FR2370685A1 - PROCESS FOR SEPARATING HYDROGEN FLUORIDE FROM ITS MIXTURES WITH OTHER ACID GASES - Google Patents
PROCESS FOR SEPARATING HYDROGEN FLUORIDE FROM ITS MIXTURES WITH OTHER ACID GASESInfo
- Publication number
- FR2370685A1 FR2370685A1 FR7733884A FR7733884A FR2370685A1 FR 2370685 A1 FR2370685 A1 FR 2370685A1 FR 7733884 A FR7733884 A FR 7733884A FR 7733884 A FR7733884 A FR 7733884A FR 2370685 A1 FR2370685 A1 FR 2370685A1
- Authority
- FR
- France
- Prior art keywords
- hydrogen fluoride
- acid gases
- mixtures
- gases
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1493—Selection of liquid materials for use as absorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/1456—Removing acid components
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Treating Waste Gases (AREA)
Abstract
Procédé de séparation du fluorure d'hydrogène de ses mélanges avec d'autres gaz acides. Le mélange gazeux contenant le fluorure d'hydrogène et les autres gaz acides, le cas échéant avec des gaz inertes, traverse dans une première étape opérationnelle 1 de l'acide sulfurique à 75-85 % en poids de preférence, à basse température, acide qui absorbe sélectivement la majeure partie du fluorure d'hydrogène du mélange gazeux, puis, dans une seconde étape opérationnelle 4, on insuffle un courant de gaz inerte dans l'acide sulfurique contenant le fluorure d'hydrogène, à température élevée, courant de gaz inerte qui élimine de l'acide sulfurique, le fluorure d'hydrogène débarrassé des autres gaz acides.Process for separating hydrogen fluoride from its mixtures with other acid gases. The gas mixture containing hydrogen fluoride and the other acid gases, where appropriate with inert gases, passes through in a first operational stage 1 sulfuric acid at 75-85% by weight preferably, at low temperature, acidic. which selectively absorbs the major part of the hydrogen fluoride from the gas mixture, then, in a second operational step 4, a stream of inert gas is blown into the sulfuric acid containing the hydrogen fluoride, at high temperature, gas stream inert which eliminates sulfuric acid, hydrogen fluoride freed from other acid gases.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19762651630 DE2651630A1 (en) | 1976-11-12 | 1976-11-12 | PROCESS FOR THE SEPARATION OF HYDROFLUOR FROM MIXTURES WITH ACID GASES |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2370685A1 true FR2370685A1 (en) | 1978-06-09 |
Family
ID=5993002
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7733884A Pending FR2370685A1 (en) | 1976-11-12 | 1977-11-10 | PROCESS FOR SEPARATING HYDROGEN FLUORIDE FROM ITS MIXTURES WITH OTHER ACID GASES |
Country Status (4)
Country | Link |
---|---|
DE (1) | DE2651630A1 (en) |
FR (1) | FR2370685A1 (en) |
GB (1) | GB1556837A (en) |
NL (1) | NL7712244A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2007147987A1 (en) * | 2006-06-21 | 2007-12-27 | Arkema France | Method of recovering hydrofluoric acid |
WO2013050690A1 (en) * | 2011-10-06 | 2013-04-11 | Arkema France | Method of recycling hydrochloric and hydrofluoric acid effluent |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112897466A (en) * | 2020-10-27 | 2021-06-04 | 贵州省化工研究院 | Method for producing anhydrous hydrogen fluoride by using fluosilicic acid in phosphoric acid |
CN114345106B (en) * | 2021-12-30 | 2023-12-12 | 湖北瓮福蓝天化工有限公司 | Method and system for removing chlorine element in anhydrous hydrogen fluoride production process |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR741966A (en) * | 1931-09-02 | 1933-02-23 | ||
FR1150956A (en) * | 1956-05-23 | 1958-01-22 | Pechiney | Concentration and purification of hydrofluoric acid |
FR1342891A (en) * | 1961-10-02 | 1963-11-15 | Stauffer Chemical Co | Process for extracting hydrofluoric acid from a dilute aqueous solution |
US3218127A (en) * | 1962-09-10 | 1965-11-16 | Tennessee Corp | Process of producing hydrogen fluoride in a two-stage procedure and effecting a rapid evolution of the hydrogen fluoride by sweeping the second stage with an inert gas |
FR2340272A1 (en) * | 1976-02-04 | 1977-09-02 | Riedel De Haen Ag | Hydrogen fluoride obtd. from waste or byprods. - by adding sulphuric acid and injecting air to remove the hydrogen fluoride |
-
1976
- 1976-11-12 DE DE19762651630 patent/DE2651630A1/en not_active Withdrawn
-
1977
- 1977-11-07 NL NL7712244A patent/NL7712244A/en not_active Application Discontinuation
- 1977-11-10 FR FR7733884A patent/FR2370685A1/en active Pending
- 1977-11-10 GB GB4683877A patent/GB1556837A/en not_active Expired
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR741966A (en) * | 1931-09-02 | 1933-02-23 | ||
FR1150956A (en) * | 1956-05-23 | 1958-01-22 | Pechiney | Concentration and purification of hydrofluoric acid |
FR1342891A (en) * | 1961-10-02 | 1963-11-15 | Stauffer Chemical Co | Process for extracting hydrofluoric acid from a dilute aqueous solution |
US3218127A (en) * | 1962-09-10 | 1965-11-16 | Tennessee Corp | Process of producing hydrogen fluoride in a two-stage procedure and effecting a rapid evolution of the hydrogen fluoride by sweeping the second stage with an inert gas |
FR2340272A1 (en) * | 1976-02-04 | 1977-09-02 | Riedel De Haen Ag | Hydrogen fluoride obtd. from waste or byprods. - by adding sulphuric acid and injecting air to remove the hydrogen fluoride |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2007147987A1 (en) * | 2006-06-21 | 2007-12-27 | Arkema France | Method of recovering hydrofluoric acid |
FR2902780A1 (en) * | 2006-06-21 | 2007-12-28 | Arkema France | PROCESS FOR RECOVERING FLUORHYDRIC ACID |
WO2013050690A1 (en) * | 2011-10-06 | 2013-04-11 | Arkema France | Method of recycling hydrochloric and hydrofluoric acid effluent |
FR2981060A1 (en) * | 2011-10-06 | 2013-04-12 | Arkema France | PROCESS FOR THE VALORISATION OF THE EFFLUENTS OF CHLOROFLUORHYDRIC ACID |
US9783427B2 (en) | 2011-10-06 | 2017-10-10 | Arkema France | Method of recycling hydrochloric and hydrofluoric acid effluent |
Also Published As
Publication number | Publication date |
---|---|
NL7712244A (en) | 1978-05-17 |
DE2651630A1 (en) | 1978-05-24 |
GB1556837A (en) | 1979-11-28 |
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