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FR2592647A1 - PROCESS FOR THE PREPARATION OF CARBON MOLDED BODIES WITH HIGH ANISOTROPY. - Google Patents

PROCESS FOR THE PREPARATION OF CARBON MOLDED BODIES WITH HIGH ANISOTROPY.

Info

Publication number
FR2592647A1
FR2592647A1 FR8700002A FR8700002A FR2592647A1 FR 2592647 A1 FR2592647 A1 FR 2592647A1 FR 8700002 A FR8700002 A FR 8700002A FR 8700002 A FR8700002 A FR 8700002A FR 2592647 A1 FR2592647 A1 FR 2592647A1
Authority
FR
France
Prior art keywords
preparation
molded bodies
carbon molded
high anisotropy
linearly
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR8700002A
Other languages
French (fr)
Other versions
FR2592647B1 (en
Inventor
Jurgen W Stadelhofer
Herbert Beneke
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rain Carbon Germany GmbH
Original Assignee
Ruetgerswerke AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ruetgerswerke AG filed Critical Ruetgerswerke AG
Publication of FR2592647A1 publication Critical patent/FR2592647A1/en
Application granted granted Critical
Publication of FR2592647B1 publication Critical patent/FR2592647B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/145—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from pitch or distillation residues
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/05—Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/20—Graphite
    • C01B32/205—Preparation
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/52—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite
    • C04B35/524—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite obtained from polymer precursors, e.g. glass-like carbon material
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G2261/30—Monomer units or repeat units incorporating structural elements in the main chain
    • C08G2261/31—Monomer units or repeat units incorporating structural elements in the main chain incorporating aromatic structural elements in the main chain
    • C08G2261/312—Non-condensed aromatic systems, e.g. benzene
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Geology (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Inorganic Fibers (AREA)
  • Manufacture Of Macromolecular Shaped Articles (AREA)

Abstract

Pour la préparation de corps moulés au carbone, notamment de fibres au carbone, il est proposé un procédé dans lequel le précurseur est un polymère obtenu à partir de composés polycycliques condensés linéairement ayant un poids moléculaire entre 500 et 1200. Il est obtenu par polymérisation de produits aromatiques annellés linéairement, substitués en position bêta et éventuellement après avoir chassé par distillation les monomères et polymères comportant moins de cinq cycles, il est soumis à une extraction fractionnée avec un gaz surcritique, afin de rétrécir la plage des poids moléculaires. Les fibres en carbone ainsi obtenues, préparées d'une manière connue, font partie de la catégorie des fibres à module d'élasticité élevé.For the preparation of carbon molded bodies, in particular carbon fibers, a process is proposed in which the precursor is a polymer obtained from linearly condensed polycyclic compounds having a molecular weight between 500 and 1200. It is obtained by polymerization of aromatic products ringed linearly, substituted in beta position and possibly after having distilled off the monomers and polymers comprising less than five cycles, it is subjected to fractional extraction with a supercritical gas, in order to narrow the range of molecular weights. The carbon fibers thus obtained, prepared in a known manner, belong to the category of fibers with a high modulus of elasticity.

FR8700002A 1986-01-03 1987-01-02 PROCESS FOR THE PREPARATION OF CARBON MOLDED BODIES WITH HIGH ANISOTROPY. Expired - Lifetime FR2592647B1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19863600063 DE3600063A1 (en) 1986-01-03 1986-01-03 METHOD FOR PRODUCING HIGH ANISOTROPY CARBON MOLDED BODIES

Publications (2)

Publication Number Publication Date
FR2592647A1 true FR2592647A1 (en) 1987-07-10
FR2592647B1 FR2592647B1 (en) 1992-11-13

Family

ID=6291396

Family Applications (1)

Application Number Title Priority Date Filing Date
FR8700002A Expired - Lifetime FR2592647B1 (en) 1986-01-03 1987-01-02 PROCESS FOR THE PREPARATION OF CARBON MOLDED BODIES WITH HIGH ANISOTROPY.

Country Status (4)

Country Link
DE (1) DE3600063A1 (en)
FR (1) FR2592647B1 (en)
GB (1) GB2185010B (en)
NL (1) NL8603289A (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2655742B2 (en) * 1990-07-16 1997-09-24 工業技術院長 Tapered carbon microelectrode and method of manufacturing the same
DE102023201375A1 (en) 2023-02-17 2024-08-22 Forschungszentrum Jülich GmbH Carbon fiber molded body

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2015175A1 (en) * 1969-03-31 1970-11-12 Kureha Kagaku Kogyo Kabushiki Kaisha, Tokio Process for the production of carbon moldings of high anisotropy
US4014980A (en) * 1972-07-27 1977-03-29 Kureha Kagaku Kogyo Kabushiki Kaisha Method for manufacturing graphite whiskers using condensed polycyclic hydrocarbons

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3535081A (en) * 1968-09-09 1970-10-20 Atomic Energy Commission Method for making graphite

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2015175A1 (en) * 1969-03-31 1970-11-12 Kureha Kagaku Kogyo Kabushiki Kaisha, Tokio Process for the production of carbon moldings of high anisotropy
US4014980A (en) * 1972-07-27 1977-03-29 Kureha Kagaku Kogyo Kabushiki Kaisha Method for manufacturing graphite whiskers using condensed polycyclic hydrocarbons

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
INDUSTRIAL AND ENGINEERING CHEMISTRY, PROCESS DESIGN AND vol. 24, no. 1, janvier 1985, WASHINGTON US pages 121 - 128; Vasilakos et al: "Sokvent effects in supercritical extraction of coal" *
REVUE DE L'INSTITUT FRANCAIS DU PETROLE. vol. 40, no. 1, février 1985, PARIS FR pages 33 - 49; Behar et al: "Application des fluides supercritiques a la production d'hydrocarbures" *

Also Published As

Publication number Publication date
GB2185010B (en) 1989-10-25
DE3600063A1 (en) 1987-07-09
GB8630347D0 (en) 1987-01-28
FR2592647B1 (en) 1992-11-13
GB2185010A (en) 1987-07-08
NL8603289A (en) 1987-08-03
DE3600063C2 (en) 1988-03-17

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Legal Events

Date Code Title Description
ST Notification of lapse