ES285166A1 - Procedure for conversion of 2-dehydro-isoemetine in 2-dehydro-emetine (Machine-translation by Google Translate, not legally binding) - Google Patents
Procedure for conversion of 2-dehydro-isoemetine in 2-dehydro-emetine (Machine-translation by Google Translate, not legally binding)Info
- Publication number
- ES285166A1 ES285166A1 ES285166A ES285166A ES285166A1 ES 285166 A1 ES285166 A1 ES 285166A1 ES 285166 A ES285166 A ES 285166A ES 285166 A ES285166 A ES 285166A ES 285166 A1 ES285166 A1 ES 285166A1
- Authority
- ES
- Spain
- Prior art keywords
- dehydro
- emetine
- translation
- conversion
- machine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XXLZPUYGHQWHRN-RPBOFIJWSA-N dehydroemetine Chemical compound COC1=C(OC)C=C2[C@@H]3CC(C[C@@H]4C5=CC(OC)=C(OC)C=C5CCN4)=C(CC)CN3CCC2=C1 XXLZPUYGHQWHRN-RPBOFIJWSA-N 0.000 title abstract 4
- 238000006243 chemical reaction Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- XXLZPUYGHQWHRN-DQEYMECFSA-N (11bs)-2-[[(1s)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl]methyl]-3-ethyl-9,10-dimethoxy-4,6,7,11b-tetrahydro-1h-benzo[a]quinolizine Chemical compound COC1=C(OC)C=C2[C@@H]3CC(C[C@H]4C5=CC(OC)=C(OC)C=C5CCN4)=C(CC)CN3CCC2=C1 XXLZPUYGHQWHRN-DQEYMECFSA-N 0.000 title 1
- HBAQYPYDRFILMT-UHFFFAOYSA-N 8-[3-(1-cyclopropylpyrazol-4-yl)-1H-pyrazolo[4,3-d]pyrimidin-5-yl]-3-methyl-3,8-diazabicyclo[3.2.1]octan-2-one Chemical class C1(CC1)N1N=CC(=C1)C1=NNC2=C1N=C(N=C2)N1C2C(N(CC1CC2)C)=O HBAQYPYDRFILMT-UHFFFAOYSA-N 0.000 abstract 1
- 125000002252 acyl group Chemical group 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 230000001590 oxidative effect Effects 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
Classifications
-
- H—ELECTRICITY
- H04—ELECTRIC COMMUNICATION TECHNIQUE
- H04Q—SELECTING
- H04Q3/00—Selecting arrangements
- H04Q3/58—Arrangements providing connection between main exchange and sub-exchange or satellite
- H04Q3/62—Arrangements providing connection between main exchange and sub-exchange or satellite for connecting to private branch exchanges
- H04Q3/625—Arrangements in the private branch exchange
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D455/00—Heterocyclic compounds containing quinolizine ring systems, e.g. emetine alkaloids, protoberberine; Alkylenedioxy derivatives of dibenzo [a, g] quinolizines, e.g. berberine
- C07D455/03—Heterocyclic compounds containing quinolizine ring systems, e.g. emetine alkaloids, protoberberine; Alkylenedioxy derivatives of dibenzo [a, g] quinolizines, e.g. berberine containing quinolizine ring systems directly condensed with at least one six-membered carbocyclic ring, e.g. protoberberine; Alkylenedioxy derivatives of dibenzo [a, g] quinolizines, e.g. berberine
- C07D455/04—Heterocyclic compounds containing quinolizine ring systems, e.g. emetine alkaloids, protoberberine; Alkylenedioxy derivatives of dibenzo [a, g] quinolizines, e.g. berberine containing quinolizine ring systems directly condensed with at least one six-membered carbocyclic ring, e.g. protoberberine; Alkylenedioxy derivatives of dibenzo [a, g] quinolizines, e.g. berberine containing a quinolizine ring system condensed with only one six-membered carbocyclic ring, e.g. julolidine
- C07D455/06—Heterocyclic compounds containing quinolizine ring systems, e.g. emetine alkaloids, protoberberine; Alkylenedioxy derivatives of dibenzo [a, g] quinolizines, e.g. berberine containing quinolizine ring systems directly condensed with at least one six-membered carbocyclic ring, e.g. protoberberine; Alkylenedioxy derivatives of dibenzo [a, g] quinolizines, e.g. berberine containing a quinolizine ring system condensed with only one six-membered carbocyclic ring, e.g. julolidine containing benzo [a] quinolizine ring systems
