FR2063575A5 - Analysis of impurities in gases - Google Patents
Analysis of impurities in gasesInfo
- Publication number
- FR2063575A5 FR2063575A5 FR6936227A FR6936227A FR2063575A5 FR 2063575 A5 FR2063575 A5 FR 2063575A5 FR 6936227 A FR6936227 A FR 6936227A FR 6936227 A FR6936227 A FR 6936227A FR 2063575 A5 FR2063575 A5 FR 2063575A5
- Authority
- FR
- France
- Prior art keywords
- carbon dioxide
- impurities
- molecular sieve
- angstrom
- helium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/40—Flow patterns using back flushing
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/08—Preparation using an enricher
- G01N2030/085—Preparation using an enricher using absorbing precolumn
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
A samle of gas to be analysed, e.g. argon, oxygen, methane impurities in carbon dioxide, is swept onto a precolumn pref. silica gel with carrier gas pref. helium. Carbon dioxide is momentarily absorbed, the impurities being carried on to a molecular sieve (13 angstrom) and detector exhausting to a secondary (5 angstrom) molecular sieve column to confirm or supplement the initial detector analysis. The pre-column is back flushed with helium to remove carbon dioxide ensuring minimal contact of CO2 with molecular sieve augmenting the sieve operational life span.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR6936227A FR2063575A5 (en) | 1969-10-22 | 1969-10-22 | Analysis of impurities in gases |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR6936227A FR2063575A5 (en) | 1969-10-22 | 1969-10-22 | Analysis of impurities in gases |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2063575A5 true FR2063575A5 (en) | 1971-07-09 |
Family
ID=9041907
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR6936227A Expired FR2063575A5 (en) | 1969-10-22 | 1969-10-22 | Analysis of impurities in gases |
Country Status (1)
Country | Link |
---|---|
FR (1) | FR2063575A5 (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1984004394A1 (en) * | 1981-11-03 | 1984-11-08 | Elf France | Method and apparatus for taking a sample from a gas effluent and application to chromatography |
GB2150458A (en) * | 1984-03-21 | 1985-07-03 | Elf France | Method and apparatus for taking a sample from a gas effluent and application to chromatography |
US4588422A (en) * | 1983-12-07 | 1986-05-13 | Elf France | Process and equipment for sampling a gaseous effluent and their application to chromatography |
FR2599152A1 (en) * | 1986-05-22 | 1987-11-27 | Flopetrol | METHOD AND APPARATUS FOR CHROMATOGRAPHIC ANALYSIS, PARTICULARLY FOR PETROLEUM LIQUIDS |
-
1969
- 1969-10-22 FR FR6936227A patent/FR2063575A5/en not_active Expired
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1984004394A1 (en) * | 1981-11-03 | 1984-11-08 | Elf France | Method and apparatus for taking a sample from a gas effluent and application to chromatography |
US4588422A (en) * | 1983-12-07 | 1986-05-13 | Elf France | Process and equipment for sampling a gaseous effluent and their application to chromatography |
GB2150458A (en) * | 1984-03-21 | 1985-07-03 | Elf France | Method and apparatus for taking a sample from a gas effluent and application to chromatography |
FR2599152A1 (en) * | 1986-05-22 | 1987-11-27 | Flopetrol | METHOD AND APPARATUS FOR CHROMATOGRAPHIC ANALYSIS, PARTICULARLY FOR PETROLEUM LIQUIDS |
EP0247929A1 (en) * | 1986-05-22 | 1987-12-02 | Flopetrol Services, Inc. | Method and apparatus for chromatographic analysis, in particular of petroleum liquids |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
CA | Change of address | ||
CD | Change of name or company name | ||
TP | Transmission of property |