FI893455A - 1,3-di-(6-O-sakkaroosi)-1,1,3,3-tetra(hydrokarbyyli)distannoksaani, menetelmä sen valmistamiseksi ja menetelmä sakkaroosin 6-asemassa olevan hydroksyyliryhmän esteröimiseksi sen avulla - Google Patents

1,3-di-(6-O-sakkaroosi)-1,1,3,3-tetra(hydrokarbyyli)distannoksaani, menetelmä sen valmistamiseksi ja menetelmä sakkaroosin 6-asemassa olevan hydroksyyliryhmän esteröimiseksi sen avulla Download PDF

Info

Publication number: FI893455A
Authority: FI; Finland
Prior art keywords: sucrose; distannoxane; hydrocarbyl; esterification; tetra
Prior art date: 1988-07-18

Application number

FI893455A

Other languages

English (en)

Swedish (sv)

Other versions

FI91874B (fi

FI91874C (fi

FI893455A0 (fi

Inventor

Juan L Navia

Original Assignee

Noramco Inc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1988-07-18

Filing date

1989-07-17

Publication date

1990-01-19

1989-07-17 Application filed by Noramco Inc filed Critical Noramco Inc

1989-07-17 Publication of FI893455A0 publication Critical patent/FI893455A0/fi

1990-01-19 Publication of FI893455A publication Critical patent/FI893455A/fi

1994-05-13 Publication of FI91874B publication Critical patent/FI91874B/fi

1994-08-25 Application granted granted Critical

1994-08-25 Publication of FI91874C publication Critical patent/FI91874C/fi

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H11/00—Compounds containing saccharide radicals esterified by inorganic acids; Metal salts thereof
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C07H13/06—Fatty acids
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H23/00—Compounds containing boron, silicon or a metal, e.g. chelates or vitamin B12

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Biochemistry (AREA)
Biotechnology (AREA)
General Health & Medical Sciences (AREA)
Genetics & Genomics (AREA)
Molecular Biology (AREA)
Saccharide Compounds (AREA)
Steroid Compounds (AREA)

FI893455A 1988-07-18 1989-07-17 1,3-di-(6-O-sakkaroosi)-1,1,3,3-tetra(hydrokarbyyli)distannoksaani, menetelmä sen valmistamiseksi ja menetelmä sakkaroosin 6-asemassa olevan hydroksyyliryhmän esteröimiseksi sen avulla FI91874C (fi)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US07/220,641 US4950746A (en)	1988-07-18	1988-07-18	Process for synthesizing sucrose derivatives by regioselective reaction
US22064188		1988-07-18

Publications (4)

Publication Number	Publication Date
FI893455A0 FI893455A0 (fi)	1989-07-17
FI893455A true FI893455A (fi)	1990-01-19
FI91874B FI91874B (fi)	1994-05-13
FI91874C FI91874C (fi)	1994-08-25

Family

ID=22824357

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
FI893455A FI91874C (fi)	1988-07-18	1989-07-17	1,3-di-(6-O-sakkaroosi)-1,1,3,3-tetra(hydrokarbyyli)distannoksaani, menetelmä sen valmistamiseksi ja menetelmä sakkaroosin 6-asemassa olevan hydroksyyliryhmän esteröimiseksi sen avulla

Country Status (24)

Country	Link
US (1)	US4950746A (fi)
EP (1)	EP0352048B1 (fi)
JP (1)	JP2725710B2 (fi)
KR (1)	KR0143234B1 (fi)
AR (1)	AR245136A1 (fi)
AT (1)	ATE114664T1 (fi)
AU (1)	AU618107B2 (fi)
CA (1)	CA1323625C (fi)
DE (1)	DE68919566T2 (fi)
DK (1)	DK170027B1 (fi)
ES (1)	ES2065386T3 (fi)
FI (1)	FI91874C (fi)
GR (1)	GR1002250B (fi)
IE (1)	IE65990B1 (fi)
IL (1)	IL91004A (fi)
MX (1)	MX172793B (fi)
NO (1)	NO171855C (fi)
NZ (1)	NZ229823A (fi)
PH (1)	PH26098A (fi)
PT (1)	PT91186B (fi)
RU (1)	RU2041233C1 (fi)
TR (1)	TR27628A (fi)
YU (1)	YU47159B (fi)
ZA (1)	ZA895427B (fi)

