GB1382340A - Production of precipitated silica - Google Patents
Production of precipitated silicaInfo
- Publication number
- GB1382340A GB1382340A GB1988072A GB1988072A GB1382340A GB 1382340 A GB1382340 A GB 1382340A GB 1988072 A GB1988072 A GB 1988072A GB 1988072 A GB1988072 A GB 1988072A GB 1382340 A GB1382340 A GB 1382340A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- concentration
- sio
- addition
- silicate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
- C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
1382340 Precipitated silica SOC FRANCAISE DES SILICATES SPECIAUX SIFRANCE 28 April 1972 [4 Nov 1971] 19880/72 Heading C1A In a method for producing silicas having a specific surface area of 100 to 600 in.<SP>2</SP>/g. which does not vary with drying by the action of strong acid on a sodium silicate, the addition of the acid to the silicate is interrupted upon 1 to 3 occasions, the first interruption taking place after the SiO 2 /Na 2 O molar ratio reaches a value of 5À5. Preferably the first interruption occurs when the ratio is 5À7 to 7 and the second when the ratio is 10 to 25. The rate of addition of the acid may be such that the variation of the alkalinity of the medium as a function of time is constant. The constant may be different in one acid adding phase from that in another. The process may be continuous or discontinuous. Preferably the silicate concentration is 100 to 200 g./litre with a SiO 2 /Na 2 O molar ratio of 1 to 4, the acid has a concentration such that the final SiO 2 concentration is 50 to 100 g./litre, the temperature is 40‹ to 95‹ C. and the total time for the acid addition is 40 to 180 minutes, the interruptions lasting 5 to 30 minutes.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7139477A FR2159580A5 (en) | 1971-11-04 | 1971-11-04 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1382340A true GB1382340A (en) | 1975-01-29 |
Family
ID=9085273
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1988072A Expired GB1382340A (en) | 1971-11-04 | 1972-04-28 | Production of precipitated silica |
Country Status (7)
Country | Link |
---|---|
JP (1) | JPS5621726B2 (en) |
DE (1) | DE2224061C3 (en) |
ES (1) | ES402045A1 (en) |
FR (1) | FR2159580A5 (en) |
GB (1) | GB1382340A (en) |
IT (1) | IT959114B (en) |
NL (1) | NL7204773A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111867974A (en) * | 2018-08-06 | 2020-10-30 | 浙江三时纪新材科技有限公司 | Novel precipitated white carbon black and preparation method thereof |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1478387A (en) * | 1973-10-03 | 1977-06-29 | Huber Corp J M | Process for producing precipitated thickener silica |
FR2353486A1 (en) | 1976-06-04 | 1977-12-30 | Rhone Poulenc Ind | NEW AMORPHIC SYNTHETIC SILICA, PROCESS FOR OBTAINING AND APPLYING THE SAID SILICA IN VULCANISATES |
FR2471949A1 (en) * | 1979-12-20 | 1981-06-26 | Rhone Poulenc Ind | Fine silica prepn. - by reaction of alkali metal and acid using sequestering agent to complex with impurity metallic ions(BR 7.7.81) |
FR2471947A1 (en) * | 1979-12-20 | 1981-06-26 | Rhone Poulenc Ind | PRECIPITATION SILICE, IN PARTICULAR AS A REINFORCING LOAD |
FR2471948A1 (en) * | 1979-12-20 | 1981-06-26 | Rhone Poulenc Ind | Silica prepn. by reacting alkali metal silicate with acid - with intermediate dilution to improve washability of prod.(BR 7.7.81) |
EP0784594A1 (en) * | 1994-10-03 | 1997-07-23 | Societe Chimique Prayon-Rupel | Method for making phosphated alkaline salts, resulting salts and silicas, and detergent or foodstuff containing such salts |
JP5502556B2 (en) * | 2010-03-30 | 2014-05-28 | 大王製紙株式会社 | Method for producing silica composite particles |
JP5486377B2 (en) * | 2010-03-31 | 2014-05-07 | 大王製紙株式会社 | Method for producing silica composite mixed inorganic particles and silica composite mixed inorganic particles |
US9695254B2 (en) | 2012-11-26 | 2017-07-04 | Braskem S.A. | Metallocene catalyst supported by hybrid supporting means, process for producing same, polymerization process for producing an ethylene homopolymer or copolymer with broad or bimodal molar mass distribution, use of the supported metallocene catalyst and ethylene polymer with broad or bimodal molar mass distribution |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1001884A (en) * | 1946-06-26 | 1952-02-28 | Saint Gobain | Powder silica manufacturing process |
US3307906A (en) * | 1965-05-24 | 1967-03-07 | Jr Oliver W Burke | Silica pigments and preparation thereof |
US3503707A (en) * | 1968-05-20 | 1970-03-31 | Burke Oliver W Jun | Silica pigments and preparation thereof |
-
1971
- 1971-11-04 FR FR7139477A patent/FR2159580A5/fr not_active Expired
-
1972
- 1972-03-27 IT IT6796872A patent/IT959114B/en active
- 1972-04-10 NL NL7204773A patent/NL7204773A/xx active Search and Examination
- 1972-04-24 ES ES402045A patent/ES402045A1/en not_active Expired
- 1972-04-28 GB GB1988072A patent/GB1382340A/en not_active Expired
- 1972-05-17 DE DE19722224061 patent/DE2224061C3/en not_active Expired
- 1972-07-20 JP JP7332872A patent/JPS5621726B2/ja not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111867974A (en) * | 2018-08-06 | 2020-10-30 | 浙江三时纪新材科技有限公司 | Novel precipitated white carbon black and preparation method thereof |
CN111867974B (en) * | 2018-08-06 | 2022-11-01 | 浙江三时纪新材科技有限公司 | Precipitated white carbon black and preparation method thereof |
Also Published As
Publication number | Publication date |
---|---|
IT959114B (en) | 1973-11-10 |
JPS4853997A (en) | 1973-07-28 |
DE2224061A1 (en) | 1973-06-20 |
JPS5621726B2 (en) | 1981-05-21 |
DE2224061C3 (en) | 1982-05-19 |
FR2159580A5 (en) | 1973-06-22 |
NL7204773A (en) | 1973-05-08 |
DE2224061B2 (en) | 1978-02-02 |
ES402045A1 (en) | 1975-03-01 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed | ||
PCNP | Patent ceased through non-payment of renewal fee |