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GB1321886A - Treatment of pigmentary titanium dioxide - Google Patents

Treatment of pigmentary titanium dioxide

Info

Publication number
GB1321886A
GB1321886A GB3227070A GB3227070A GB1321886A GB 1321886 A GB1321886 A GB 1321886A GB 3227070 A GB3227070 A GB 3227070A GB 3227070 A GB3227070 A GB 3227070A GB 1321886 A GB1321886 A GB 1321886A
Authority
GB
United Kingdom
Prior art keywords
tio
silicate
coating
hydrated
treatment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3227070A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NAT LEAD CO
NL Industries Inc
Original Assignee
NAT LEAD CO
NL Industries Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NAT LEAD CO, NL Industries Inc filed Critical NAT LEAD CO
Publication of GB1321886A publication Critical patent/GB1321886A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/006Coating of the granules without description of the process or the device by which the granules are obtained
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09CTREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/36Compounds of titanium
    • C09C1/3607Titanium dioxide
    • C09C1/3653Treatment with inorganic compounds
    • C09C1/3661Coating
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/19Oil-absorption capacity, e.g. DBP values
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/60Optical properties, e.g. expressed in CIELAB-values
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/90Other properties not specified above

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

1321886 Coated TiO 2 NATIONAL LEAD CO 2 July 1970 [3 July 1969 20 April 1970] 32270/70 Heading C1N Pigmentary TiO 2 is coated with hydrated Al silicate, preferably 4À5-20% by wt. of the TiO 2 , and optionally with up to 2% of porous hydrated Al 2 O 3 , by maintaining an aqueous slurry of TiO 2 at a pH of 8À5-10À5 and at a temperature of from 70‹ C. to its b.pt, simultaneously adding solutions of salts of Si and Al (e.g. Na silicate, Al 2 (SO 4 ) 3 ) in a SiO 2 : Al 2 O 3 wt. ratio of 2 : 1 to 8 : 1 to precipitate Al silicate at a rate not greater than 10% per hr. on a TiO 2 wt. basis, and ageing the slurry at a pH of 7À0-10À5; a further Al silicate coating, and/or a porous hydrated Al 2 O 3 coating is then provided (the latter by lowering the pH to 5À0-5À5, adding Na aluminate or Al 2 (SO 4 ) 3 and then adjusting the pH to 7-8). The pigment may be dried and milled before and after the Al 2 O 3 coating. Drying may be effected at 120-350‹ C. or up to 500‹ C. for Al 2 O 3 , followed by steam fluid energy milling using a steam : pigment ratio of 3 : 1 to 5 : 1.
GB3227070A 1969-07-03 1970-07-02 Treatment of pigmentary titanium dioxide Expired GB1321886A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US83908869A 1969-07-03 1969-07-03
US3021970A 1970-04-20 1970-04-20

Publications (1)

Publication Number Publication Date
GB1321886A true GB1321886A (en) 1973-07-04

Family

ID=26705793

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3227070A Expired GB1321886A (en) 1969-07-03 1970-07-02 Treatment of pigmentary titanium dioxide

Country Status (8)

Country Link
BE (1) BE752899A (en)
DE (1) DE2033038C3 (en)
FI (1) FI49173C (en)
FR (1) FR2054611B1 (en)
GB (1) GB1321886A (en)
NL (1) NL158212B (en)
NO (1) NO133809C (en)
SE (1) SE362889B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2311823A1 (en) * 1975-05-23 1976-12-17 Du Pont PIGMENT TIO2 COATED WITH DENSE SILICA AND ALUMINA / POROUS SILICA

Also Published As

Publication number Publication date
DE2033038B2 (en) 1978-02-16
DE2033038C3 (en) 1978-10-12
FI49173C (en) 1975-04-10
NL7009716A (en) 1971-01-05
BE752899A (en) 1970-12-16
FI49173B (en) 1974-12-31
SE362889B (en) 1973-12-27
NL158212B (en) 1978-10-16
FR2054611B1 (en) 1973-04-06
NO133809B (en) 1976-03-22
NO133809C (en) 1976-06-30
FR2054611A1 (en) 1971-04-23
DE2033038A1 (en) 1971-01-21

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Legal Events

Date Code Title Description
PS Patent sealed
732 Registration of transactions, instruments or events in the register (sect. 32/1977)
PCNP Patent ceased through non-payment of renewal fee