Families Citing this family (51)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5089608A (en) *	1990-03-23	1992-02-18	Mcneil-Ppc, Inc.	Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols
US5034551A (en) *	1990-04-23	1991-07-23	Noramco, Inc.	Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds
US5023329A (en) *	1990-04-23	1991-06-11	Noramco, Inc.	Sucrose-6-ester production process
GR910100356A (el) *	1990-08-27	1992-08-31	Mcneil Ppc Inc	Καταλυόμενη μέ?οδος εστέρος-6-σακχαρόζης.
US5470969A (en) *	1990-08-27	1995-11-28	Mcneil-Ppc, Inc.	Catalyzed sucrose-6-ester process
FR2670493A1 (fr) *	1990-12-13	1992-06-19	Isochem Sa	Nouveaux composes monoesters du saccharose tels que les 2-0-acylsaccharoses et les 6-0-acylsaccharoses, ainsi que leurs procedes de synthese.
US5298611A (en) *	1993-03-12	1994-03-29	Mcneil-Ppc, Inc.	Sucralose pentaester production
IL114551A0 (en)	1994-07-11	1995-11-27	Us Agriculture	Chemically synthesized sugar esters for the control of soft bodied arthropods
US6608039B1 (en)	1994-07-11	2003-08-19	The United States Of America As Represented By The Secretary Of Agriculture	Chemically synthesized sugar esters for the control of soft-bodied arthropods
US5498709A (en) *	1994-10-17	1996-03-12	Mcneil-Ppc, Inc.	Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
ATE231876T1 (de)	1995-11-28	2003-02-15	Mcneil Ppc Inc	Herstellungsverfahren für sucrose-6-ester
US6121430A (en) *	1998-12-28	2000-09-19	University Of Iowa Research Foundation	Regiospecific synthesis of glucose-based surfactants
ES2305124T3 (es)	2000-11-17	2008-11-01	TATE & LYLE TECHNOLOGY LIMITED	Forma fundible de sucralosa.
CA2429228C (en)	2000-11-17	2008-08-26	Mcneil-Ppc, Inc.	Improved sucralose composition and process for the crystallization thereof
US6890581B2 (en) *	2002-04-05	2005-05-10	Tate & Lyle Public Limited Company	Methods for buffer stabilized aqueous deacylation
US6943248B2 (en) *	2003-04-30	2005-09-13	Tate & Lyle Public Limited Company	Crystalline form of sucralose, and method for producing it
CN1176094C (zh) *	2003-05-23	2004-11-17	广东省食品工业研究所	一种三氯蔗糖的合成方法
US20050214425A1 (en) *	2004-03-23	2005-09-29	Roma Vazirani	Sugar substitute prepared with nutritive and high-intensity sweeteners
US20090105470A1 (en) *	2005-02-22	2009-04-23	Pharmed Medicare Private Limited , A Corporation	Tin Mediated Regioselective Synthesis of Sucrose-6-Esters
US7750146B2 (en)	2005-03-18	2010-07-06	Tate & Lyle Plc	Granular sucralose
US20060247180A1 (en) *	2005-04-29	2006-11-02	Bergey James L	Purgative composition and uses thereof
US20060276639A1 (en) *	2005-06-01	2006-12-07	Healthy Brands, Llc	Conversion of sucralose-6-ester to sucralose
CN100418976C (zh) *	2006-04-03	2008-09-17	广州科宏食品添加物有限公司	一种三氯蔗糖的制备方法
CN101092438A (zh) *	2006-06-22	2007-12-26	南京莱因医药科技有限公司	6－o－苯甲酰三氯半乳型蔗糖四乙酯的制备方法
GB0702854D0 (en) *	2007-01-09	2007-03-28	Tate & Lyle Plc	Method for the synthesis of sucrose-6-esters
