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FI20185810A1 - Arrangement and method for thermal desorption measurement - Google Patents

Arrangement and method for thermal desorption measurement Download PDF

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Publication number
FI20185810A1
FI20185810A1 FI20185810A FI20185810A FI20185810A1 FI 20185810 A1 FI20185810 A1 FI 20185810A1 FI 20185810 A FI20185810 A FI 20185810A FI 20185810 A FI20185810 A FI 20185810A FI 20185810 A1 FI20185810 A1 FI 20185810A1
Authority
FI
Finland
Prior art keywords
arrangement
sample
thermal desorption
desorption measurement
heating
Prior art date
Application number
FI20185810A
Other languages
Finnish (fi)
Swedish (sv)
Other versions
FI128645B (en
Inventor
Evgenii Malitckii
Yuriy Yagodzinskyy
Hannu Hänninen
Original Assignee
Aalto Univ Foundation Sr
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aalto Univ Foundation Sr filed Critical Aalto Univ Foundation Sr
Priority to FI20185810A priority Critical patent/FI128645B/en
Priority to PCT/FI2019/050688 priority patent/WO2020065135A1/en
Publication of FI20185810A1 publication Critical patent/FI20185810A1/en
Application granted granted Critical
Publication of FI128645B publication Critical patent/FI128645B/en

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20Metals
    • G01N33/202Constituents thereof
    • G01N33/2022Non-metallic constituents
    • G01N33/2025Gaseous constituents
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N7/00Analysing materials by measuring the pressure or volume of a gas or vapour
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00Particle spectrometers or separator tubes
    • H01J49/02Details
    • H01J49/04Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
    • H01J49/0468Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components with means for heating or cooling the sample
    • H01J49/049Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components with means for heating or cooling the sample with means for applying heat to desorb the sample; Evaporation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N2030/0075Separation due to differential desorption
    • G01N2030/008Thermal desorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Pathology (AREA)
  • Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)

Abstract

An arrangement (100) for detecting atoms and/or molecules desorbed from at least one sample, the arrangement comprising at least one desorption chamber (102) adapted to keep an ultra-low pressure, wherein the desorbed atoms and/or molecules may be detected by heating the sample in the desorption chamber (102). The arrangement additionally comprises a cooling system (106) for cooling the sample prior to the heating of the sample.
FI20185810A 2018-09-28 2018-09-28 Arrangement and method for thermal desorption measurement FI128645B (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
FI20185810A FI128645B (en) 2018-09-28 2018-09-28 Arrangement and method for thermal desorption measurement
PCT/FI2019/050688 WO2020065135A1 (en) 2018-09-28 2019-09-27 Arrangement and method for thermal desorption measurement

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FI20185810A FI128645B (en) 2018-09-28 2018-09-28 Arrangement and method for thermal desorption measurement

Publications (2)

Publication Number Publication Date
FI20185810A1 true FI20185810A1 (en) 2020-03-29
FI128645B FI128645B (en) 2020-09-30

Family

ID=69952885

Family Applications (1)

Application Number Title Priority Date Filing Date
FI20185810A FI128645B (en) 2018-09-28 2018-09-28 Arrangement and method for thermal desorption measurement

Country Status (2)

Country Link
FI (1) FI128645B (en)
WO (1) WO2020065135A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113976090A (en) * 2020-12-31 2022-01-28 苏州开洛泰克科学仪器科技有限公司 Centralized self-diagnosis vacuum desorption device and use method thereof

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR870001397B1 (en) * 1983-01-22 1987-07-25 신닛뽄 세이데쓰 가부시끼가이샤 Sample collection tube and hydrogen quantification device for the determination of the amount of hydrogen in molten metal
JP5405218B2 (en) * 2008-07-31 2014-02-05 電子科学株式会社 Sample analysis method, sample carrying member, sample carrying method, and temperature programmed desorption analyzer

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113976090A (en) * 2020-12-31 2022-01-28 苏州开洛泰克科学仪器科技有限公司 Centralized self-diagnosis vacuum desorption device and use method thereof
CN113976090B (en) * 2020-12-31 2024-05-14 苏州开洛泰克科学仪器科技有限公司 Centralized self-diagnosis vacuum desorption device and use method thereof

Also Published As

Publication number Publication date
FI128645B (en) 2020-09-30
WO2020065135A1 (en) 2020-04-02

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