GB429616A - Improved packing for fractionating columns - Google Patents
Improved packing for fractionating columnsInfo
- Publication number
- GB429616A GB429616A GB34081/33A GB3408133A GB429616A GB 429616 A GB429616 A GB 429616A GB 34081/33 A GB34081/33 A GB 34081/33A GB 3408133 A GB3408133 A GB 3408133A GB 429616 A GB429616 A GB 429616A
- Authority
- GB
- United Kingdom
- Prior art keywords
- silicon carbide
- sand
- sawdust
- mixture
- packed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000012856 packing Methods 0.000 title abstract 2
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 abstract 4
- 239000000203 mixture Substances 0.000 abstract 3
- 239000013078 crystal Substances 0.000 abstract 2
- 239000004576 sand Substances 0.000 abstract 2
- 229910010271 silicon carbide Inorganic materials 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 229910021417 amorphous silicon Inorganic materials 0.000 abstract 1
- 239000011230 binding agent Substances 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 229920002678 cellulose Polymers 0.000 abstract 1
- 239000001913 cellulose Substances 0.000 abstract 1
- 239000000571 coke Substances 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 229910021426 porous silicon Inorganic materials 0.000 abstract 1
- 238000001953 recrystallisation Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/30—Loose or shaped packing elements, e.g. Raschig rings or Berl saddles, for pouring into the apparatus for mass or heat transfer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/30—Details relating to random packing elements
- B01J2219/302—Basic shape of the elements
- B01J2219/30296—Other shapes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/30—Details relating to random packing elements
- B01J2219/304—Composition or microstructure of the elements
- B01J2219/30416—Ceramic
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Ceramic Products (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
<PICT:0429616/III/1> In the manufacture of porous silicon carbide for use as a packing in fractionating columns, a mixture containing a small amount of sawdust with as much as 97,5 per cent of amorphous silicon carbide known as "fire sand" is packed around a graphite core in an electric furnace. Around this layer is packed the usual mixture of coke, sand, sawdust and salt, and the charge is raised to a temperature approaching 2000 C. Crystals of large size are formed about the core, and may be crushed to pieces 3 having dimensions of from 1 to 3 inches for use in stills. In an alternative method, ordinary silicon carbide reduced to the size of grit is moistened with a binder, such as the residue obtained by evaporating sulphite cellulose lye, and moulded into spherical or other forms. The latter are heated in a sand-carbon mixture or in a reducing atmosphere to temperatures of 2000--2600 DEG C., and recrystallization of the silicon carbide is effected with the formation of large crystals. Specifications 366,605 and 393,283 are referred to.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US429616XA | 1932-12-05 | 1932-12-05 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB429616A true GB429616A (en) | 1935-06-04 |
Family
ID=21924688
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB34081/33A Expired GB429616A (en) | 1932-12-05 | 1933-12-04 | Improved packing for fractionating columns |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB429616A (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5242626A (en) * | 1991-03-14 | 1993-09-07 | Zaidan Hojin Nanyo Kyokai | Process for contacting gas and liquid |
WO2006127671A3 (en) * | 2005-05-24 | 2007-04-26 | Crystaphase Products Inc | Separation method and assembly for process streams |
US10557486B2 (en) | 2016-02-12 | 2020-02-11 | Crystaphase Products, Inc. | Use of treating elements to facilitate flow in vessels |
US10744426B2 (en) | 2015-12-31 | 2020-08-18 | Crystaphase Products, Inc. | Structured elements and methods of use |
US11052363B1 (en) | 2019-12-20 | 2021-07-06 | Crystaphase Products, Inc. | Resaturation of gas into a liquid feedstream |
US11752477B2 (en) | 2020-09-09 | 2023-09-12 | Crystaphase Products, Inc. | Process vessel entry zones |
-
1933
- 1933-12-04 GB GB34081/33A patent/GB429616A/en not_active Expired
Cited By (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5242626A (en) * | 1991-03-14 | 1993-09-07 | Zaidan Hojin Nanyo Kyokai | Process for contacting gas and liquid |
US10500581B1 (en) | 2003-03-25 | 2019-12-10 | Crystaphase International, Inc. | Separation method and assembly for process streams in component separation units |
US10543483B2 (en) | 2003-03-25 | 2020-01-28 | Crystaphase International, Inc. | Separation method and assembly for process streams in component separation units |
US10525456B2 (en) | 2003-03-25 | 2020-01-07 | Crystaphase International, Inc. | Separation method and assembly for process streams in component separation units |
US7722832B2 (en) | 2003-03-25 | 2010-05-25 | Crystaphase International, Inc. | Separation method and assembly for process streams in component separation units |
US20100243519A1 (en) * | 2003-03-25 | 2010-09-30 | Glover John N | Separation Method and Assembly for Process Streams in Component Separation Units |
US10421067B2 (en) * | 2003-03-25 | 2019-09-24 | Crystaphase International, Inc. | Separation method and assembly for process streams in component separation units |
US10421068B2 (en) | 2003-03-25 | 2019-09-24 | Crystaphase International, Inc. | Separation method and assembly for process streams in component separation units |
EP3040119A1 (en) * | 2005-05-24 | 2016-07-06 | Crystaphase International, Inc. | Separation method and assembly for process streams in component separation units |
JP2008545527A (en) * | 2005-05-24 | 2008-12-18 | クリスタフエーズ・インターナシヨナル・インコーポレーテツド | Separation method and assembly for a process stream in a component separator |
WO2006127671A3 (en) * | 2005-05-24 | 2007-04-26 | Crystaphase Products Inc | Separation method and assembly for process streams |
US11000785B2 (en) | 2015-12-31 | 2021-05-11 | Crystaphase Products, Inc. | Structured elements and methods of use |
US10744426B2 (en) | 2015-12-31 | 2020-08-18 | Crystaphase Products, Inc. | Structured elements and methods of use |
US10655654B2 (en) | 2016-02-12 | 2020-05-19 | Crystaphase Products, Inc. | Use of treating elements to facilitate flow in vessels |
US10662986B2 (en) | 2016-02-12 | 2020-05-26 | Crystaphase Products, Inc. | Use of treating elements to facilitate flow in vessels |
US10738806B2 (en) | 2016-02-12 | 2020-08-11 | Crystaphase Products, Inc. | Use of treating elements to facilitate flow in vessels |
US10876553B2 (en) | 2016-02-12 | 2020-12-29 | Crystaphase Products, Inc. | Use of treating elements to facilitate flow in vessels |
US10920807B2 (en) | 2016-02-12 | 2021-02-16 | Crystaphase Products, Inc. | Use of treating elements to facilitate flow in vessels |
US10557486B2 (en) | 2016-02-12 | 2020-02-11 | Crystaphase Products, Inc. | Use of treating elements to facilitate flow in vessels |
US11156240B2 (en) | 2016-02-12 | 2021-10-26 | Crystaphase Products, Inc. | Use of treating elements to facilitate flow in vessels |
US11754100B2 (en) | 2016-02-12 | 2023-09-12 | Crystaphase Products, Inc. | Use of treating elements to facilitate flow in vessels |
US11052363B1 (en) | 2019-12-20 | 2021-07-06 | Crystaphase Products, Inc. | Resaturation of gas into a liquid feedstream |
US11752477B2 (en) | 2020-09-09 | 2023-09-12 | Crystaphase Products, Inc. | Process vessel entry zones |
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