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ES481498A1 - Un metodo para reducir el contenido en eteres ciclicos oli- gomeros de un polimerizado de thf-oxido de alquileno. - Google Patents

Un metodo para reducir el contenido en eteres ciclicos oli- gomeros de un polimerizado de thf-oxido de alquileno.

Info

Publication number
ES481498A1
ES481498A1 ES481498A ES481498A ES481498A1 ES 481498 A1 ES481498 A1 ES 481498A1 ES 481498 A ES481498 A ES 481498A ES 481498 A ES481498 A ES 481498A ES 481498 A1 ES481498 A1 ES 481498A1
Authority
ES
Spain
Prior art keywords
cyclic ether
copolymerizate
ether content
oligomeric cyclic
reducing oligomeric
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES481498A
Other languages
English (en)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of ES481498A1 publication Critical patent/ES481498A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/16—Cyclic ethers having four or more ring atoms
    • C08G65/20—Tetrahydrofuran
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G2650/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterized by the type of post-polymerisation functionalisation
    • C08G2650/12—Depolymerisation, e.g. to reform the monomer
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G2650/28—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the polymer type
    • C08G2650/34—Oligomeric, e.g. cyclic oligomeric

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyethers (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

Un método para reducir el contenido en éteres cíclicos oligómeros de un polimerizado de THF/óxido de alquileno sustancialmente libre de monómeros, que supone poner en contacto el polimerizado, a una temperatura de 70-150ºC, con 1-50%, en peso, de polimerizado, de una arcilla montmorillonítica de sodio o calcio activada por ácido, durante un tiempo suficiente para reducir significativamente el contenido en éter cíclico oligómero del polimerizado.
ES481498A 1978-06-13 1979-06-12 Un metodo para reducir el contenido en eteres ciclicos oli- gomeros de un polimerizado de thf-oxido de alquileno. Expired ES481498A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US91519078A 1978-06-13 1978-06-13
US05/970,733 US4192943A (en) 1978-06-13 1978-12-21 Method for reducing oligomeric cyclic ether content of a polymerizate

Publications (1)

Publication Number Publication Date
ES481498A1 true ES481498A1 (es) 1980-04-01

Family

ID=27129663

Family Applications (1)

Application Number Title Priority Date Filing Date
ES481498A Expired ES481498A1 (es) 1978-06-13 1979-06-12 Un metodo para reducir el contenido en eteres ciclicos oli- gomeros de un polimerizado de thf-oxido de alquileno.

Country Status (5)

