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FR3122661B1 - Procede optimise d'hydrotraitement et d’hydroconversion de charges issues de sources renouvelables - Google Patents

Procede optimise d'hydrotraitement et d’hydroconversion de charges issues de sources renouvelables Download PDF

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Publication number
FR3122661B1
FR3122661B1 FR2104684A FR2104684A FR3122661B1 FR 3122661 B1 FR3122661 B1 FR 3122661B1 FR 2104684 A FR2104684 A FR 2104684A FR 2104684 A FR2104684 A FR 2104684A FR 3122661 B1 FR3122661 B1 FR 3122661B1
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FR
France
Prior art keywords
hydroconversion
effluent
hydrotreatment
feeds
renewable sources
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR2104684A
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English (en)
Other versions
FR3122661A1 (fr
Inventor
Christophe Bouchy
Anne-Sophie Gay
Almendros Mélanie Gomez
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR2104684A priority Critical patent/FR3122661B1/fr
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to PCT/EP2022/060159 priority patent/WO2022233561A1/fr
Priority to BR112023021919A priority patent/BR112023021919A2/pt
Priority to US18/558,622 priority patent/US20240240108A1/en
Priority to CN202280032957.7A priority patent/CN117280014A/zh
Priority to EP22723126.3A priority patent/EP4334412A1/fr
Priority to ARP220101151A priority patent/AR125744A1/es
Publication of FR3122661A1 publication Critical patent/FR3122661A1/fr
Application granted granted Critical
Publication of FR3122661B1 publication Critical patent/FR3122661B1/fr
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/12—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by hydrogenation
    • C11C3/126—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by hydrogenation using catalysts based principally on other metals or derivates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/42—Catalytic treatment
    • C10G3/44—Catalytic treatment characterised by the catalyst used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/12—Silica and alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/888—Tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/20—Sulfiding
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/50—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids in the presence of hydrogen, hydrogen donors or hydrogen generating compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/54—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids characterised by the catalytic bed
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/58—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins
    • C10G45/60—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G49/00—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00
    • C10G49/002—Apparatus for fixed bed hydrotreatment processes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/12—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by hydrogenation
    • C11C3/123—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by hydrogenation using catalysts based principally on nickel or derivates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Catalysts (AREA)

Abstract

La présente invention décrit un procédé de traitement d'une charge issue d'une source renouvelable comprenant une étape a) d'hydrotraitement de ladite charge, une étape b) de séparation d'au moins une partie de l’effluent issu de l'étape a) en au moins une fraction légère et au moins un effluent liquide hydrocarboné, une étape c) d'élimination d'au moins une partie de l'eau de l'effluent liquide hydrocarboné issu de l'étape b), une étape d) d’hydroconversion d'au moins une partie de l'effluent liquide hydrocarboné issu de l'étape c), ladite étape d) d’hydroconversion étant caractérisée d’une part par l’utilisation d’un catalyseur bifonctionnel comprenant une phase sulfure de molybdène et/ou de tungstène promue par du nickel et/ou du cobalt et d’autre part un rapport entre la pression partielle d’hydrogène sulfuré et d’hydrogène en entrée de l’unit d’hydroconversion inférieur à 5.10-5 et une étape e) de fractionnement de l'effluent issu de l'étape d) pour obtenir au moins une fraction distillat moyen.
FR2104684A 2021-05-04 2021-05-04 Procede optimise d'hydrotraitement et d’hydroconversion de charges issues de sources renouvelables Active FR3122661B1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR2104684A FR3122661B1 (fr) 2021-05-04 2021-05-04 Procede optimise d'hydrotraitement et d’hydroconversion de charges issues de sources renouvelables
BR112023021919A BR112023021919A2 (pt) 2021-05-04 2022-04-15 Método aperfeiçoado para o hidrotratamento e a hidroconversão de cargas oriundas de fontes renováveis
US18/558,622 US20240240108A1 (en) 2021-05-04 2022-04-15 Optimized process for the hydrotreating and hydroconversion of feedstocks derived from renewable sources
CN202280032957.7A CN117280014A (zh) 2021-05-04 2022-04-15 用于源自可再生资源的原料的加氢处理和加氢转化的优化方法
PCT/EP2022/060159 WO2022233561A1 (fr) 2021-05-04 2022-04-15 Procede optimise d'hydrotraitement et d'hydroconversion de charges issues de sources renouvelables
EP22723126.3A EP4334412A1 (fr) 2021-05-04 2022-04-15 Procede optimise d'hydrotraitement et d'hydroconversion de charges issues de sources renouvelables
ARP220101151A AR125744A1 (es) 2021-05-04 2022-05-02 Procedimiento optimizado de hidrotratamiento y de hidroconversión de cargas resultantes de fuentes renovables

