[go: up one dir, main page]

GB248375A - Improvements in the preparation and treatment of olefines - Google Patents

Improvements in the preparation and treatment of olefines

Info

Publication number
GB248375A
GB248375A GB5268/26A GB526826A GB248375A GB 248375 A GB248375 A GB 248375A GB 5268/26 A GB5268/26 A GB 5268/26A GB 526826 A GB526826 A GB 526826A GB 248375 A GB248375 A GB 248375A
Authority
GB
United Kingdom
Prior art keywords
acid
treatment
olefines
tank
tertiary
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB5268/26A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
PETROLEUM CHEMICAL CORP
Original Assignee
PETROLEUM CHEMICAL CORP
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by PETROLEUM CHEMICAL CORP filed Critical PETROLEUM CHEMICAL CORP
Publication of GB248375A publication Critical patent/GB248375A/en
Expired legal-status Critical Current

Links

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

248,375. Petroleum Chemical Corporation, (Assignees of Davis, H. S., and Murray, W. J.). Feb. 24, 1925, [Convention date]. Olefines; sulphates, ethereal; monohydric alcohols; amyl chlorides.-A mixture of olefines obtained, for example, by cracking petroleum vapours and containing ethylene is fractionated and each fraction is separately treated with an acid reagent, preferably in a selective manner, for the production of derivatives. To obtain the olefine mixtures, gas oil from a tank 1 is cracked, after preliminary vaporization, in a tube 7 at a temperature of 600-659‹ C., and the products, after treatment in a separator 8, traverse towers 11, 12, a condenser 13, and a cooler 18. The tower 12 is fed with the condensate from the condenser 13 and the tower 11 with the bulk of the condensate from the tower 12 part of which is, however, stripped of its lighter hydrocarbons in a tower 12<a>. The uncondensed effluent from the cooler 18 constitutes the olefme mixture, which is scrubbed in towers 20, 21 by cool oil delivered from a tank 23; the unabsorbed residue, consisting mainly of ethylene and propylene, is collected in a holder 22. The saturated oil leaving the tank 20 passes through a still 29 and vaporizer 30 to a tower 31 in which the dissolved olefines are separated. These may be separated together or may be treated in a condenser 34, separator 35, compressor 36 and storage tank 37 to yield a condensate, comprising mainly amylenes, which is collected in a tank 17, and an uncondensed residue, consisting mainly of butylenes, which is collected in a holder 40. Alternatively, the olefine mixture from the cooler 18 may be fractionated by compression followed by distillation. The ethylene-propylene fraction collected in the holder 22 may be subjected to successive treatments with sulphuric acid. In the first treatment, with acid of 80-84 per cent strength, any olefines higher than propylene in. cidentally present are removed, while in the second treatment, with more concentrated acid, propylene is absorbed; the ethylene remains substantially unaffected and may be in turn absorbed in hot sulphuric acid. The products may be hydrolyzed to yield, particularly, ethyl and isopropyl alcohols. The butylene fraction collected in the holder 40 may be similarly treated. In the first treatment, with acid of about 60 per cent strength, isobutylene is removed and any diolefines incidentally present are polymerized, while in the second treatment, with acid of about 80 per cent strength, the remaining butylenes are absorbed. The products on hydrolysis yield tertiary and secondary butyl alcohols which may be distilled off preferably, in the case of the tertiary compound, after neutralization of the liquor. The amylene fraction collected in the tank 17 may similarly be treated with sulphuric acid in stages. The first treatment absorbs the amylenes convertible into tertiary derivatives, together with any isobutylene. diolefines, and acetylenic hydrocarbons incidentally present. In the second treatment, with stronger acid, the remaining amylenes, together with secondary hexylenes &c. are absorbed. The corresponding alcohols may be obtained by dilution and distillation, preferably, in the case of the tertiary alcohols, after neutralization. Alternatively, the amylene fraction may be distilled, into fractions comprising (a) isopropylethylene, (b) the remaining amylenes, and (c) hexylenes and higher olefines. which fractions may be separately treated. Fraction (b) may be treated with concentrated hydrochloric acid, whereon the amylenes which are convertible into tertiary derivatives, together with diolefines &c., are converted into easily separable chlorides which may be hydrolyzed, preferably with the addition of alkali, to yield tertiary alcohols.
GB5268/26A 1925-02-24 1926-02-24 Improvements in the preparation and treatment of olefines Expired GB248375A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US248375XA 1925-02-24 1925-02-24

Publications (1)

Publication Number Publication Date
GB248375A true GB248375A (en) 1927-01-27

Family

ID=21822656

Family Applications (1)

Application Number Title Priority Date Filing Date
GB5268/26A Expired GB248375A (en) 1925-02-24 1926-02-24 Improvements in the preparation and treatment of olefines

Country Status (1)

Country Link
GB (1) GB248375A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4552090A (en) * 1984-02-29 1985-11-12 Fabricated Metals, Inc. Bulk material container with a rigid follower

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4552090A (en) * 1984-02-29 1985-11-12 Fabricated Metals, Inc. Bulk material container with a rigid follower

Similar Documents

Publication Publication Date Title
GB248375A (en) Improvements in the preparation and treatment of olefines
US2271092A (en) Process for preparing alkyl sulphate liquors
US2094546A (en) Manufacture of alkyl sulphates
US2474568A (en) Dilution and hydrolysis of diethyl sulfate solutions
US1465600A (en) Process of separating olefines from gaseous mixtures
US2541673A (en) Weak-acid isopropanol process
US3203872A (en) Secondary butanol purification process
US1919618A (en) Process of making ethyl alcohol
US2081166A (en) Process of making alcohols by use of ethyl sulphuric acid
US2668863A (en) Purification of alcohols
US2106877A (en) Process of producing alcohols from
DE2049049C3 (en) Process for the production of isoprene from isobutene
US2035449A (en) Purifying naphtha
US2058851A (en) Process for sulphating mixtures of olefines
US1745028A (en) Process of converting gaseous aliphatic ethylene hydrocarbons into liquid hydrocarbons
US2514291A (en) Production of secondary butyl alcohol
US2809927A (en) Separation of sec-butyl ether from polymeric hydrocarbons
US1809788A (en) Method for production of alcohols from olefines
US2937714A (en) Process for the separation of acetylene and olefins
US2962537A (en) Removal of sulfur contaminants from hydrocarbon streams
SU72784A1 (en) The method of obtaining trimethylcarbinol
US2158559A (en) Production of motor fuel
US1729782A (en) Separation of olefines from petroleum products
US2066461A (en) Process of separating and recovering hydrocarbons and alkyl esters from mixtures thereof
US2015223A (en) Recovery of ethylene