GB1377841A - Preparation of hydrocarbon conversion catalysts - Google Patents
Preparation of hydrocarbon conversion catalystsInfo
- Publication number
- GB1377841A GB1377841A GB144772A GB144772A GB1377841A GB 1377841 A GB1377841 A GB 1377841A GB 144772 A GB144772 A GB 144772A GB 144772 A GB144772 A GB 144772A GB 1377841 A GB1377841 A GB 1377841A
- Authority
- GB
- United Kingdom
- Prior art keywords
- catalyst
- ammonium nitrate
- base
- ions
- hydrocarbon conversion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003054 catalyst Substances 0.000 title abstract 7
- 239000004215 Carbon black (E152) Substances 0.000 title abstract 3
- 238000006243 chemical reaction Methods 0.000 title abstract 3
- 229930195733 hydrocarbon Natural products 0.000 title abstract 3
- 150000002430 hydrocarbons Chemical class 0.000 title abstract 3
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 abstract 4
- 239000002585 base Substances 0.000 abstract 4
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 4
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 abstract 2
- 229910021536 Zeolite Inorganic materials 0.000 abstract 2
- 229910000323 aluminium silicate Inorganic materials 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- 150000002500 ions Chemical class 0.000 abstract 2
- 239000010457 zeolite Substances 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- JLVVSXFLKOJNIY-UHFFFAOYSA-N Magnesium ion Chemical compound [Mg+2] JLVVSXFLKOJNIY-UHFFFAOYSA-N 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 238000004517 catalytic hydrocracking Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- 239000012013 faujasite Substances 0.000 abstract 1
- -1 hydrogen ions Chemical class 0.000 abstract 1
- 229910001425 magnesium ion Inorganic materials 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229910052763 palladium Inorganic materials 0.000 abstract 1
- 239000002243 precursor Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/90—Regeneration or reactivation
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
- C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
- C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
- C10G47/12—Inorganic carriers
- C10G47/16—Crystalline alumino-silicate carriers
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Catalysts (AREA)
Abstract
1377841 Hydrocarbon conversion catalysts EXXON RESEARCH & ENG CO 12 Jan 1972 [18 Jan 1971] 1447/72 Heading B1E [Also in Division C5] A process for preparing an improved crystalline aluminosilicate zeolite-containing catalyst comprises contacting a crystalline aluminosilicate zeolite-containing catalyst which has become at least partially deactivated after being used in a hydrocarbon conversion process with a solution containing hydrogen ions, hydrogen precursor ions or a mixture of said ions such that the alkali metal content of said catalyst is reduced by at least 0.5 wt % based on the total weight of said partially deactivated catalyst. Examples relate to a synthetic faujasite base-exchanged with ammonium and magnesium ions, mixed with alumina and impregnated with palladium: this was used for hydrocracking and cylically regenerated by carbon bum-off until its activity was reduced by 53%. The used catalyst was treated by (Ex. 1A) one base exchange at room temperature with ammonium nitrate, and calcination; (Ex. 2A) three base exchanges with ammonium nitrate at room temperature; (Ex. 2B) three base exchanges with ammonium nitrate at 100‹F; and (Ex. 2C) one base exchange with ammonium nitrate at 180‹F.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10722471A | 1971-01-18 | 1971-01-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1377841A true GB1377841A (en) | 1974-12-18 |
Family
ID=22315519
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB144772A Expired GB1377841A (en) | 1971-01-18 | 1972-01-12 | Preparation of hydrocarbon conversion catalysts |
Country Status (2)
| Country | Link |
|---|---|
| CA (1) | CA1003392A (en) |
| GB (1) | GB1377841A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0204750A1 (en) * | 1984-11-08 | 1986-12-17 | Chevron Research Company | Rejuvenation of a deactivated catalyst |
-
1972
- 1972-01-11 CA CA132,178A patent/CA1003392A/en not_active Expired
- 1972-01-12 GB GB144772A patent/GB1377841A/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0204750A1 (en) * | 1984-11-08 | 1986-12-17 | Chevron Research Company | Rejuvenation of a deactivated catalyst |
| EP0204750A4 (en) * | 1984-11-08 | 1987-12-02 | Chevron Res | Rejuvenation of a deactivated catalyst. |
Also Published As
| Publication number | Publication date |
|---|---|
| CA1003392A (en) | 1977-01-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |