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GB224913A - Improvements in or relating to the manufacture of alkyl resorcinols - Google Patents

Improvements in or relating to the manufacture of alkyl resorcinols

Info

Publication number
GB224913A
GB224913A GB27259/24A GB2725924A GB224913A GB 224913 A GB224913 A GB 224913A GB 27259/24 A GB27259/24 A GB 27259/24A GB 2725924 A GB2725924 A GB 2725924A GB 224913 A GB224913 A GB 224913A
Authority
GB
United Kingdom
Prior art keywords
pure
propyl
purifying
resorcinol
butyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB27259/24A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sharp and Dohme Inc
Original Assignee
Sharp and Dohme Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sharp and Dohme Inc filed Critical Sharp and Dohme Inc
Publication of GB224913A publication Critical patent/GB224913A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/02Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with no unsaturation outside the aromatic ring
    • C07C39/08Dihydroxy benzenes; Alkylated derivatives thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

n-Propyl and n-butyl resorcinols are prepared in a pure state, for use for example therapeutically, by heating resorcinol with pure propionic or pure n-butyric acid in presence of a condensing agent, such as zinc chloride, separating and purifying the intermediate ketone, reducing it, such as by zinc amalgam and hydrochloric acid, and finally purifying the resulting n-propyl or n-butyl resorcinol by vacuum distillation and recrystallization from benzene. The intermediate ketone may be purified by distillation in vacuo. An example shows the preparation of the n-propyl body. The Specification as open to inspection under Sect. 91 (3) (a) is not limited to the use of the pure acids and refers also to other methods of purifying the final alkyl resorcinol. This subject-matter does not appear in the Specification as accepted.
GB27259/24A 1923-07-31 1923-11-28 Improvements in or relating to the manufacture of alkyl resorcinols Expired GB224913A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US224913XA 1923-07-31 1923-07-31

Publications (1)

Publication Number Publication Date
GB224913A true GB224913A (en) 1925-04-28

Family

ID=21809876

Family Applications (1)

Application Number Title Priority Date Filing Date
GB27259/24A Expired GB224913A (en) 1923-07-31 1923-11-28 Improvements in or relating to the manufacture of alkyl resorcinols

Country Status (1)

Country Link
GB (1) GB224913A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5325479A (en) * 1989-05-08 1994-06-28 Apple Computer, Inc. Method and apparatus for moving control points in displaying digital typeface on raster output devices

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5325479A (en) * 1989-05-08 1994-06-28 Apple Computer, Inc. Method and apparatus for moving control points in displaying digital typeface on raster output devices

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