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GB1382340A - Production of precipitated silica - Google Patents

Production of precipitated silica

Info

Publication number
GB1382340A
GB1382340A GB1988072A GB1988072A GB1382340A GB 1382340 A GB1382340 A GB 1382340A GB 1988072 A GB1988072 A GB 1988072A GB 1988072 A GB1988072 A GB 1988072A GB 1382340 A GB1382340 A GB 1382340A
Authority
GB
United Kingdom
Prior art keywords
acid
concentration
sio
addition
silicate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB1988072A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SIFRANCE
Original Assignee
SIFRANCE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SIFRANCE filed Critical SIFRANCE
Publication of GB1382340A publication Critical patent/GB1382340A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

1382340 Precipitated silica SOC FRANCAISE DES SILICATES SPECIAUX SIFRANCE 28 April 1972 [4 Nov 1971] 19880/72 Heading C1A In a method for producing silicas having a specific surface area of 100 to 600 in.<SP>2</SP>/g. which does not vary with drying by the action of strong acid on a sodium silicate, the addition of the acid to the silicate is interrupted upon 1 to 3 occasions, the first interruption taking place after the SiO 2 /Na 2 O molar ratio reaches a value of 5À5. Preferably the first interruption occurs when the ratio is 5À7 to 7 and the second when the ratio is 10 to 25. The rate of addition of the acid may be such that the variation of the alkalinity of the medium as a function of time is constant. The constant may be different in one acid adding phase from that in another. The process may be continuous or discontinuous. Preferably the silicate concentration is 100 to 200 g./litre with a SiO 2 /Na 2 O molar ratio of 1 to 4, the acid has a concentration such that the final SiO 2 concentration is 50 to 100 g./litre, the temperature is 40‹ to 95‹ C. and the total time for the acid addition is 40 to 180 minutes, the interruptions lasting 5 to 30 minutes.
GB1988072A 1971-11-04 1972-04-28 Production of precipitated silica Expired GB1382340A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7139477A FR2159580A5 (en) 1971-11-04 1971-11-04

Publications (1)

Publication Number Publication Date
GB1382340A true GB1382340A (en) 1975-01-29

Family

ID=9085273

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1988072A Expired GB1382340A (en) 1971-11-04 1972-04-28 Production of precipitated silica

Country Status (7)

Country Link
JP (1) JPS5621726B2 (en)
DE (1) DE2224061C3 (en)
ES (1) ES402045A1 (en)
FR (1) FR2159580A5 (en)
GB (1) GB1382340A (en)
IT (1) IT959114B (en)
NL (1) NL7204773A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111867974A (en) * 2018-08-06 2020-10-30 浙江三时纪新材科技有限公司 Novel precipitated white carbon black and preparation method thereof

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1478387A (en) * 1973-10-03 1977-06-29 Huber Corp J M Process for producing precipitated thickener silica
FR2353486A1 (en) 1976-06-04 1977-12-30 Rhone Poulenc Ind NEW AMORPHIC SYNTHETIC SILICA, PROCESS FOR OBTAINING AND APPLYING THE SAID SILICA IN VULCANISATES
FR2471949A1 (en) * 1979-12-20 1981-06-26 Rhone Poulenc Ind Fine silica prepn. - by reaction of alkali metal and acid using sequestering agent to complex with impurity metallic ions(BR 7.7.81)
FR2471947A1 (en) * 1979-12-20 1981-06-26 Rhone Poulenc Ind PRECIPITATION SILICE, IN PARTICULAR AS A REINFORCING LOAD
FR2471948A1 (en) * 1979-12-20 1981-06-26 Rhone Poulenc Ind Silica prepn. by reacting alkali metal silicate with acid - with intermediate dilution to improve washability of prod.(BR 7.7.81)
EP0784594A1 (en) * 1994-10-03 1997-07-23 Societe Chimique Prayon-Rupel Method for making phosphated alkaline salts, resulting salts and silicas, and detergent or foodstuff containing such salts
JP5502556B2 (en) * 2010-03-30 2014-05-28 大王製紙株式会社 Method for producing silica composite particles
JP5486377B2 (en) * 2010-03-31 2014-05-07 大王製紙株式会社 Method for producing silica composite mixed inorganic particles and silica composite mixed inorganic particles
US9695254B2 (en) 2012-11-26 2017-07-04 Braskem S.A. Metallocene catalyst supported by hybrid supporting means, process for producing same, polymerization process for producing an ethylene homopolymer or copolymer with broad or bimodal molar mass distribution, use of the supported metallocene catalyst and ethylene polymer with broad or bimodal molar mass distribution

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1001884A (en) * 1946-06-26 1952-02-28 Saint Gobain Powder silica manufacturing process
US3307906A (en) * 1965-05-24 1967-03-07 Jr Oliver W Burke Silica pigments and preparation thereof
US3503707A (en) * 1968-05-20 1970-03-31 Burke Oliver W Jun Silica pigments and preparation thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111867974A (en) * 2018-08-06 2020-10-30 浙江三时纪新材科技有限公司 Novel precipitated white carbon black and preparation method thereof
CN111867974B (en) * 2018-08-06 2022-11-01 浙江三时纪新材科技有限公司 Precipitated white carbon black and preparation method thereof

Also Published As

Publication number Publication date
IT959114B (en) 1973-11-10
JPS4853997A (en) 1973-07-28
DE2224061A1 (en) 1973-06-20
JPS5621726B2 (en) 1981-05-21
DE2224061C3 (en) 1982-05-19
FR2159580A5 (en) 1973-06-22
NL7204773A (en) 1973-05-08
DE2224061B2 (en) 1978-02-02
ES402045A1 (en) 1975-03-01

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee