ES2629996A1 - Solid agrochemical formulation (Machine-translation by Google Translate, not legally binding) - Google Patents
Solid agrochemical formulation (Machine-translation by Google Translate, not legally binding) Download PDFInfo
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- ES2629996A1 ES2629996A1 ES201730178A ES201730178A ES2629996A1 ES 2629996 A1 ES2629996 A1 ES 2629996A1 ES 201730178 A ES201730178 A ES 201730178A ES 201730178 A ES201730178 A ES 201730178A ES 2629996 A1 ES2629996 A1 ES 2629996A1
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
- A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/08—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
Abstract
Description
Se describe un método para preparar la presente formulación (denominado en lo sucesivo "presente método de preparación"). El presente método de preparación comprende una etapa de mezclar el presente compuesto éster y esfenvalerato para preparar una solución uniforme (en lo sucesivo, denominada “etapa A”) y una etapa de impregnación de la solución uniforme preparada en la etapa A en un vehículo absorbente de aceite (en lo sucesivo en el presente documento denominada “etapa B”). A method for preparing the present formulation (hereinafter referred to as "present method of preparation") is described. The present method of preparation comprises a step of mixing the present ester and sphevalerate compound to prepare a uniform solution (hereinafter referred to as "stage A") and an impregnation stage of the uniform solution prepared in stage A in an absorbent vehicle of oil (hereinafter referred to as "stage B").
En la etapa A, esfenvalerato que se calienta para fundir cuando es necesario y el compuesto éster presente se mezclan. Durante el perıodo de las operaciones, se puede añadir un tensioactivo a la mezcla. Esfenvalerato y el presente compuesto éster se mezclan hasta que se forma una mezcla uniforme para obtener una solución uniforme. La operación de mezcla en la etapa A se realiza usando un agitador. Entre los ejemplos del agitador se incluyen un homogeneizador y un agitador de hélice y similares. Cuando esfenvalerato se calienta para fundirse, la solución se enfría a temperatura ambiente. In step A, sphevalerate which is heated to melt when necessary and the ester compound present is mixed. During the period of the operations, a surfactant can be added to the mixture. Esfenvalerate and the present ester compound are mixed until a uniform mixture is formed to obtain a uniform solution. The mixing operation in step A is performed using a stirrer. Examples of the agitator include a homogenizer and a helix agitator and the like. When sphevalerate is heated to melt, the solution is cooled to room temperature.
En la etapa B, la solución uniforme preparada en la etapa A (en lo sucesivo denominada “presente solución” y el vehículo absorbente de aceite se mezclan. Durante el perıodo de las operaciones, se puede añadir un tensioactivo y/o un agente colorante a la mezcla. La presente solución y el vehículo absorbente de aceite se mezclan para impregnar la presente solución en el vehículo absorbente de aceite. La operación de mezcla en la etapa B se realiza usando una máquina mezcladora. Entre los ejemplos de la máquina mezcladora se incluyen un mezclador de cinta, un mezclador Henschel, un mezclador nauta y un mezclador Loedige, y similares. In step B, the uniform solution prepared in step A (hereinafter referred to as "present solution" and the oil absorbing vehicle are mixed. During the period of the operations, a surfactant and / or a coloring agent can be added to the mixture The present solution and the oil absorbing vehicle are mixed to impregnate the present solution in the oil absorbing vehicle The mixing operation in step B is performed using a mixing machine Examples of the mixing machine include a belt mixer, a Henschel mixer, a nauta mixer and a Loedige mixer, and the like.
Un método para cultivar un cultivo en la presente invención (en lo sucesivo, denominado "presente método de cultivo") comprende una etapa de aplicar una cantidad eficaz de la presente formulación al suelo, en el que se cultiva un cultivo (en lo sucesivo, denominado "etapa I"). Entre los ejemplos de una forma de aplicación en la etapa I se incluyen una aplicación en surco, una aplicación de fila lateral y un tratamiento de orificio de perforación (incorporación en el suelo), y similares. A method for cultivating a crop in the present invention (hereinafter referred to as "present cultivation method") comprises a step of applying an effective amount of the present formulation to the soil, in which a crop is cultivated (hereinafter, called "stage I"). Examples of a form of application in stage I include a groove application, a lateral row application and a drill hole treatment (soil incorporation), and the like.
La cantidad de aplicación de la presente formulación aplicado en la etapa I se puede variar dependiendo del tipo de cultivo, de las condiciones de cultivo para el cultivo, del momento de la aplicación, de las condiciones meteorológicas y similares, y que está dentro de un intervalo de normalmente de 5 a 5.000 g y, preferiblemente, de 10 a 2.000 g por 1 hectárea del suelo donde se cultiva el cultivo. The amount of application of the present formulation applied in stage I can be varied depending on the type of crop, the crop conditions for the crop, the time of application, the weather conditions and the like, and which is within a normally range from 5 to 5,000 g and preferably from 10 to 2,000 g per 1 hectare of the soil where the crop is grown.
9 9
la formulación sólida agroquímica (1) de la presente invención (de ahora en adelante the solid agrochemical formulation (1) of the present invention (hereafter
denominada "presente Formulación (1)"). denominated "present Formulation (1)").
Ejemplo de preparación 2 Preparation Example 2
Se calentaron 1,2 partes en peso de esfenvalerato a 60 ºC para fundir y, después, se añadieron 3,8 partes en peso de LINPLAST 13XP. Los ingredientes se mezclaron hasta que se formó una mezcla uniforme y la mezcla uniforme se enfrió a temperatura ambiente para obtener una "solución B”. La solución uniforme B se añadió a 95,0 partes en peso de yeso granular, y después la mezcla se agitó usando una espátula durante 5 minutos para obtener la formulación sólida agroquímica (2) de la presente invención (de ahora en adelante denominada "presente Formulación (2)"). 1.2 parts by weight of sphevalerate were heated to 60 ° C to melt and then 3.8 parts by weight of LINPLAST 13XP were added. The ingredients were mixed until a uniform mixture formed and the uniform mixture was cooled to room temperature to obtain a "solution B." The uniform solution B was added to 95.0 parts by weight of granular plaster, and then the mixture was stirred using a spatula for 5 minutes to obtain the solid agrochemical formulation (2) of the present invention (hereafter referred to as "present Formulation (2)").
Ejemplo de preparación 3 Preparation Example 3
Se calentaron 1,2 partes en peso de esfenvalerato a 60 ºC para fundir y, después, se añadieron 3,8 partes en peso de CITROFLEX A-2. Los ingredientes se mezclaron hasta que se formó una mezcla uniforme y la mezcla uniforme se enfrió a temperatura ambiente para obtener una "solución C”. La solución uniforme C se añadió a 95,0 partes en peso de yeso granular, y después la mezcla se agitó usando una espátula durante 5 minutos para obtener la formulación sólida agroquímica (3) de la presente invención (de ahora en adelante denominada "presente Formulación (3)"). 1.2 parts by weight of sphevalerate were heated at 60 ° C to melt and then 3.8 parts by weight of CITROFLEX A-2 were added. The ingredients were mixed until a uniform mixture formed and the uniform mixture was cooled to room temperature to obtain a "solution C." The uniform solution C was added to 95.0 parts by weight of granular plaster, and then the mixture was stirred using a spatula for 5 minutes to obtain the solid agrochemical formulation (3) of the present invention (hereafter referred to as "present Formulation (3)").