- C07D455/08—Heterocyclic compounds containing quinolizine ring systems, e.g. emetine alkaloids, protoberberine; Alkylenedioxy derivatives of dibenzo [a, g] quinolizines, e.g. berberine containing quinolizine ring systems directly condensed with at least one six-membered carbocyclic ring, e.g. protoberberine; Alkylenedioxy derivatives of dibenzo [a, g] quinolizines, e.g. berberine containing a quinolizine ring system condensed with only one six-membered carbocyclic ring, e.g. julolidine containing benzo [a] quinolizine ring systems having an isoquinolyl-1, a substituted isoquinolyl-1 or an alkylenedioxyisoquinolyl-1 radical linked through only one carbon atom, attached in position 2, e.g. emetine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Astronomy & Astrophysics (AREA)
- General Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- Computer Networks & Wireless Communication (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Process for conversion of 2-dehydro-isoemetin to 2-dehydro-emetine, characterized in that it comprises oxidizing racemic or optically active 2-dehydro-isoemethine, or N-acylated and N-carbalkoxylated derivatives thereof, with a mercuric salt, reduce the oxidation product thus obtained, isolate the desired racemic or optically active 2-dehydro-emetine or its N-acylated and N-carbalkoxylated derivative from the stereoisomeric mixture constituted by the racemic or optically active 2-dehydroemetine and the 2-dehydro -isoemethine or its N-acylated and N-carbalkoxylated derivatives, and, if desired, separating the racemates into their enantiomers and, if desired, removing the acyl or carbaloxy group. (Machine-translation by Google Translate, not legally binding)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH188562A CH419137A (en) | 1962-02-16 | 1962-02-16 | Process for the conversion of 2-dehydro-isoemetine into 2-dehydro-emetine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES285166A1 true ES285166A1 (en) | 1963-08-01 |
Family
ID=4220865
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES285166A Expired ES285166A1 (en) | 1962-02-16 | 1963-02-15 | Procedure for conversion of 2-dehydro-isoemetine in 2-dehydro-emetine (Machine-translation by Google Translate, not legally binding) |
Country Status (11)
| Country | Link |
|---|---|
| BE (1) | BE628009A (en) |
| BR (1) | BR6346786D0 (en) |
| CH (1) | CH419137A (en) |
| DK (1) | DK104175C (en) |
| ES (1) | ES285166A1 (en) |
| FR (1) | FR1348760A (en) |
| GB (1) | GB980591A (en) |
| MY (1) | MY6600031A (en) |
| NL (1) | NL124479C (en) |
| OA (1) | OA00960A (en) |
| SE (1) | SE308315B (en) |
-
1962
- 1962-02-16 CH CH188562A patent/CH419137A/en unknown
-
1963
- 1963-02-04 SE SE1197/63A patent/SE308315B/xx unknown
- 1963-02-05 BE BE628009A patent/BE628009A/en unknown
- 1963-02-11 FR FR924310A patent/FR1348760A/en not_active Expired
- 1963-02-12 BR BR146786/63A patent/BR6346786D0/en unknown
- 1963-02-13 DK DK66963AA patent/DK104175C/en active
- 1963-02-13 GB GB5820/63A patent/GB980591A/en not_active Expired
- 1963-02-14 NL NL288989A patent/NL124479C/nl active
- 1963-02-15 ES ES285166A patent/ES285166A1/en not_active Expired
-
1964
- 1964-12-26 OA OA51055A patent/OA00960A/en unknown
-
1966
- 1966-12-31 MY MY196631A patent/MY6600031A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| SE308315B (en) | 1969-02-10 |
| GB980591A (en) | 1965-01-13 |
| FR1348760A (en) | 1964-01-10 |
| OA00960A (en) | 1968-03-22 |
| BR6346786D0 (en) | 1973-06-14 |
| CH419137A (en) | 1966-08-31 |
| MY6600031A (en) | 1966-12-31 |
| BE628009A (en) | 1963-08-05 |
| NL124479C (en) | 1968-06-17 |
| DK104175C (en) | 1966-04-18 |
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