[go: up one dir, main page]

GB1430288A - Prepration of sucrose derivatives - Google Patents

Prepration of sucrose derivatives

Info

Publication number
GB1430288A
GB1430288A GB4998573A GB4998573A GB1430288A GB 1430288 A GB1430288 A GB 1430288A GB 4998573 A GB4998573 A GB 4998573A GB 4998573 A GB4998573 A GB 4998573A GB 1430288 A GB1430288 A GB 1430288A
Authority
GB
United Kingdom
Prior art keywords
product
hexaacetate
sucrose
stage
acetylated
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4998573A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tate and Lyle PLC
Original Assignee
Tate and Lyle PLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate and Lyle PLC filed Critical Tate and Lyle PLC
Priority to GB4998573A priority Critical patent/GB1430288A/en
Priority to DE19742449870 priority patent/DE2449870C3/en
Priority to CA211,989A priority patent/CA1020161A/en
Priority to IE217674A priority patent/IE40084B1/en
Priority to JP12155974A priority patent/JPS555519B2/ja
Priority to CH1425974A priority patent/CH609063A5/en
Priority to DK560274A priority patent/DK134649B/en
Priority to IT7018474A priority patent/IT1024697B/en
Priority to BE149888A priority patent/BE821491A/en
Priority to LU71183A priority patent/LU71183A1/xx
Priority to NL7414081A priority patent/NL7414081A/en
Publication of GB1430288A publication Critical patent/GB1430288A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Saccharide Compounds (AREA)

Abstract

6,6'-Dichloro-6,6'-dideoxysucrose is prepared by the following reaction steps: a) reaction of sucrose with methanesulphonyl chloride in N,N-dimethylformamide, b) complete acetylation of the resulting chlorinated sucrose and isolation of the acetylated product containing 6,6'-dichloro-6,6'-dideoxysucrose hexaacetate, c) purification of the said hexaacetate and d) deacetylation of the purified hexaacetate. To suppress the formation of a trichlorinated by-product, it is advantageous to allow the reaction in stage a) to start at a temperature in the range from -40 to -15 DEG C. In order, furthermore, to remove any formate by-products which are present in the product, it is advisable for the acetylated product which has been obtained in stage b) to be deacetylated before the purification stage c) and subsequently acetylated once again. The product prepared according to the invention is used as intermediate for the preparation of sucrose derivatives which are required, for example, for the preparation of resins.
GB4998573A 1973-10-26 1973-10-26 Prepration of sucrose derivatives Expired GB1430288A (en)

Priority Applications (11)

Application Number Priority Date Filing Date Title
GB4998573A GB1430288A (en) 1973-10-26 1973-10-26 Prepration of sucrose derivatives
DE19742449870 DE2449870C3 (en) 1973-10-26 1974-10-21 Process for the preparation of 6,6'-dichloro-6,6'-dideoxy-sucrose
CA211,989A CA1020161A (en) 1973-10-26 1974-10-22 Preparation of sucrose derivatives
IE217674A IE40084B1 (en) 1973-10-26 1974-10-22 Preparation of sucrose derivatives
JP12155974A JPS555519B2 (en) 1973-10-26 1974-10-23
CH1425974A CH609063A5 (en) 1973-10-26 1974-10-24 Process for the preparation of sucrose derivatives
DK560274A DK134649B (en) 1973-10-26 1974-10-25 Process for the preparation of 6,6'-dichloro-6,6'-didesoxysaccharose, neat or mixed with 1 ', 6,6'-trichloro-1', 6,6'-tridesoxysaccharose.
IT7018474A IT1024697B (en) 1973-10-26 1974-10-25 PROCEDURE FOR THE PREPARATION OF SUCROSE DERIVATIVES, PARTICULARLY USEFUL AS INTERMEDIATES IN THE PRODUCTION OF SYNTHETIC RESINS
BE149888A BE821491A (en) 1973-10-26 1974-10-25 PREPARATION OF SUCROSE DERIVATIVES
LU71183A LU71183A1 (en) 1973-10-26 1974-10-25
NL7414081A NL7414081A (en) 1973-10-26 1974-10-28 PROCESS FOR PREPARING SUCROSE COMPOUNDS.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB4998573A GB1430288A (en) 1973-10-26 1973-10-26 Prepration of sucrose derivatives

