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GB2071518A - Elutriators - Google Patents

Elutriators Download PDF

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Publication number
GB2071518A
GB2071518A GB8106811A GB8106811A GB2071518A GB 2071518 A GB2071518 A GB 2071518A GB 8106811 A GB8106811 A GB 8106811A GB 8106811 A GB8106811 A GB 8106811A GB 2071518 A GB2071518 A GB 2071518A
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GB
United Kingdom
Prior art keywords
filter
elutriator
passageway
air
instrument
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
GB8106811A
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GB2071518B (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NAT RES DEV
National Research Development Corp of India
Original Assignee
NAT RES DEV
National Research Development Corp of India
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NAT RES DEV, National Research Development Corp of India filed Critical NAT RES DEV
Priority to GB8106811A priority Critical patent/GB2071518B/en
Publication of GB2071518A publication Critical patent/GB2071518A/en
Application granted granted Critical
Publication of GB2071518B publication Critical patent/GB2071518B/en
Expired legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D39/00Filtering material for liquid or gaseous fluids
    • B01D39/14Other self-supporting filtering material ; Other filtering material
    • B01D39/16Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres
    • B01D39/1669Cellular material
    • B01D39/1676Cellular material of synthetic origin
    • AHUMAN NECESSITIES
    • A62LIFE-SAVING; FIRE-FIGHTING
    • A62BDEVICES, APPARATUS OR METHODS FOR LIFE-SAVING
    • A62B23/00Filters for breathing-protection purposes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2202Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
    • G01N1/2205Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling with filters
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2202Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
    • G01N2001/222Other features
    • G01N2001/2223Other features aerosol sampling devices

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  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biomedical Technology (AREA)
  • Emergency Management (AREA)
  • Engineering & Computer Science (AREA)
  • Business, Economics & Management (AREA)
  • Molecular Biology (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Filtering Materials (AREA)

Abstract

An elutriator is provided comprising a filter formed by a random fibrous network having interstices of such size and distribution as to capture a major proportion of the non-respirable airborne particles in an air flow therethrough within a prescribed range of velocity for which particle capture is predominantly by inertial impaction. The filter suitably comprises porous foamed plastics material, preferably in a structure of contiguous layers having successively changing pore sizes and distribution, preferably of a polyester, and preferably having an oil coating. The filter will normally have a penetration function approximating the so-called Johannesburg curve, and is suitably employed as a pre-filter in a gravimetric particle sampling instrument.

