ES8602626A1 - Procedimiento de preparar compuestos oxima o-substituida - Google Patents
Procedimiento de preparar compuestos oxima o-substituidaInfo
- Publication number
- ES8602626A1 ES8602626A1 ES542138A ES542138A ES8602626A1 ES 8602626 A1 ES8602626 A1 ES 8602626A1 ES 542138 A ES542138 A ES 542138A ES 542138 A ES542138 A ES 542138A ES 8602626 A1 ES8602626 A1 ES 8602626A1
- Authority
- ES
- Spain
- Prior art keywords
- oxima
- procedure
- formula
- alkyl
- preparing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000001875 compounds Chemical class 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 150000002923 oximes Chemical class 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical class [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 150000002367 halogens Chemical group 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 229910000000 metal hydroxide Inorganic materials 0.000 abstract 1
- 150000004692 metal hydroxides Chemical class 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/14—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCEDIMIENTO PARA PREPARAR COMPUESTOS OXIMA O-SUSTITUIDA. CONSISTE EN HACER REACCIONAR UNA OXIMA DE FORMULA (II) CON HIDROXIDO DE METAL ALCALINO O ALCALINOTERREO EN EXCESO DE OXIMA, A LA MEZCLA OBTENIDA SE LA SOMETE A DESTILACION AGEOTROPICA PARA ELIMINAR EL AGUA PRESENTE EN LA MEZCLA. SE HACE REACCIONAR LA SAL DE METAL ALCALINO O ALCALINOTERREO DE LA OXIMA CON UN COMPUESTO DE FORMULA R3X PARA OBTENER LA OXIMA -O-SUSTITUIDA DE FORMULA (I), EN DONDE X ES HALOGENO, R1 Y R2 PUEDEN SER HIDROGENO, ALQUILO, FENILO O FENIALQUILO Y R3 ES ALQUENILO, ALQUILO O ALQUILO SUSTITUIDO CON UNO O MAS GRUPO CARBOXI, AMIDO, CIANO O ALCOXICARBONILO.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US59943284A | 1984-04-12 | 1984-04-12 |
Publications (2)
Publication Number | Publication Date |
---|---|
ES542138A0 ES542138A0 (es) | 1985-12-16 |
ES8602626A1 true ES8602626A1 (es) | 1985-12-16 |
Family
ID=24399590
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES542138A Expired ES8602626A1 (es) | 1984-04-12 | 1985-04-11 | Procedimiento de preparar compuestos oxima o-substituida |
Country Status (6)
Country | Link |
---|---|
EP (1) | EP0158159B1 (es) |
JP (1) | JPS60231645A (es) |
KR (1) | KR870001679B1 (es) |
CA (1) | CA1259629A (es) |
DE (1) | DE3565398D1 (es) |
ES (1) | ES8602626A1 (es) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3620166A1 (de) * | 1986-06-14 | 1987-12-17 | Bayer Ag | Verfahren zur herstellung von hydroxybenzaldoxim-o-ethern |
EP0417167A1 (en) * | 1988-05-27 | 1991-03-20 | AlliedSignal Inc. | Process for the synthesis of o-substituted oxime compounds |
US5393921A (en) * | 1993-07-07 | 1995-02-28 | The Gillette Company | Process for synthesizing O-substituted oxime compounds and conversion to the corresponding O-substituted hydroxylamine |
US5488162A (en) * | 1994-01-03 | 1996-01-30 | Buckland; Paul R. | Process for preparing o-alkylhydroxylamine salts without the isolation of intermediates |
DE4437905A1 (de) * | 1994-10-22 | 1996-04-25 | Basf Ag | Verfahren zur Herstellung von O-substituierten Hydroxylammoniumsalzen |
DE4437904A1 (de) * | 1994-10-22 | 1996-04-25 | Basf Ag | Verfahren zur Herstellung von Isopropylidenaminooxyessigsäure(methoxycarbonylmethylen)ester I |
US5777164A (en) * | 1997-04-14 | 1998-07-07 | Eastman Chemical Company | Process for the preparation of high purity O-substituted hydroxylamine derivatives |
CN101565386B (zh) * | 2009-05-18 | 2012-06-27 | 浙江大学宁波理工学院 | 合成肟醚的方法 |
CN103044283A (zh) * | 2012-09-07 | 2013-04-17 | 赵立地 | 一种制备肟醚的方法 |
CN109942454A (zh) * | 2019-03-25 | 2019-06-28 | 西安集佰侬生物科技有限公司 | 一种乙烯拮抗剂及其制备方法 |
CN110606813A (zh) * | 2019-09-17 | 2019-12-24 | 浙江圣安化工股份有限公司 | 一种含活性基团的肟醚及其合成方法 |
CN111004147B (zh) * | 2019-12-16 | 2022-10-28 | 山东金城柯瑞化学有限公司 | 一种温和条件下铜盐催化合成丁酮肟甲醚的新方法 |
CN114835660B (zh) * | 2022-04-11 | 2024-03-22 | 浙江理工大学 | 一种肟醚的制备方法 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2820013A1 (de) * | 1978-05-08 | 1979-11-22 | Hoechst Ag | Verfahren zur herstellung von o-alkylierten hydroxylaminen |
DE2927117A1 (de) * | 1979-07-05 | 1981-01-08 | Basf Ag | Verfahren zur herstellung von o-substituierten ketoximen |
DE3473593D1 (en) * | 1983-04-04 | 1988-09-29 | Allied Corp | Process for the production of o-substituted oximes |
-
1985
- 1985-03-16 EP EP85103052A patent/EP0158159B1/en not_active Expired
- 1985-03-16 DE DE8585103052T patent/DE3565398D1/de not_active Expired
- 1985-03-28 CA CA000477740A patent/CA1259629A/en not_active Expired
- 1985-04-02 KR KR1019850002215A patent/KR870001679B1/ko not_active IP Right Cessation
- 1985-04-11 ES ES542138A patent/ES8602626A1/es not_active Expired
- 1985-04-12 JP JP60078257A patent/JPS60231645A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
EP0158159B1 (en) | 1988-10-05 |
EP0158159A1 (en) | 1985-10-16 |
KR850007583A (ko) | 1985-12-07 |
KR870001679B1 (ko) | 1987-09-22 |
DE3565398D1 (en) | 1988-11-10 |
CA1259629A (en) | 1989-09-19 |
ES542138A0 (es) | 1985-12-16 |
JPS60231645A (ja) | 1985-11-18 |
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