Publications (1)

Publication Number Publication Date
GB1430288A true GB1430288A (en) 1976-03-31

Family

ID=10454222

Family Applications (1)

Application Number Title Priority Date Filing Date
GB4998573A Expired GB1430288A (en) 1973-10-26 1973-10-26 Prepration of sucrose derivatives

Country Status (11)

Country Link
JP (1) JPS555519B2 (en)
BE (1) BE821491A (en)
CA (1) CA1020161A (en)
CH (1) CH609063A5 (en)
DE (1) DE2449870C3 (en)
DK (1) DK134649B (en)
GB (1) GB1430288A (en)
IE (1) IE40084B1 (en)
IT (1) IT1024697B (en)
LU (1) LU71183A1 (en)
NL (1) NL7414081A (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4435440A (en) * 1976-01-08 1984-03-06 Tate & Lyle Limited Sweeteners

Also Published As

Publication number Publication date
CH609063A5 (en) 1979-02-15
DK134649B (en) 1976-12-13
NL7414081A (en) 1975-04-29
DE2449870C3 (en) 1980-09-11
DE2449870B2 (en) 1980-01-17
DK134649C (en) 1977-05-16
IE40084B1 (en) 1979-03-14
IE40084L (en) 1975-04-26
JPS5071612A (en) 1975-06-13
IT1024697B (en) 1978-07-20
BE821491A (en) 1975-04-25
DK560274A (en) 1975-06-16
CA1020161A (en) 1977-11-01
DE2449870A1 (en) 1975-04-30
JPS555519B2 (en) 1980-02-07
LU71183A1 (en) 1975-04-17

Similar Documents

Publication Publication Date Title
JPS55130937A (en) Preparation of ester
ATE7688T1 (en) 2.3-DIALKOXYPROPYLGLYCERYL ETHER, PROCESS FOR THEIR PREPARATION AND COSMETIC COMPOSITION CONTAINING THEM.
SE8200518L (en) MANUFACTURE OF OLD PYRONS
GB965637A (en) L-ornithine l-aspartate
GB1430288A (en) Prepration of sucrose derivatives
ATE111108T1 (en) PROCESS FOR PRODUCTION OF CYCLOOCTAAMYLOSE.
IT1008711B (en) PROCEDURE FOR PREPARING M PHENOXYLBENZYL ALCOHOL AND ITS DERIVATIVES
GB952805A (en) Process for the production of isocyanide dichloride derivatives
Bouveng et al. Synthesis and paper electrophoresis of the galactose monomethyl ethers
US2750418A (en) Production of unsaturated 1, 4-dicarbonyl compounds
IE43625L (en) Phosphorus compounds containing carboxylic groups.
ATE10487T1 (en) PROCESS FOR THE PREPARATION OF ANHYDROUS 2HYDROXY-3-CHLORPROPYLTRIALKYLAMMONIUM CHLORIDE.
GB992742A (en) Preparation of permonosulphates
GB1323478A (en) Process of preparing polyalkylenglycol dibenzoates
GB878737A (en) Preparation of alkyl chlorides
KR920014762A (en) Process for preparing dialkylaminopropanediol
SE7605928L (en) WAY TO MAKE THE 1.5 AND 1,8-DIAMINON AGREEMENTS
US2022446A (en) Process of preparing organic cellulose esters
KR950016554A (en) Manufacturing method of processed rice and products containing same
KR930002388A (en) Catalysts used in the preparation of tertiary olefins from alkyl-tert-altyl ethers
US3948974A (en) Esterification of orthophthalic acid with olefin
US3686297A (en) {62 ,{62 ,{62 {40 -trichloro-{60 -hydroxy-iso-butyric acid
JPS55130994A (en) Novel maltosan derivative and its production
JPS5799544A (en) Preparation of chloroacetaldehyde
JPS5331628A (en) Isolation and purification of aromatic compounds with monohalogenated side chains

Legal Events

Date Code Title Description
429A Application made for amendment of specification (sect. 29/1949)
429H Application (made) for amendment of specification now open to opposition (sect. 29/1949)
429D Case decided by the comptroller ** specification amended (sect. 29/1949)
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee