GB1120770A - Manufacture of organic isocyanates - Google Patents
Manufacture of organic isocyanatesInfo
- Publication number
- GB1120770A GB1120770A GB3521466A GB3521466A GB1120770A GB 1120770 A GB1120770 A GB 1120770A GB 3521466 A GB3521466 A GB 3521466A GB 3521466 A GB3521466 A GB 3521466A GB 1120770 A GB1120770 A GB 1120770A
- Authority
- GB
- United Kingdom
- Prior art keywords
- organic isocyanates
- stage
- manufacture
- isocyanates
- phosgene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000012948 isocyanate Substances 0.000 title abstract 3
- 150000002513 isocyanates Chemical class 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 abstract 2
- 125000002924 primary amino group Chemical class [H]N([H])* 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Organic isocyanates are prepared by mixing in a first stage an excess of phosgene with a solution or suspension of a primary amine in an inert solvent while passing HCl in an amount not above 1 mole per mole NH2 group, and in a second stage or series of subsequent stages completing the reaction by heating, with optional addition of further phosgene. Examples describe the production of tolylene diisocyanate, but other isocyanates are listed.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB3521466A GB1120770A (en) | 1966-08-05 | 1966-08-05 | Manufacture of organic isocyanates |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB3521466A GB1120770A (en) | 1966-08-05 | 1966-08-05 | Manufacture of organic isocyanates |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1120770A true GB1120770A (en) | 1968-07-24 |
Family
ID=10375165
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3521466A Expired GB1120770A (en) | 1966-08-05 | 1966-08-05 | Manufacture of organic isocyanates |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1120770A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003099770A1 (en) * | 2002-05-23 | 2003-12-04 | Basf Aktiengesellschaft | Method for producing isocyanates |
CN104640840A (en) * | 2012-09-24 | 2015-05-20 | 拜耳材料科技股份有限公司 | Method for producing diisocyanates by phosgenating diamine suspensions |
-
1966
- 1966-08-05 GB GB3521466A patent/GB1120770A/en not_active Expired
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2003099770A1 (en) * | 2002-05-23 | 2003-12-04 | Basf Aktiengesellschaft | Method for producing isocyanates |
US7112694B2 (en) | 2002-05-23 | 2006-09-26 | Basf Aktiengesellschaft | Method for producing isocyanates |
CN100361968C (en) * | 2002-05-23 | 2008-01-16 | 巴斯福股份公司 | Method for producing isocyanates |
CN101108812B (en) * | 2002-05-23 | 2010-06-02 | 巴斯福股份公司 | Method for producing isocyanates |
CN104640840A (en) * | 2012-09-24 | 2015-05-20 | 拜耳材料科技股份有限公司 | Method for producing diisocyanates by phosgenating diamine suspensions |
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