAOYSA-N 0.000 abstract 1
- 239000001632 sodium acetate Substances 0.000 abstract 1
- 235000017281 sodium acetate Nutrition 0.000 abstract 1
- RBKBGHZMNFTKRE-UHFFFAOYSA-K trisodium 2-[(2-oxido-3-sulfo-6-sulfonatonaphthalen-1-yl)diazenyl]benzoate Chemical compound C1=CC=C(C(=C1)C(=O)[O-])N=NC2=C3C=CC(=CC3=CC(=C2[O-])S(=O)(=O)O)S(=O)(=O)[O-].[Na+].[Na+].[Na+] RBKBGHZMNFTKRE-UHFFFAOYSA-K 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/655—Compounds containing ammonium groups
- D06P1/66—Compounds containing ammonium groups containing quaternary ammonium groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
- D06P3/20—Wool using mordant dyes using metallisable dyes
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
526,760. Dyeing wool; dye preparations. EVEREST, A. E., and WALLWORK, J. A. March 16, 1939, No. 8483. [Classes 2 (iii) and 15 (ii)] Loose wool, sun-faded woollen materials and mixtures of chemically treated with untreated wool are dyed in level shades in a liquor comprising an acid or chrome dyestuff (the term "acid dyestuff" including the Indigosol and Soledon (Registered Trade Mark) colours) and a small proportion of a compound containing a surface-active cation. Specified compounds of this type are Repellat L.T.S. (laurylpyridinium sulphate), Lissolamine (Registered Trade Mark) A or V and Sapamin (Registered Trade Mark) K.W. conc. (diethylaminoethylolcylamide hydrochloride). A dry powdered preparation containing the dyestuff, a small proportion of such compound and a compound containing a surface-active anion may be added to the dyebath. In examples, (1) scoured loose wool, wetted out with boiling water, is entered into a cold aqueous dyebath containing Carmoisime WS, Glauber salt, sulphuric acid and Lissolamine V, the temperature is slowly raised to the boil, boiling is continued for 10 minutes with addition of more sulphuric acid, boiling is then maintained for a further 20 minutes and the wool is rinsed, hydro-extracted and dried ; (2) scoured loose wool, similarly wetted out, is entered into a cold aqueous bath containing Solochrome red BS, sulphuric acid, Lissolamine A and pyridine, the temperature is slowly raised to the boil, so maintained for 30 minutes, then cooled to 80 ‹C. for addition of potassium bichromate solution and again maintained at the boil for 30 minutes, and the wool is rinsed, hydroextracted and dried ; (3) scoured loose wool is entered dry into an aqueous dyebath at 80‹C. containing Milling scarlet G, Gardinol (Registered Trade Mark) Rand Lissolamine A, the temperature is raised to the boil, acetic acid is added and boiling continued for 40 minutes with addition of more acetic acid after 10 minutes and the wool is rinsed, hydro-extracted and dried ; (4) scoured loose wool, wetted out with boiling water, is entered into an aqueous dyebath at 50‹C. containing anthraquinone violet, Gardinol R, Lissolamine A, acetic acid and Glauber salt, the temperature is raised to just below boiling and so maintained for 1 hour with an addition of potassium bichromate after 30 minutes and the wool is rinsed, hydroextracted and dried ; (5) scoured loose wool, wetted out with boiling water, is entered into a cold aqueous bath containing Sapamin K.W. conc. and acetic acid, the temperature is slowly raised to 60‹C., an aqueous solution of Kiton fast yellow 2G and Solway blue S.E.S. is added, the temperature is raised to boiling, so maintained for 10 minutes, more acetic acid is added and dyeing continued just below the boil for 20 minutes and the wool is hydroextracted and dried ; (6) a wetted out lightfaded wool flannel is.entered into a cold dyebath containing Carmoisine WS, Lissolamine A, Glauber salt and sulphuric acid, the temperature is slowly raised to just below the boil and so maintained for 30 minutes and the flannel is hydro-extracted and dried; (7) a similar flannel is entered into a cold aqueous dyebath containing Solochrome black 6 BFA, Gardinol WA, Repellat LTS, sodium acetate and acetic acid, the temperature is slowly raised to just below the boil, so maintained for 20 minutes, then cooled for addition of potassium bichromate solution and boiled for 30 minutes and the flannel is rinsed, hydroextracted and dried ; (8) Carmoisine WS, Lissolamine A and Gardinol R are mixed dry to obtain a powder suitable for direct addition to the dyebath.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB848339A GB526760A (en) | 1939-03-16 | 1939-03-16 | A process for dyeing wool and improved dyestuff preparations for use therein |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB848339A GB526760A (en) | 1939-03-16 | 1939-03-16 | A process for dyeing wool and improved dyestuff preparations for use therein |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB526760A true GB526760A (en) | 1940-09-25 |
Family
ID=9853330
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB848339A Expired GB526760A (en) | 1939-03-16 | 1939-03-16 | A process for dyeing wool and improved dyestuff preparations for use therein |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB526760A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2434178A (en) * | 1948-01-06 | Metachkome dyeing with a colloid | ||
| US2524041A (en) * | 1946-07-11 | 1950-10-03 | Arkansas Company Inc | Tippy wool dyeing assistants |
| US2539907A (en) * | 1948-04-14 | 1951-01-30 | Hat Corp America | Dyed carroted fur fibers and fabrics and method of dyeing the same |
| US3098690A (en) * | 1963-07-23 | Process fok union dyeing of acryloni- |
-
1939
- 1939-03-16 GB GB848339A patent/GB526760A/en not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2434178A (en) * | 1948-01-06 | Metachkome dyeing with a colloid | ||
| US3098690A (en) * | 1963-07-23 | Process fok union dyeing of acryloni- | ||
| US2524041A (en) * | 1946-07-11 | 1950-10-03 | Arkansas Company Inc | Tippy wool dyeing assistants |
| US2539907A (en) * | 1948-04-14 | 1951-01-30 | Hat Corp America | Dyed carroted fur fibers and fabrics and method of dyeing the same |
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