GB0702857D0 (en) *	2007-01-19	2007-03-28	Tate & Lyle Plc	Improved sucralose production method
US20080227971A1 (en) *	2007-01-19	2008-09-18	Leinhos Duane A	Deacylation of sucralose-6-acylates
US20090076261A1 (en) *	2007-09-13	2009-03-19	Polymed Therapeutics, Inc.	Novel process for preparing sucrose-6-esters
CN101245085B (zh)	2007-12-19	2012-02-01	上海同辰生物科技有限公司	一种三氯蔗糖的合成及纯化工艺
AR070082A1 (es) *	2008-01-04	2010-03-10	Tate & Lyle Technology Ltd	Metodo para la produccion de sucralosa
US7932380B2 (en)	2008-03-06	2011-04-26	Wanhe International (Group) Co. Ltd.	Process for the preparation of sucralose
US8557976B2 (en) *	2008-03-13	2013-10-15	Tate & Lyle Technology Limited	Microbial consortia and methods for their use
WO2009117317A1 (en) *	2008-03-20	2009-09-24	Tate & Lyle Technology Ltd	Removal of acids from tertiary amide solvents
US8436157B2 (en) *	2008-03-26	2013-05-07	Tate & Lyle Technology Limited	Method for the production of sucralose
US8497367B2 (en) *	2008-04-03	2013-07-30	Tate & Lyle Technology Limited	Sucralose purification process
AR071134A1 (es) *	2008-04-03	2010-05-26	Tate & Lyle Technology Ltd	Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
JP5653341B2 (ja) *	2008-04-03	2015-01-14	テートアンドライルテクノロジーリミテッド	スクラロース抽出効率に対する炭水化物濃度の影響
US20090259036A1 (en) *	2008-04-03	2009-10-15	Tate & Lyle Technology Limited	Extraction of less polar impurities from sucralose containing aqueous feed streams
US20090299055A1 (en) *	2008-04-03	2009-12-03	Tate & Lyle Technology Limited	Purification of Sucralose Containing Feed Streams for Sucralose Crystallization
GB2469157B (en)	2009-03-30	2011-07-06	John Kerr	Process for removing dimethylamine during sucralose production
GB2469158B (en) *	2009-03-31	2011-09-28	Peter J Seaberg	Base-assisted formation of tin-sucrose adducts
GB2471348B (en)	2009-06-22	2011-12-14	Tate & Lyle Technology Ltd	A method for producing sucralose-6-acylate
GB2474311B (en) *	2009-10-12	2012-10-17	Tate & Lyle Technology Ltd	Low temperature, single solvent process for the production of sucrose-6-ester
GB2474310B (en) *	2009-10-12	2012-02-29	Tate & Lyle Technology Ltd	Process for the production of sucrose-6-ester
CN101759728B (zh) *	2010-01-08	2012-01-11	江苏巨邦制药有限公司	三氯蔗糖的生产及精制方法
GB201110520D0 (en)	2011-05-10	2011-08-03	Tate & Lyle Technology Ltd	Extraction of carboxylic acids with tin compounds
US10227367B2 (en)	2013-12-16	2019-03-12	Tate & Lyle Technology Limited	Chlorination of sucrose-6-esters
WO2016020635A1 (en)	2014-08-08	2016-02-11	Tate & Lyle Technology Limited	Chlorination of sucrose-6-esters
GB2536480B (en)	2015-03-17	2019-09-04	Tate & Lyle Tech Ltd	DMF Distillation
WO2017091435A1 (en) *	2015-11-24	2017-06-01	Archer Daniels Midland Company	Oligomerizations of fdca and glycols in a one-pot esterification-transesterification process catalyzed by homogeneous organometallic lewis acids
GB2551591B (en)	2016-06-23	2019-08-07	Tate & Lyle Tech Ltd	Liquid-liquid extraction of DMF