Country Link
US (1) US4192943A (es)
EP (1) EP0006107B1 (es)
CA (1) CA1143893A (es)
DE (1) DE2966417D1 (es)
ES (1) ES481498A1 (es)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4376190A (en) * 1979-11-26 1983-03-08 Minnesota Mining And Manufacturing Company Cation complexes between cation guests and polymer hosts that contain cyclic ether units
DE3042960A1 (de) * 1980-11-14 1982-07-08 Basf Ag, 6700 Ludwigshafen Verfahren zur depolymerisation von polytetramethylenglykolether
US4306058A (en) * 1980-11-19 1981-12-15 E. I. Du Pont De Nemours And Company Method for reducing oligomeric cyclic ether content of a polymerizate
US4511742A (en) * 1982-08-30 1985-04-16 The B. F. Goodrich Company Extraction of oligomers from polymers of epihalohydrin
DE3346136A1 (de) * 1983-12-21 1985-07-04 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen herstellung von polyoxibutylenpolyoxialkylenglykolen
DE3505152A1 (de) * 1985-02-15 1986-09-04 Basf Ag, 6700 Ludwigshafen Verfahren zur einengung der molekulargewichtsverteilung von polytetrahydrofuran
US4585592A (en) * 1985-02-28 1986-04-29 Basf Aktiengesellschaft Reducing the content of oligomeric cyclic ethers in polyoxybutylene polyoxyalkylene glycols
DE3514547A1 (de) * 1985-04-23 1986-10-23 Basf Ag, 6700 Ludwigshafen Verfahren zur verminderung des anteils von cyclischen oligomeren ethern in polytetramethylenetherglykolen oder polyoxibutylen-polyoxialkylenglykolen
DE3541155A1 (de) * 1985-11-21 1987-05-27 Basf Ag Verfahren zur depolymerisation von polyoxibutylenpolyoxialkylenglykolen und polyoxibutylenpolyoxialkylenethern
DE3606479A1 (de) * 1986-02-28 1987-09-03 Basf Ag Verfahren zur herstellung von polyoxibutylenpolyoxialkylenglykolen mit enger molekulargewichtsverteilung und vermindertem gehalt an oligomeren cyclischen ethern
DE3725577A1 (de) * 1987-08-01 1989-02-09 Basf Ag Verfahren zur reinigung von polyoxybutylenpolyoxyalkylenglykolen
IT1231506B (it) * 1989-08-24 1991-12-07 Pressindustria S P A Milano Procedimento per la purificazione di polieteri polioli.
DE19715831A1 (de) * 1997-04-16 1998-10-22 Basf Ag Verfahren zur Entfärbung von Polymerisaten oder Copolymerisaten des Tetrahydrofurans
US5997732A (en) * 1997-12-22 1999-12-07 Chevron U.S.A. Inc. Clay treatment process for white mineral oil
DE19801462A1 (de) * 1998-01-16 1999-07-22 Basf Ag Katalysator und Verfahren zur Herstellung von Polytetrahydrofuran
DE10210728A1 (de) * 2002-03-12 2003-10-02 Basf Ag Verfahren zur Herstellung von Polytetrahydrofuran mit vermindertem Gehalt an oligomeren cyclischen Ethern
US8372946B2 (en) * 2009-04-15 2013-02-12 Invista North America S.A R.L. Copolyether glycol manufacturing process
US8609805B2 (en) 2009-04-15 2013-12-17 Invista North America S.A R.L. Copolyether glycol manufacturing process
US20100267905A1 (en) * 2009-04-15 2010-10-21 Invista North America S.A R.L. Copolyether glycol manufacturing process
JP5744841B2 (ja) * 2009-04-15 2015-07-08 インヴィスタ テクノロジーズ エスアエルエル コポリエーテルグリコールの製法
EP2614103B1 (en) 2010-09-10 2015-04-15 Invista Technologies S.a r.l. Polyetheramines, compositions including polyetheramines, and methods of making
CN103333332B (zh) * 2013-07-01 2015-12-23 达利(中国)有限公司 一种染色促进剂的制备方法及其应用

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2520733A (en) * 1946-08-26 1950-08-29 Shell Dev Polymers of trimethylene glycol
US2510540A (en) * 1947-03-17 1950-06-06 Shell Dev Synthetic lubricant
GB854958A (en) 1957-03-14 1960-11-23 Bayer Ag Copolymerising mono-epoxides with tetrahydrofurane
US3053903A (en) * 1957-12-11 1962-09-11 Shell Oil Co Production of high molecular weight polyoxyalkylene compounds
GB854998A (en) * 1958-04-24 1960-11-23 Sartorius Werke Ag Improvements in or relating to burettes
US3321412A (en) * 1963-03-29 1967-05-23 Mobil Oil Corp Polymerization of alkylene oxides in the presence of aluminosilicate catalysts
US3454652A (en) * 1966-09-22 1969-07-08 Ouaker Oats Co The Process for production of tetrahydrofuran polymers
FR2174670A1 (en) * 1972-03-06 1973-10-19 Maries Kuhlmann Wyandott Polyols purificn - by centrifuging a water/polyol/solvent mixt
US3925484A (en) * 1973-11-08 1975-12-09 Du Pont Process for making polytetramethylene ether glycol having a narrow molecular weight distribution
US4029879A (en) * 1975-11-17 1977-06-14 Basf Wyandotte Corporation Process for the removal of catalysts from polyether polyols employing water and adsorbent

Also Published As

Publication number Publication date
CA1143893A (en) 1983-03-29
EP0006107B1 (en) 1983-11-23
US4192943A (en) 1980-03-11
DE2966417D1 (en) 1983-12-29
EP0006107A1 (en) 1980-01-09

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