Description

SPECIFICATION Elutriators Airborne dust in a working environment may be inhaled by workers and cause respiratory impairment. It is accordingly appropriate in some circumstances to limit the concentration of airborne dust to a level which is considered tolerable: indeed this is a legal requirement in some industrial situations.
This, in turn, leads to a requirement to sample the air and measure the concentration of hazardous dust particles in order to assess whether a given environment is tolerable or not.
In circumstances where the dust concentration varies from point to point in the working environment, it may be necessary for sampling instruments to be carried or worn by the workers and such personal instruments, together with associated power supplies, must necessarily be small and lightweight to be acceptable. A widely used technique employed for such personal instruments is to draw air at a controlled rate through a piece of filter material of known weight and then to weigh the filter material after a measured period of time to determine from the increase in weight, the air flow rate, and period of use, the weight of airborne dust per unit volume of air.However, because of the limitations on sizes and weight such personal gravimetric sampling instruments can only operate at a small airflow rate, the weight of collected dust over a reasonable period of time is correspondingly small, and so precise weighing is required if suitably accurate results are to be obtained. These instruments accordingly require specialist attention and are costly to employ.
Similar considerations of size and weight can also apply to gravimetric sampling instruments for use at a fixed point if the instrument, with its power supply has to be carried any relatively long distance to the sampling point, as can be the case in mining, or if use of a large instrument could impede working operations.
A further requirement for a dust sampling instrument in many instances is that the instrument should sample only dust particles that are small enough to reach the lungs in order to provide a more accurate measure of the respirable hazard. This requirement is commonly met by the use of one of two forms of size selector, usually termed an elutriator. One such form is a so-called parallel plate elutriator in which air flow to a sampling instrument is first passed between horizontal parallel plates having a length and spacing such that the larger, non-respirable particles of airborne dust have time to deposit therebetween rather than continue to the sampler.
The other form of elutriator involves a cyclone in which air is caused to rotate and deposit nonrespirable particles by centrifugal force.
The size of both of these forms of elutriator increases with the air flow rate capability thereof and so, again, is subject to limitation in many situations requiring dust sampling. A further disadvantage in the case of parallel plate elutriators is the inherent requirement to maintain the plates horizontal, and this renders such elutriators unsuitable for incorporation in a personal dust sampling instrument.
An object of the present invention is to improve the above situation by providing an elutriator, and also a particle sampling instrument incorporating the same, operable at higher air flow rates, without suffering disadvantages of size and weight.
In a more general aspect the present invention provides an elutriator comprising a filter formed by a random fibrous network having interstices of such size and distribution as to capture a major proportion of the non-respirable airborne particles in an air flow therethrough within a prescribed range of velocity for which particle capture is predominantly by inertial impaction. In this connection it is to be understood that particle capture in a filter can involve both sedimentation and inertial impaction, but that the latter dominates at higher air flow velocities.
While the filter can be formed by a mat of discrete fibres, it suitably comprises porous foam plastics material and in a presently preferred form comprises a structure of contiguous layers of such material having successively changing pore size and distribution therethrough from one layer to the next. Also, the foam material is preferably a polyester for consistency, and may be provided with an oil coating.
Also, the filter can, and for most purposes will, have a penetration function which approximates the so-called Johannesburg curve (which defines a penetration function recommended by a pneumoconiosis conference in Johannesburg in 1959, and was reported in the conference proceeding by Orenstein, 1960).
The proposed elutriator will, as is evident from the foregoing introductory discussion, commonly be used in association with a particle sampling instrument and this conveniently involves incorporation of the elutriator as a pre-filter in a gravimetric sampling instrument.
In this last connection, the present invention accordingly provides in a more particular aspect thereof, a gravimetric particle sampling instrument comprising a housing defining an air passageway therethrough and having mounted therein an electric fan to draw and pass air into and through said passageway, a main filter across the passageway to collect respirable particles borne by such air, and a pre-filter of the presently proposed elutriator form located across the passageway upstream of the main filter to collect non-respirable particles borne by said air.
The main filter is suitably of bag form and the fan of axial type, but alternatives are possible.
The proposed instrument can, of course, be employed for fixed site sampling, but it is particularly advantageous for personal mobile use.
In the latter case the instrument can be beneficially incorporated in a helmet according to UK Patent No. 1,426,432 or 1,495,020 in which a bag filter and fan are already provided to supply the user with respiration air.
In order that the invention may be more fully understood and readily carried into effect, the same will now be described further by way of example and with reference to the accompanying drawings, in which:~ Figure 1 graphically illustrates the Johannesburg curve and related penetration characteristics respectively of an elutriator according to the invention and a cyclone elutriator, Figure 2 schematically illustrates one form of sampling instrument according to the invention, and Figure 3 similarly illustrates another such form of instrument.