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4435440A (en) *	1976-01-08	1984-03-06	Tate & Lyle Limited	Sweeteners
DE3065399D1 (en) *	1979-12-18	1983-11-24	Tate & Lyle Plc	Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
EP0031651B1 (en) *	1979-12-20	1983-03-23	TATE & LYLE PUBLIC LIMITED COMPANY	Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
ATE9355T1 (de) *	1980-07-08	1984-09-15	Tate & Lyle Public Limited Company	Verfahren zur herstellung von 4,1',6'-trichlor4,1',6'-trideoxygalactosucrose (tgs).

1988
- 1988-07-18 US US07/220,641 patent/US4950746A/en not_active Expired - Lifetime
1989
- 1989-07-04 NZ NZ229823A patent/NZ229823A/xx unknown
- 1989-07-12 AU AU38048/89A patent/AU618107B2/en not_active Expired
- 1989-07-12 YU YU139389A patent/YU47159B/sh unknown
- 1989-07-17 DE DE68919566T patent/DE68919566T2/de not_active Expired - Lifetime
- 1989-07-17 CA CA000605839A patent/CA1323625C/en not_active Expired - Lifetime
- 1989-07-17 DK DK352689A patent/DK170027B1/da not_active IP Right Cessation
- 1989-07-17 IL IL9100489A patent/IL91004A/en unknown
- 1989-07-17 PT PT91186A patent/PT91186B/pt active IP Right Grant
- 1989-07-17 FI FI893455A patent/FI91874C/fi not_active IP Right Cessation
- 1989-07-17 GR GR890100456A patent/GR1002250B/el not_active IP Right Cessation
- 1989-07-17 RU SU4614609/04A patent/RU2041233C1/ru not_active IP Right Cessation
- 1989-07-17 IE IE231089A patent/IE65990B1/en not_active IP Right Cessation
- 1989-07-17 EP EP89307228A patent/EP0352048B1/en not_active Expired - Lifetime
- 1989-07-17 AR AR89314425A patent/AR245136A1/es active
- 1989-07-17 JP JP1182762A patent/JP2725710B2/ja not_active Expired - Lifetime
- 1989-07-17 ES ES89307228T patent/ES2065386T3/es not_active Expired - Lifetime
- 1989-07-17 ZA ZA895427A patent/ZA895427B/xx unknown
- 1989-07-17 AT AT89307228T patent/ATE114664T1/de not_active IP Right Cessation
- 1989-07-17 NO NO892926A patent/NO171855C/no not_active IP Right Cessation
- 1989-07-18 PH PH38957A patent/PH26098A/en unknown
- 1989-07-18 TR TR00931/89A patent/TR27628A/xx unknown
- 1989-07-18 MX MX016842A patent/MX172793B/es unknown
- 1989-07-18 KR KR1019890010134A patent/KR0143234B1/ko not_active IP Right Cessation

Also Published As

Publication number	Publication date
YU139389A (en)	1991-02-28
NO892926L (no)	1990-01-19
NO171855B (no)	1993-02-01
PT91186B (pt)	1995-03-01
FI91874B (fi)	1994-05-13
GR1002250B (en)	1996-04-23
KR0143234B1 (ko)	1998-07-01
IE65990B1 (en)	1995-11-29
AU3804889A (en)	1990-01-18
DE68919566T2 (de)	1995-04-13
DK352689A (da)	1990-01-19
NZ229823A (en)	1991-01-29
KR910002884A (ko)	1991-02-26
CA1323625C (en)	1993-10-26
NO171855C (no)	1993-05-12
YU47159B (sh)	1995-01-31
EP0352048B1 (en)	1994-11-30
DE68919566D1 (de)	1995-01-12
MX16842A (es)	1993-04-01
IL91004A0 (en)	1990-02-09
EP0352048A3 (en)	1991-09-04
IE892310L (en)	1990-01-18
NO892926D0 (no)	1989-07-17
PT91186A (pt)	1990-02-08
MX172793B (es)	1994-01-13
FI91874C (fi)	1994-08-25
PH26098A (en)	1992-02-06
GR890100456A (el)	1990-06-27
AR245136A1 (es)	1993-12-30
RU2041233C1 (ru)	1995-08-09
JP2725710B2 (ja)	1998-03-11
JPH0273096A (ja)	1990-03-13
EP0352048A2 (en)	1990-01-24
DK352689D0 (da)	1989-07-17
US4950746A (en)	1990-08-21
TR27628A (tr)	1995-06-14
FI893455A0 (fi)	1989-07-17
AU618107B2 (en)	1991-12-12
ES2065386T3 (es)	1995-02-16
ATE114664T1 (de)	1994-12-15
IL91004A (en)	1994-04-12
DK170027B1 (da)	1995-05-01
ZA895427B (en)	1991-03-27

