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FR3081866B1 - Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle - Google Patents

Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle Download PDF

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Publication number
FR3081866B1
FR3081866B1 FR1854763A FR1854763A FR3081866B1 FR 3081866 B1 FR3081866 B1 FR 3081866B1 FR 1854763 A FR1854763 A FR 1854763A FR 1854763 A FR1854763 A FR 1854763A FR 3081866 B1 FR3081866 B1 FR 3081866B1
Authority
FR
France
Prior art keywords
preparation
salt
fluorosulfonyl group
imides containing
c3hf6
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1854763A
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English (en)
Other versions
FR3081866A1 (fr
Inventor
Gregory Schmidt
Dominique Deur-Bert
Remy Teissier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1854763A priority Critical patent/FR3081866B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to PCT/FR2019/051237 priority patent/WO2019229359A1/fr
Priority to EP19737832.6A priority patent/EP3802486A1/fr
Priority to CN201980035495.2A priority patent/CN112166104A/zh
Priority to JP2020567031A priority patent/JP2021526146A/ja
Priority to US17/059,574 priority patent/US20210214220A1/en
Priority to KR1020207034328A priority patent/KR20210015820A/ko
Publication of FR3081866A1 publication Critical patent/FR3081866A1/fr
Application granted granted Critical
Publication of FR3081866B1 publication Critical patent/FR3081866B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C311/48—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups having nitrogen atoms of sulfonamide groups further bound to another hetero atom
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/086—Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
    • C07C303/40—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reactions not involving the formation of sulfonamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/42—Separation; Purification; Stabilisation; Use of additives
    • C07C303/44—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00—Electrolytic production of organic compounds
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
    • H01M10/0566—Liquid materials
    • H01M10/0568—Liquid materials characterised by the solutes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M2300/00—Electrolytes
    • H01M2300/0017—Non-aqueous electrolytes
    • H01M2300/0025—Organic electrolyte
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Electrochemistry (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

La présente invention concerne un procédé de préparation d'un composé de formule (III) suivante : R2-(SO2)-NM-(SO2)-F (III) dans laquelle R2 représente l'un des radicaux suivants : F, CF3, CHF2, CH2F, C2HF4, C2H2F3, C2H3F2, C2F5, C3F7, C3H4F3, C3HF6, C4F9, C4H2F7, C4H4F5, C5F11, C6F13, C7F15, C8F17 ou C9F19,; M représente un cation monovalent ou divalent; ledit procédé comprenant : - une étape b) de fluoration d'un composé de formule (I) suivante : R1-(SO2)-NH-(SO2)-CI (I) dans laquelle R1 représente l'un des radicaux suivants : CI, F, CF3, CHF2, CH2F, C2HF4, C2H2F3, C2H3F2, C2F5, C3F7, C3H4F3, C3HF6, C4F9, C4H2F7, C4H4F5, C5F11, C6F13, C7F15, C3F17 ou C9F19, R1 représentant de préférence CI; avec au moins un agent de fluoration; - une étape c) de distillation de la composition obtenue à l'étape b).
FR1854763A 2018-06-01 2018-06-01 Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle Active FR3081866B1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR1854763A FR3081866B1 (fr) 2018-06-01 2018-06-01 Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle
EP19737832.6A EP3802486A1 (fr) 2018-06-01 2019-05-28 Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle
CN201980035495.2A CN112166104A (zh) 2018-06-01 2019-05-28 制备含有氟磺酰基基团的酰亚胺盐的方法
JP2020567031A JP2021526146A (ja) 2018-06-01 2019-05-28 フルオロスルホニル基を含有するイミド塩を調製するための方法
PCT/FR2019/051237 WO2019229359A1 (fr) 2018-06-01 2019-05-28 Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle
US17/059,574 US20210214220A1 (en) 2018-06-01 2019-05-28 Method for preparing imide salts containing a fluorosulfonyl group
KR1020207034328A KR20210015820A (ko) 2018-06-01 2019-05-28 플루오로설포닐 기를 함유하는 이미드 염의 제조 방법

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1854763 2018-06-01
FR1854763A FR3081866B1 (fr) 2018-06-01 2018-06-01 Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle

Publications (2)

Publication Number Publication Date
FR3081866A1 FR3081866A1 (fr) 2019-12-06
FR3081866B1 true FR3081866B1 (fr) 2020-05-08

Family

ID=63557603

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1854763A Active FR3081866B1 (fr) 2018-06-01 2018-06-01 Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle

Country Status (7)

Country Link
US (1) US20210214220A1 (fr)
EP (1) EP3802486A1 (fr)
JP (1) JP2021526146A (fr)
KR (1) KR20210015820A (fr)
CN (1) CN112166104A (fr)
FR (1) FR3081866B1 (fr)
WO (1) WO2019229359A1 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3081456B1 (fr) 2018-05-23 2020-12-18 Arkema France Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle
FR3081457B1 (fr) * 2018-05-23 2020-05-08 Arkema France Procede de preparation du sel de lithium du bis(fluorosulfonyl)imide
FR3138132A1 (fr) 2022-07-22 2024-01-26 Arkema France Composition de sel pour électrolyte à faible teneur en ions sulfamate
FR3138131A1 (fr) 2022-07-22 2024-01-26 Arkema France Composition de sel pour électrolyte à faible teneur en acétamide
FR3152645A1 (fr) 2023-09-01 2025-03-07 Arkema France Electrolyte a faible teneur en ion sulfamate

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007068822A2 (fr) 2005-12-12 2007-06-21 Phostech Lithium Inc. Sels de sulfonyl-1, 2, 4-triazole
WO2009123328A1 (fr) * 2008-03-31 2009-10-08 Nippon Shokubai Co., Ltd. Sel sulfonylimide et procédé de production de celui-ci
US8377406B1 (en) * 2012-08-29 2013-02-19 Boulder Ionics Corporation Synthesis of bis(fluorosulfonyl)imide
FR2998297B1 (fr) 2012-11-22 2014-11-14 Arkema France Procede de preparation de sel d'imides contenant un groupement fluorosulfonyle
FR3008093B1 (fr) * 2013-07-04 2015-12-11 Rhodia Operations Procede de fluoration de composes halogenures de sulfonyle
US8722005B1 (en) 2013-07-26 2014-05-13 Boulder Ionics Corporation Synthesis of hydrogen bis(fluorosulfonyl)imide
US9284268B2 (en) * 2013-11-04 2016-03-15 Coorstek Fluorochemicals, Inc. Synthesis of fluorotrifluoromethylsulfonyl imide
FR3020060B1 (fr) * 2014-04-18 2016-04-01 Arkema France Preparation d'imides contenant un groupement fluorosulfonyle
JP6691740B2 (ja) * 2015-04-24 2020-05-13 ステラケミファ株式会社 フルオロスルホニルイミド化合物の製造方法
CN104925765B (zh) 2015-05-21 2017-08-08 上海康鹏科技有限公司 一种双氟磺酰亚胺锂盐的制备方法
CN110467163B (zh) 2018-05-10 2021-05-18 浙江蓝天环保高科技股份有限公司 一种双氟磺酰亚胺的制备方法

Also Published As

Publication number Publication date
JP2021526146A (ja) 2021-09-30
CN112166104A (zh) 2021-01-01
FR3081866A1 (fr) 2019-12-06
KR20210015820A (ko) 2021-02-10
WO2019229359A1 (fr) 2019-12-05
US20210214220A1 (en) 2021-07-15
EP3802486A1 (fr) 2021-04-14

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