In Figure 1 the solid line trace is the Johnannesburg curve, which shows the penetra tion of unit density spheres through an idealised parallel plate elutriator as a function of the sphere diameter, penetration and diameter being represented respectively by the vertical axis P and the horizontal axis D. The penetration value of the function for any particle is equal to that for a unit density sphere having the same settling velocity as the particle.
The related penetration characteristics represented by the crosses in Figure 1 are those for an elutriator according to the invention. This elutriator comprised 3 porous polyester foam filter having pore size of approximately 0.3mm, 32000 pores per metre (ppm), and being 7mm thick. The results of Figure 1 were obtained by application to the filter at a velocity of 20 cm ~ s~1, of monodisperse aerosols of sucrose of between 2 and 11 micrometres diameter. These aerosols were produced by a vibrating orifice aerosol generator, made electrically neutral by a small radio-active source and detected by an optical particle counter. Initially, large particles were not captured efficiently - seemingly because of failure to adhere on contact.However, this was corrected by immersing the foam in a mixture of low vapour pressure oil and alcohol, and allowing the alcohol to evaporate and to leave a thin-film of oil on the fibres of the foam. It appears that porous foam materials more readily retain such a coating than do filters of discrete fibres. This is thought to arise from the fact that creation of the porous foam interstices by multiple spherical expansions within the initial body of material produces fibres seen to be of generally triangular cross-section with concavely curved sides, and this concavity affords better retention than in a discrete fibre of circular or other wholly convex cross-section.
The related transfer characteristics represented by the dots in Figure 1 are those for a cyclone elutriator (Maguire et al, 1973, Staub 33,95) and are shown for comparative purposes.
Clearly, from Figure 1 , an elutriator of the presently proposed form can provide penetration characteristics which closely approximate to the Johannesburg curve and are comparable with those of existing, alternative forms.
The foam filter referred to in connection with Figure 1 was in fact an earlier form tested during development of the invention, and development has continued with the use of filters comprising contiguous layers of foam material having successively varying characteristics from one layer to the next. These multi-layer filters can give further improved results.
For example one such multi-layer filter comprised five successive layers of porous foam as above but with differing characteristics as follows: 12mm thickness having 400ppm, 12mm of 800 ppm, 9mm of 1200 ppm, 6mm of 1800 ppm, and 4mm of 3200 ppm. An area of 1 250mm2 of this filter could collect 1.5gm of a given dust before the collection characteristics changed by 10% i.e. the integrated weight of dust penetrating the filter becomes 10% less than it would be with a clean filter. This can be compared with the performance of a single layer foam filter of a thickness to give the same initial performance but collecting only about 0.25gm of the dust before its collection characteristic suffered a 10% change.
Turning to practical application of the invention: it has been indicated that this can involve incorporation as a pre-filter in a gravimetric particle sampling instrument and Figure 2 schematically illustrates one form of such an instrument suitable for fixed site or personal use.
The instrument of Figure 2 comprises a generally tubular housing 10 defining an air passageway therethrough, the housing having a narrower intermediate portion 11 flaring outwardly at its opposite ends to diametrally enlarged end portions 12 and 13. The housing portion 11 carried a battery-operable axial fan 14 therein, the batteries being located in a compartment formed with the housing or in a separate compartment having a lead connection to the fan. A pre-filter elutriator 15 according to the invention is located in the open end of housing portion 12, where it is retained by a grill 16. This open end may have a protective cover 17 releasably connected thereto in a spaced disposition above and around the end to define a generally inverted dish-shaped air inlet channel as indicated by arrows. The remaining housing portion 13 is elongated and surrounds, as a protective cover, a bag filter 18 suspended therein with its mouth uppermost to receive air blown by the fan. Portion 13 is suitably releasable to facilitate insertion and removal of the bag filter.
The instrument is intended to be used generally upright as illustrated with the lower open end of the portion 13 clear of the ground or other obstructions. This can be effected in any suitable manner at a fixed site. Alternatively, the instrument can be suspended in front of a worker by use of straps passing around his neck and waist.
The fan is suitably of axial form, which is likely to be simpler than an alternative form such as a centrifugal fan.
Figure 3 schematically Ilustrates yet another form of gravimetric particle sampling instrument which in this case is specifically intended for personal use by incorporation in a helmet. The helmet in fact accords with the afore-mentioned Patents and requires no detailed description thereover other than to note that the present invention provides in the helmet a pre-filter elutriator 20, battery-operable axial fan 21, and a bag filter 22, these items being located in a passageway leading through the helmet from its rear, between the helmet outer shell 23 and inner shell or harness 24, and then forwardly and downwardly behind a visor 25 to atmosphere, the filtered air serving for respiration by the user.
While reference has been made to the use of a bag form for the main, respirable particle filter, alternative forms can be used involving flat, pleated or other structures.