Publication	Publication Date	Title
FI893455A (fi)	1990-01-19	1,3-di-(6-O-sakkaroosi)-1,1,3,3-tetra(hydrokarbyyli)distannoksaani, menetelmä sen valmistamiseksi ja menetelmä sakkaroosin 6-asemassa olevan hydroksyyliryhmän esteröimiseksi sen avulla
PT85745A (en)	1987-10-01	Process for the preparation of sucrose derivatives
NZ237764A (en)	1993-05-26	Preparation of 1,3-di-(6-0-sucrose)-1,1,3,3-tetra(hydrocarbyl)distannoxane derivatives by reaction of sucrose and di(hydrocarbyl)tin oxide; preparation of sucrose-6-esters
FI900886A0 (fi)	1990-02-22	Menetelmä uusien terapeuttisesti käyttökelpoisten pyridiinijohdannaisten valmistamiseksi
FI891654A0 (fi)	1989-04-06	Anordning foer vaermebehandling och/eller torkning av en materialbana i omlopp.
FI875727A0 (fi)	1987-12-28	Nya oligosackarider, immunogener och vacciner och foerfarande foer framstaellning av saodana oligosackarider, immunogener och vacciner.
FI892058A0 (fi)	1989-04-28	Fenolin valmistusmenetelmä
NO892458D0 (no)	1989-06-13	Fremstilling av sukrosepolyester.
FI874361A0 (fi)	1987-10-05	Anvaendning av garvmedel och/eller klorogensyra samt naerings-, njutnings- och/eller laekemedel med garvmedels- och/eller klorogensyratillsats.
FI895663A0 (fi)	1989-11-27	Menetelmä kloorifluoribenseenin tai difluoribenseenin valmistamiseksi
FI92065C (fi)	1994-09-26	Menetelmä farmaseuttisten piperidiinijohdannaisten valmistamiseksi
FI95914C (fi)	1996-04-10	Polypeptidijohdannaisia ja menetelmä niiden valmistamiseksi
FI902355A0 (fi)	1990-05-11	Uusien tieno-triatsolo-diatsepiinijohdosten valmistusmenetelmä
FI92205C (fi)	1994-10-10	Menetelmä terapeuttisesti käyttökelpoisten N-pyrrolo- ja pyrido /3,2,1,-j k/ /1,4/ bentsodiatsepinyyli-N'-aryyliurea ja tioureajohdannaisten valmistamiseksi
FI103868B1 (fi)	1999-10-15	Menetelmä farmaseuttisen koostumuksen valmistamiseksi fibriinin saostumisen tai kiinnikasvettumien estämiseksi
FI98811B (fi)	1997-05-15	Menetelmä immuunijärjestelmään vaikuttavien bentseenijohdannaisten valmistamiseksi
FI99080B (fi)	1997-06-30	Menetelmä ruoansulatuskanavan ulkopuoliseen annosteluun tarkoitettujen emulsioiden valmistamiseksi
FI874501A (fi)	1988-04-15	Foerfarande foer framstaellning av loesliga och/eller delbara tabletter och sao erhaollna tabletter.
FI871545A0 (fi)	1987-04-08	Foerfarande foer framstaellning av en synergistisk blandning foer terapi av kancer innehaollande interleukin 2 och/eller interferon- och tumoernekrosisfaktor.
FI884696A (fi)	1988-10-12	Foerfarande foer framstaellning av en cellulosamassa och/eller foer avlaegsning av lignin fraon sekundaerfibrer.
FI98727B (fi)	1997-04-30	Menetelmä TiO2-pigmenttien valmistamiseksi
FI894359A (fi)	1990-03-17	Menetelmä sakkaroosin tai sen johdannaisen klooraamiseksi
FI891100A0 (fi)	1989-03-08	Process och anlaeggning foer behandling av en gasstroem innehaollande sjaelvantaendbart damm.
FI892650A0 (fi)	1989-05-31	Legeringsmedel framstaellda av med pulvras och/eller keramiska fibrer foerstaerkt bly eller av dess legeringar samt anvaendning av dem.
FI880039A0 (fi)	1988-01-06	Betongvikt med inbaeddade eller faestade anoder foer katodiskt skydd av bultar och bultfoerbindningar.

Legal Events

Date	Code	Title	Description
1994-04-18	BB	Publication of examined application
2004-08-31	MM	Patent lapsed	Owner name: NORAMCO, INC.