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2104684A FR3122661B1 (fr) 2021-05-04 2021-05-04 Procede optimise d'hydrotraitement et d’hydroconversion de charges issues de sources renouvelables
FR2104684 2021-05-04

Publications (2)

Publication Number Publication Date
FR3122661A1 FR3122661A1 (fr) 2022-11-11
FR3122661B1 true FR3122661B1 (fr) 2024-05-17

Family

ID=76920900

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2104684A Active FR3122661B1 (fr) 2021-05-04 2021-05-04 Procede optimise d'hydrotraitement et d’hydroconversion de charges issues de sources renouvelables

Country Status (7)

Country Link
US (1) US20240240108A1 (fr)
EP (1) EP4334412A1 (fr)
CN (1) CN117280014A (fr)
AR (1) AR125744A1 (fr)
BR (1) BR112023021919A2 (fr)
FR (1) FR3122661B1 (fr)
WO (1) WO2022233561A1 (fr)

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4992605A (en) 1988-02-16 1991-02-12 Craig Wayne K Production of hydrocarbons with a relatively high cetane rating
CA2149685C (fr) 1994-06-30 1999-09-14 Jacques Monnier Conversion en additif pour carburant diesel de tallol dont on a extrait le brai
FR2846574B1 (fr) 2002-10-30 2006-05-26 Inst Francais Du Petrole Catalyseur et procede d'hydrocraquage de charges hydrocarbonees
ATE490298T1 (de) 2005-01-14 2010-12-15 Neste Oil Oyj Verfahren zur herstellung von kohlenwasserstoffen
EP1741768B2 (fr) 2005-07-04 2023-04-05 Neste Oyj Procédé pour la production d'hydrocarbures dans l'intervalle des Diesels
EP1976629A1 (fr) 2006-01-23 2008-10-08 Shell Internationale Research Maatschappij B.V. Catalyseur d hydrogenation et son utilisation pour l hydrogenation de produits finaux de fischer-tropsch
CA2728813C (fr) 2008-06-25 2016-09-13 Shell Internationale Research Maatschappij B.V. Procede de fabrication d'hydrocarbures paraffiniques
FR2940144B1 (fr) 2008-12-23 2016-01-22 Inst Francais Du Petrole Methode de transformation d'effluents d'origine renouvelable en carburant d'excellente qualite mettant en oeuvre un catalyseur a base de molybdene
FR2943071B1 (fr) 2009-03-10 2011-05-13 Inst Francais Du Petrole Procede d'hydrodesoxygenation de charges issues de sources renouvelables avec conversion limitee en decarboxylation mettant en oeuvre un catalyseur a base de nickel et de molybdene
US8729330B2 (en) 2010-03-09 2014-05-20 Exxonmobil Research And Engineering Company Hydroprocessing of diesel range biomolecules
FR2987842B1 (fr) * 2012-03-12 2015-02-27 IFP Energies Nouvelles Procede optimise pour la valorisation de bio-huiles en carburants hydrocarbones
DK201800550A1 (en) * 2018-09-06 2019-08-19 Haldor Topsøe A/S 2 stage process with conversion of light ends product

Also Published As

Publication number Publication date
US20240240108A1 (en) 2024-07-18
AR125744A1 (es) 2023-08-09
BR112023021919A2 (pt) 2023-12-19
FR3122661A1 (fr) 2022-11-11
WO2022233561A1 (fr) 2022-11-10
CN117280014A (zh) 2023-12-22
EP4334412A1 (fr) 2024-03-13

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