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GB1188321A - Improvements in the Manufacture of Phosphonitrogenous Fertilisers - Google Patents

Improvements in the Manufacture of Phosphonitrogenous Fertilisers

Info

Publication number
GB1188321A
GB1188321A GB3323866A GB3323866A GB1188321A GB 1188321 A GB1188321 A GB 1188321A GB 3323866 A GB3323866 A GB 3323866A GB 3323866 A GB3323866 A GB 3323866A GB 1188321 A GB1188321 A GB 1188321A
Authority
GB
United Kingdom
Prior art keywords
phosphate
ammonium
caso
converted
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3323866A
Inventor
Douglas Allison Mitchell
Ray Fowler
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Power Gas Corp Ltd
Original Assignee
Power Gas Corp Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Power Gas Corp Ltd filed Critical Power Gas Corp Ltd
Priority to GB3323866A priority Critical patent/GB1188321A/en
Priority to NO16905067A priority patent/NO117542B/no
Publication of GB1188321A publication Critical patent/GB1188321A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
  • Fertilizers (AREA)

Abstract

1,188,321. Ammonium phosphate. POWERGAS CORP. Ltd. 12 July, 1967 [23 July, 1966], No. 33238/66. Heading C1A. In a process for producing phosphonitrogenous fertilizers, phosphate rock is acidulated with nitric acid to form a slurry containing unreacted phosphate rock, this is reacted with sulphuric acid so that substantially all the P 2 O 5 initially present is converted to H 3 PO 4 , CaSO 4 also being formed, adding sufficient (NH 4 ) 2 SO 4 to convert the calcium in solution into CaSO 4 , removing the CaSO 4 from the reaction product, withdrawing the reaction product and neutralizing it with ammonia so that free phosphoric acid is converted to ammonium phosphate. The reactions with sulphuric acid and ammonium sulphate are preferably carried out at 60‹ .to 90‹ C. When the ammonium phosphate is monoammonium phosphate a potassium salt or potassium hydroxide may be added to the product solution to convert all or a part of the mono-ammonium phosphate into diammonium phosphate and.potassium hydrogen phosphate. Some of the calcium sulphate produced may be converted to calcium carbonate by reaction with carbon dioxide and ammonia, the ammonium sulphate solution produced being used in the process. An example of the process is given.
GB3323866A 1966-07-23 1966-07-23 Improvements in the Manufacture of Phosphonitrogenous Fertilisers Expired GB1188321A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
GB3323866A GB1188321A (en) 1966-07-23 1966-07-23 Improvements in the Manufacture of Phosphonitrogenous Fertilisers
NO16905067A NO117542B (en) 1966-07-23 1967-07-14

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB3323866A GB1188321A (en) 1966-07-23 1966-07-23 Improvements in the Manufacture of Phosphonitrogenous Fertilisers

Publications (1)

Publication Number Publication Date
GB1188321A true GB1188321A (en) 1970-04-15

Family

ID=10350334

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3323866A Expired GB1188321A (en) 1966-07-23 1966-07-23 Improvements in the Manufacture of Phosphonitrogenous Fertilisers

Country Status (2)

Country Link
GB (1) GB1188321A (en)
NO (1) NO117542B (en)

Also Published As

Publication number Publication date
NO117542B (en) 1969-08-25

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Legal Events

Date Code Title Description
PS Patent sealed
PLNP Patent lapsed through nonpayment of renewal fees