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GB1272638A - Chromatographic apparatus - Google Patents

Chromatographic apparatus

Info

Publication number
GB1272638A
GB1272638A GB26209/69A GB2620969A GB1272638A GB 1272638 A GB1272638 A GB 1272638A GB 26209/69 A GB26209/69 A GB 26209/69A GB 2620969 A GB2620969 A GB 2620969A GB 1272638 A GB1272638 A GB 1272638A
Authority
GB
United Kingdom
Prior art keywords
stream
column
travelling
unit
columns
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB26209/69A
Inventor
John William Drinkwater
Albert Evans
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shell Internationale Research Maatschappij BV
Original Assignee
Shell Internationale Research Maatschappij BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Internationale Research Maatschappij BV filed Critical Shell Internationale Research Maatschappij BV
Priority to GB26209/69A priority Critical patent/GB1272638A/en
Priority to DE19702024569 priority patent/DE2024569A1/en
Priority to FR7018246A priority patent/FR2048544A5/fr
Priority to US00039602A priority patent/US3714812A/en
Publication of GB1272638A publication Critical patent/GB1272638A/en
Expired legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/46—Flow patterns using more than one column
    • G01N30/468—Flow patterns using more than one column involving switching between different column configurations
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/64—Electrical detectors
    • G01N30/70—Electron capture detectors
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/46—Flow patterns using more than one column
    • G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/26—Conditioning of the fluid carrier; Flow patterns
    • G01N30/38—Flow patterns
    • G01N30/46—Flow patterns using more than one column
    • G01N30/466—Flow patterns using more than one column with separation columns in parallel
    • G01N30/467—Flow patterns using more than one column with separation columns in parallel all columns being identical
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6047—Construction of the column with supporting means; Holders

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

1,272,638. Continuous gas chromatographic analysis system. SHELL INTERNATIONAL MAATSCHAPPIJ N.V. 22 May, 1969, No. 26209/69. Heading B1X. An electron capturing tracer travelling at the interface between, for example, two hydrocarbon liquids flowing in pipeline 18 are continuously monitored by entraining liquid samples removed by means of sampling valve 1 in a stream of purified carrier gas, e.g. nitrogen, and passing the stream to, and through, chromatography column 16 in unit 2. Unit 2 comprises a continuously or intermittently rotating turret of preferably six columns so arranged that while one column 16 is on-stream, another column 17 previously on-stream is backflushed with a sidestream 15 ofcarrier gas prior to coming on-stream again. Effluent from all the on-stream columns passes through an aftercolumn 13 which records a baseline against which the tracer material may be detected by electron capture detector 3. Sulphur hexafluoride or trichlorofluoromethane are suitable travelling tracers for hydrocarbon oils.
GB26209/69A 1969-05-22 1969-05-22 Chromatographic apparatus Expired GB1272638A (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
GB26209/69A GB1272638A (en) 1969-05-22 1969-05-22 Chromatographic apparatus
DE19702024569 DE2024569A1 (en) 1969-05-22 1970-05-20 Chromatography Process and Apparatus
FR7018246A FR2048544A5 (en) 1969-05-22 1970-05-20
US00039602A US3714812A (en) 1969-05-22 1970-05-22 Electron capture identification apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB26209/69A GB1272638A (en) 1969-05-22 1969-05-22 Chromatographic apparatus

Publications (1)

Publication Number Publication Date
GB1272638A true GB1272638A (en) 1972-05-03

Family

ID=10240063

Family Applications (1)

Application Number Title Priority Date Filing Date
GB26209/69A Expired GB1272638A (en) 1969-05-22 1969-05-22 Chromatographic apparatus

Country Status (4)

Country Link
US (1) US3714812A (en)
DE (1) DE2024569A1 (en)
FR (1) FR2048544A5 (en)
GB (1) GB1272638A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5047073A (en) * 1990-02-27 1991-09-10 Transducer Research, Inc. Sorption separation apparatus and methods

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2276589A1 (en) * 1974-06-26 1976-01-23 Commissariat Energie Atomique Apparatus for analysis of gases - uses continuous process operating in real time involving introduction of tracer into gas
US4535620A (en) * 1983-08-12 1985-08-20 Internorth, Inc. Method for automatically measuring the amount of water in a natural gas pipeline with the aid of a computer controlled gas chromatograph
AU640314B2 (en) * 1991-05-03 1993-08-19 Nalco Chemical Company Identification of liquid hydrocarbons using chemical markers
FI20115785A0 (en) * 2011-08-08 2011-08-08 Thermo Fisher Scientific Oy Method and apparatus for automatic analysis

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2234499A (en) * 1937-04-27 1941-03-11 Mine Safety Appliances Co Air testing device
US3199274A (en) * 1961-07-26 1965-08-10 Perkin Elmer Corp Chromatography apparatus
US3363447A (en) * 1966-02-14 1968-01-16 Universal Oil Prod Co Multiple chromatograph column heater unit
US3444722A (en) * 1966-09-09 1969-05-20 Phillips Petroleum Co Device for supplying carrier gas to transport eluted portion of sample and to backflush chromatographic column
US3550429A (en) * 1967-11-16 1970-12-29 Texaco Inc Chromatographic analysis

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5047073A (en) * 1990-02-27 1991-09-10 Transducer Research, Inc. Sorption separation apparatus and methods

Also Published As

Publication number Publication date
DE2024569A1 (en) 1970-12-10
US3714812A (en) 1973-02-06
FR2048544A5 (en) 1971-03-19

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee