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FR3062384B1 - Procede de preparation d'un materiau composite phosphate de vanadium-carbone par voie liquide - Google Patents

Procede de preparation d'un materiau composite phosphate de vanadium-carbone par voie liquide Download PDF

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Publication number
FR3062384B1
FR3062384B1 FR1750832A FR1750832A FR3062384B1 FR 3062384 B1 FR3062384 B1 FR 3062384B1 FR 1750832 A FR1750832 A FR 1750832A FR 1750832 A FR1750832 A FR 1750832A FR 3062384 B1 FR3062384 B1 FR 3062384B1
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France
Prior art keywords
composite material
vanadium
phosphate composite
preparation
carbon phosphate
Prior art date
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Active
Application number
FR1750832A
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English (en)
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FR3062384A1 (fr
Inventor
Renald David
Christine Surcin
Mathieu Morcrette
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Universite De Picardie Jules Verne Fr
Centre National de la Recherche Scientifique CNRS
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Centre National de la Recherche Scientifique CNRS
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Priority to FR1750832A priority Critical patent/FR3062384B1/fr
Application filed by Centre National de la Recherche Scientifique CNRS filed Critical Centre National de la Recherche Scientifique CNRS
Priority to US16/481,705 priority patent/US11569497B2/en
Priority to CN201880009629.9A priority patent/CN110770165A/zh
Priority to EP18712940.8A priority patent/EP3577068A1/fr
Priority to JP2019541233A priority patent/JP7106551B2/ja
Priority to PCT/FR2018/050248 priority patent/WO2018142082A1/fr
Priority to KR1020197022282A priority patent/KR102574245B1/ko
Publication of FR3062384A1 publication Critical patent/FR3062384A1/fr
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Publication of FR3062384B1 publication Critical patent/FR3062384B1/fr
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/37—Phosphates of heavy metals
    • C01B25/372—Phosphates of heavy metals of titanium, vanadium, zirconium, niobium, hafnium or tantalum
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/455—Phosphates containing halogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/05—Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/054—Accumulators with insertion or intercalation of metals other than lithium, e.g. with magnesium or aluminium
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/362—Composites
    • H01M4/366—Composites as layered products
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/583—Carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • H01M4/587—Carbonaceous material, e.g. graphite-intercalation compounds or CFx for inserting or intercalating light metals
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/621—Binders
    • H01M4/622—Binders being polymers
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624—Electric conductive fillers
    • H01M4/625—Carbon or graphite
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/01—Crystal-structural characteristics depicted by a TEM-image
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/02—Amorphous compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
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    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/74—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by peak-intensities or a ratio thereof only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/76—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by a space-group or by other symmetry indications
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
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    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/77—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by unit-cell parameters, atom positions or structure diagrams
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/88—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by thermal analysis data, e.g. TGA, DTA, DSC
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/027—Negative electrodes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Composite Materials (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

L'invention concerne un procédé de préparation d'un matériau composite phosphate de vanadium-carbone, un matériau composite phosphate de vanadium-carbone obtenu selon ledit procédé, ainsi que les utilisations dudit matériau composite, notamment comme précurseur pour la synthèse de matériaux électrochimiquement actifs d'électrode ou comme matériau actif d'anode.
FR1750832A 2017-02-01 2017-02-01 Procede de preparation d'un materiau composite phosphate de vanadium-carbone par voie liquide Active FR3062384B1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR1750832A FR3062384B1 (fr) 2017-02-01 2017-02-01 Procede de preparation d'un materiau composite phosphate de vanadium-carbone par voie liquide
CN201880009629.9A CN110770165A (zh) 2017-02-01 2018-02-01 用于制备磷酸钒-碳复合材料的液体方法
EP18712940.8A EP3577068A1 (fr) 2017-02-01 2018-02-01 Procédé de préparation d'un matériau composite phosphate de vanadium-carbone par voie liquide
JP2019541233A JP7106551B2 (ja) 2017-02-01 2018-02-01 リン酸バナジウム－炭素複合材料を作製するための液体法
US16/481,705 US11569497B2 (en) 2017-02-01 2018-02-01 Liquid process for preparing a vanadium phosphate-carbon composite material
PCT/FR2018/050248 WO2018142082A1 (fr) 2017-02-01 2018-02-01 Procédé de préparation d'un matériau composite phosphate de vanadium-carbone par voie liquide
KR1020197022282A KR102574245B1 (ko) 2017-02-01 2018-02-01 인산 바나듐-탄소 복합 재료 제조를 위한 액체 방법

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1750832 2017-02-01
FR1750832A FR3062384B1 (fr) 2017-02-01 2017-02-01 Procede de preparation d'un materiau composite phosphate de vanadium-carbone par voie liquide

Publications (2)

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FR3062384A1 FR3062384A1 (fr) 2018-08-03
FR3062384B1 true FR3062384B1 (fr) 2021-02-12

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FR1750832A Active FR3062384B1 (fr) 2017-02-01 2017-02-01 Procede de preparation d'un materiau composite phosphate de vanadium-carbone par voie liquide

Country Status (7)

Country Link
US (1) US11569497B2 (fr)
EP (1) EP3577068A1 (fr)
JP (1) JP7106551B2 (fr)
KR (1) KR102574245B1 (fr)
CN (1) CN110770165A (fr)
FR (1) FR3062384B1 (fr)
WO (1) WO2018142082A1 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112850684B (zh) * 2019-11-27 2022-07-08 中国科学院大连化学物理研究所 一种氟磷酸钒锂的制备方法及应用
CN112421027B (zh) * 2020-11-17 2022-02-11 常州大学 表面改性的多孔六边形Na3V2(PO4)2F3碳包覆微米球及其制备方法和应用
CN112694076B (zh) * 2020-12-28 2022-05-13 大连博融新材料有限公司 一种碳复合磷酸钒的修复方法
CN112678787B (zh) * 2020-12-28 2022-05-13 大连博融新材料有限公司 一种晶相纯度高且可溶高价钒含量低的复合磷酸钒、其制备方法及用途
WO2023108571A1 (fr) * 2021-12-16 2023-06-22 宁德时代新能源科技股份有限公司 Élément de batterie, batterie, appareil électrique, procédé de fabrication et dispositif de fabrication

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KR100814540B1 (ko) 2001-04-06 2008-03-17 발렌스 테크놀로지, 인코포레이티드 나트륨 이온 배터리
US20070160519A1 (en) * 2005-03-28 2007-07-12 Jeremy Barker Method Of Making Active Materials For Use In Secondary Electrochemical Cells
US20090035661A1 (en) * 2007-08-01 2009-02-05 Jeffrey Swoyer Synthesis of cathode active materials
CN102259844A (zh) * 2011-06-29 2011-11-30 扬州欧畅电源科技有限公司 锂离子电池正极材料磷酸亚铁锂的磷酸固相法合成工艺
CN102623708A (zh) * 2012-04-12 2012-08-01 上海智荣科技有限责任公司 锂离子电池正极用磷酸钒锂/石墨烯复合材料的制备方法
CN102774821B (zh) * 2012-07-30 2014-05-21 四川大学 一种磷酸钒锂的固相-水热制备方法
CN103094568A (zh) * 2013-01-29 2013-05-08 河北师范大学 一种磷酸铁锂材料的制备方法
CN103346317B (zh) * 2013-07-01 2015-10-28 金瑞新材料科技股份有限公司 复合掺杂及包覆型锂离子电池正极材料LiFePO4及其制备方法
CN103594716A (zh) * 2013-11-21 2014-02-19 天津工业大学 一种制备钠离子电池正极材料氟磷酸钒钠的方法
CN103872324B (zh) * 2014-03-28 2016-08-24 中南大学 一种花瓣状锂离子电池负极材料vpo4的制备方法
CN104134799B (zh) * 2014-08-15 2016-12-07 武汉理工力强能源有限公司 碳修饰多孔磷酸钒锂纳米球材料及其制备方法和应用
FR3042313B1 (fr) * 2015-10-13 2020-04-03 Commissariat A L'energie Atomique Et Aux Energies Alternatives Procede de preparation d'un materiau particulaire na3v2(po4)2f3
CN105470479B (zh) * 2015-11-26 2017-12-01 中南大学 一种改性的磷酸锰锂复合正极材料及其制备方法
CN105552328A (zh) * 2015-12-24 2016-05-04 华中科技大学 一种磷酸钒钠钠离子电池正极材料及其制备方法
CN105655565B (zh) * 2016-04-08 2018-01-09 苏州大学 一种钠离子电池复合正极材料及其制备方法

Also Published As

Publication number Publication date
EP3577068A1 (fr) 2019-12-11
US11569497B2 (en) 2023-01-31
JP7106551B2 (ja) 2022-07-26
US20190393492A1 (en) 2019-12-26
WO2018142082A1 (fr) 2018-08-09
FR3062384A1 (fr) 2018-08-03
CN110770165A (zh) 2020-02-07
KR20190140900A (ko) 2019-12-20
KR102574245B1 (ko) 2023-09-04
JP2020506148A (ja) 2020-02-27

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