Claims (9)

1. An elutriator comprising a filter formed by a random fibrous network having interstices of such size and distribution as to capture a major proportion of the non-respirable airborne particles in an air flow therethrough within a prescribed range of velocity for which particle capture is predominantly by inertial impaction
2. An elutriator according to Claim 1 wherein said network is formed by a porous foamed plastics material.
3. An elutriator according to Claim 2 wherein said network is formed by a structure of contiguous layers of said material having successively changed pore sizes and distribution therethrough.
4. An elutriator according to Claim 2 or 3 wherein said material is a polyester.
5. An elutriator according to Claims 2, 3 or 4 wherein said material has an oil coating.
6. An elutriator according to any preceding claim having a penetration function which approximates the Johannesburg curve.
7. A gravimetric particle sampling instrument comprising a housing defining an air passageway therethrough, an electric fan mounted in said passageway to draw and pass air into and through said passageway, a main filter located across said passageway to collect respirable particles borne by said air passing therethrough, and a pre-filter according to any preceding claim located across said passageway upstream of said main filter to collect non-respirable particles borne by said air passing therethrough.
8. An instrument according to Claim 7 wherein said housing is in the form of a helmet.
9. An instrument according to Claim 7 or 8 wherein said main filter is of bag form located downstream of said fan, and said pre-filter is located upstream of said fan.
GB8106811A 1980-03-04 1981-03-04 Elutriators Expired GB2071518B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB8106811A GB2071518B (en) 1980-03-04 1981-03-04 Elutriators

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB8007385 1980-03-04
GB8106811A GB2071518B (en) 1980-03-04 1981-03-04 Elutriators

Publications (2)

Publication Number Publication Date
GB2071518A true GB2071518A (en) 1981-09-23
GB2071518B GB2071518B (en) 1984-03-14

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2172814A (en) * 1985-03-26 1986-10-01 Pipercross Ltd Air filter element
GB2204810A (en) * 1987-05-21 1988-11-23 Icleen Umweltprod Schaan Air filter
FR2660873A1 (en) * 1990-04-17 1991-10-18 Graseby Ionics Ltd SPRAY.
EP0462477A2 (en) * 1990-06-19 1991-12-27 Mine Safety Appliances Company Cover assembly and pre-filter for a respirator
EP0572945A1 (en) * 1992-06-02 1993-12-08 Fraunhofer-Gesellschaft Zur Förderung Der Angewandten Forschung E.V. Dust collector
EP0837312A1 (en) * 1996-10-16 1998-04-22 Institute of Occupational Safety and Health, Council of Labor Affairs Method and device for aerosol size-selective sampling
US6575165B1 (en) 2000-08-03 2003-06-10 3M Innovative Properties Company Apparatus and method for breathing apparatus component coupling
US7458284B2 (en) * 2006-05-19 2008-12-02 Institute Of Occupational Safety And Health, Council Of Labor Affairs Three-stage dust sampler

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2172814A (en) * 1985-03-26 1986-10-01 Pipercross Ltd Air filter element
GB2204810A (en) * 1987-05-21 1988-11-23 Icleen Umweltprod Schaan Air filter
FR2660873A1 (en) * 1990-04-17 1991-10-18 Graseby Ionics Ltd SPRAY.
EP0462477A2 (en) * 1990-06-19 1991-12-27 Mine Safety Appliances Company Cover assembly and pre-filter for a respirator
EP0462477A3 (en) * 1990-06-19 1992-05-20 Mine Safety Appliances Company Cover assembly and pre-filter for a respirator
EP0572945A1 (en) * 1992-06-02 1993-12-08 Fraunhofer-Gesellschaft Zur Förderung Der Angewandten Forschung E.V. Dust collector
EP0837312A1 (en) * 1996-10-16 1998-04-22 Institute of Occupational Safety and Health, Council of Labor Affairs Method and device for aerosol size-selective sampling
US6575165B1 (en) 2000-08-03 2003-06-10 3M Innovative Properties Company Apparatus and method for breathing apparatus component coupling
US7458284B2 (en) * 2006-05-19 2008-12-02 Institute Of Occupational Safety And Health, Council Of Labor Affairs Three-stage dust sampler

Also Published As

Publication number Publication date
GB2071518B (en) 1984-03-14

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Legal Events

Date Code Title Description
732 Registration of transactions, instruments or events in the register (sect. 32/1977)
PCNP Patent ceased through non-payment of renewal fee

Effective date: 19960304