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ES425041A1 - Process for working up nitration mixtures - Google Patents

Process for working up nitration mixtures

Info

Publication number
ES425041A1
ES425041A1 ES425041A ES425041A ES425041A1 ES 425041 A1 ES425041 A1 ES 425041A1 ES 425041 A ES425041 A ES 425041A ES 425041 A ES425041 A ES 425041A ES 425041 A1 ES425041 A1 ES 425041A1
Authority
ES
Spain
Prior art keywords
reaction mixture
nitric acid
working
nitration
organic solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES425041A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19732317277 external-priority patent/DE2317277C3/en
Application filed by BASF SE filed Critical BASF SE
Publication of ES425041A1 publication Critical patent/ES425041A1/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/16—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
    • C01B21/38—Nitric acid
    • C01B21/46—Purification; Separation ; Stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/45—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by at least one doubly—bound oxygen atom, not being part of a —CHO group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Procedure for the preparation of a reaction mixture obtained by nitration of aliphatic or cycloaliphatic ketones, if necessary in the presence of the corresponding alcohols, with nitric acid at least 95% by weight, in the presence of an inert organic solvent for the organic compounds characterized in that the reaction mixture is diluted with so much water that, before separation from the organic phase, it contains 10-70% by weight nitric acid, and the separated aqueous phase is extracted with an inert organic solvent . (Machine-translation by Google Translate, not legally binding)
ES425041A 1973-04-06 1974-04-05 Process for working up nitration mixtures Expired ES425041A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19732317277 DE2317277C3 (en) 1973-04-06 Processing of nitriding mixtures

Publications (1)

Publication Number Publication Date
ES425041A1 true ES425041A1 (en) 1976-06-01

Family

ID=5877209

Family Applications (1)

Application Number Title Priority Date Filing Date
ES425041A Expired ES425041A1 (en) 1973-04-06 1974-04-05 Process for working up nitration mixtures

Country Status (8)

Country Link
JP (1) JPS5046618A (en)
BE (1) BE813291A (en)
DD (1) DD112984A5 (en)
ES (1) ES425041A1 (en)
FR (1) FR2224443B3 (en)
GB (1) GB1455594A (en)
IT (1) IT1013072B (en)
NL (1) NL7404407A (en)

Also Published As

Publication number Publication date
DE2317277A1 (en) 1974-10-24
FR2224443A1 (en) 1974-10-31
GB1455594A (en) 1976-11-17
DE2317277B2 (en) 1977-02-10
FR2224443B3 (en) 1978-05-05
JPS5046618A (en) 1975-04-25
IT1013072B (en) 1977-03-30
BE813291A (en) 1974-10-04
DD112984A5 (en) 1975-05-12
NL7404407A (en) 1974-10-08

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