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GB1351632A - Process for the preparation of bis-4-aminophenyl-methane - Google Patents

Process for the preparation of bis-4-aminophenyl-methane

Info

Publication number
GB1351632A
GB1351632A GB2283771A GB2283771A GB1351632A GB 1351632 A GB1351632 A GB 1351632A GB 2283771 A GB2283771 A GB 2283771A GB 2283771 A GB2283771 A GB 2283771A GB 1351632 A GB1351632 A GB 1351632A
Authority
GB
United Kingdom
Prior art keywords
aminophenyl
methane
bis
mixing
mineral acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2283771A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Magyar Tudomanyos Akademia
Original Assignee
Magyar Tudomanyos Akademia
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Magyar Tudomanyos Akademia filed Critical Magyar Tudomanyos Akademia
Publication of GB1351632A publication Critical patent/GB1351632A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/44—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring
    • C07C211/49—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring having at least two amino groups bound to the carbon skeleton
    • C07C211/50—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring having at least two amino groups bound to the carbon skeleton with at least two amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
    • C07C209/78—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton from carbonyl compounds, e.g. from formaldehyde, and amines having amino groups bound to carbon atoms of six-membered aromatic rings, with formation of methylene-diarylamines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/44—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring
    • C07C211/45—Monoamines
    • C07C211/46—Aniline

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1351632 Bis-(4-aminophenyl)-methane MAGYAR TUDOMANYOS AKADEMIA 19 April 1971 [2 March 1970] 22837/71 Heading C2C Bis-(4-aminophenyl)-methane is prepared by pre-mixing a mixture of aniline and a mineral acid with an aqueous solution of formaldehyde or a precursor thereof in a pre-mixing chamber and reacting the resulting mixture in a single stage in a tubular reactor in continuous operation to inhibit mixing of reacted with unreacted materials, the pre-mixing and subsequent reaction being performed at from 60 to 90‹ C. The mineral acid is preferably hydrochloric acid and the ratio of aniline to mineral acid is preferably not greater than 1À8 : 1. The product may be treated with an aqueous solution of an alkali metal hydroxide.
GB2283771A 1970-03-02 1971-04-19 Process for the preparation of bis-4-aminophenyl-methane Expired GB1351632A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
HU71MA2075A HUH2984A (en) 1970-03-02 1970-03-02 Process for producing diamino-diphenylmethane

Publications (1)

Publication Number Publication Date
GB1351632A true GB1351632A (en) 1974-05-01

Family

ID=10998451

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2283771A Expired GB1351632A (en) 1970-03-02 1971-04-19 Process for the preparation of bis-4-aminophenyl-methane

Country Status (5)

Country Link
BR (1) BR7101266D0 (en)
DD (1) DD88541A (en)
DE (1) DE2108462A1 (en)
GB (1) GB1351632A (en)
HU (1) HUH2984A (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2238920C3 (en) * 1972-08-08 1984-09-27 Bayer Ag, 5090 Leverkusen Process for the production of polyamines
DE2343658C2 (en) * 1973-08-30 1982-06-03 Bayer Ag, 5090 Leverkusen Process for the production of polyamines

Also Published As

Publication number Publication date
HUH2984A (en) 1970-03-02
BR7101266D0 (en) 1973-03-08
DE2108462A1 (en) 1971-09-16
DD88541A (en) 1972-03-12

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Legal Events

Date Code Title Description
CSNS Application of which complete specification have been accepted and published, but patent is not sealed