Ejemplo de preparación 4 Preparation Example 4
Se calentaron 1,2 partes en peso de esfenvalerato a 60 ºC para fundir y, después, se añadieron 3,8 partes en peso de citrato de trietilo. Los ingredientes se mezclaron hasta que se formó una mezcla uniforme y la mezcla uniforme se enfrió a temperatura ambiente para obtener una "solución D”. La solución uniforme D se añadió a 95,0 partes en peso de yeso granular, y después la mezcla se agitó usando un mezclador nauta durante 5 minutos para obtener la formulación sólida agroquímica (4) de la presente invención (de ahora en adelante denominada "presente Formulación (4)"). 1.2 parts by weight of sphevalerate were heated to 60 ° C to melt and then 3.8 parts by weight of triethyl citrate were added. The ingredients were mixed until a uniform mixture formed and the uniform mixture was cooled to room temperature to obtain a "solution D". The uniform solution D was added to 95.0 parts by weight of granular plaster, and then the mixture was stirred using a Nauta mixer for 5 minutes to obtain the solid agrochemical formulation (4) of the present invention (hereafter referred to as "present Formulation (4)").
Ejemplo de preparación comparativo 1 Comparative Preparation Example 1
Se calentaron 1,2 partes en peso de esfenvalerato a 60 ºC para fundir y, después, se 1.2 parts by weight of sphevalerate were heated at 60 ° C to melt and then
13 13
añadieron 3,8 partes en peso de Solvesso 200. Los ingredientes se mezclaron hasta que se formó una mezcla uniforme y la mezcla uniforme se enfrió a temperatura ambiente para obtener una "solución I”. La solución uniforme I se añadió a 95,0 partes en peso de yeso granular, y después la mezcla se agitó usando una espátula durante 5 minutos para obtener la formulación sólida agroquímica comparativa (1) de la presente invención (de ahora en adelante denominada "presente formulación comparativa (1)"). added 3.8 parts by weight of Solvesso 200. The ingredients were mixed until a uniform mixture formed and the uniform mixture was cooled to room temperature to obtain a "solution I". The uniform solution I was added to 95.0 parts by weight of granular plaster, and then the mixture was stirred using a spatula for 5 minutes to obtain the comparative agrochemical solid formulation (1) of the present invention (hereafter referred to as "present comparative formulation (1)").
A continuación, se describen Ejemplos de ensayo. Next, Test Examples are described.
Ejemplo de ensayo 1 Test Example 1
Se introdujo suelo en un recipiente de plástico que tenía un diámetro de 7 cm y una profundidad de 12 cm, y se formó un surco de 3 cm de profundidad de modo que tuviera una forma de V en una dirección perpendicular a la superficie del suelo. Se colocó un (1) grano de semilla de maíz en el surco y la formulación sólida agroquímica se aplicó al interior del surco de manera que la tasa de aplicación de esfenvalerato por área del suelo en el recipiente fuera de 120 g/ha y, después, el surco se cerró colocando en el suelo de un lado del surco sobre el surco. Soil was introduced into a plastic container that had a diameter of 7 cm and a depth of 12 cm, and a groove 3 cm deep was formed so that it had a V-shape in a direction perpendicular to the soil surface. One (1) corn seed grain was placed in the groove and the solid agrochemical formulation was applied to the interior of the groove so that the rate of application of sphevalerate per area of soil in the container was 120 g / ha and then , the groove was closed by placing on the ground on one side of the groove above the groove.
El maíz se cultivó en un invernadero. Diez (10) días después de la aplicación de la formulación sólida agroquímica, 20 cabezas de larvas recién nacidas del gusano de la raíz del maíz occidental (Diabrotica virgifera virgifera) se liberaron por una planta de maíz. Este se denominó "parcela tratada”. The corn was grown in a greenhouse. Ten (10) days after the application of the agrochemical solid formulation, 20 heads of newly born larvae of the western corn root worm (Diabrotica virgifera virgifera) were released by a corn plant. This was called "treated plot."
Por otra parte, el maíz se cultivó de una manera similar a las de la parcela tratada, excepto que la formulación sólida agroquímica no se aplicó, y se liberaron 20 cabezas de larvas recién nacidas de Diabrotica virgifera virgifera. Este se denominó "parcela no tratada”. On the other hand, corn was grown in a manner similar to those of the treated plot, except that the solid agrochemical formulation was not applied, and 20 heads of newly born larvae of Diabrotica virgifera virgifera were released. This was called "untreated plot."
Diez (10) días después de la liberación de los insectos, se recogieron las plantas de maíz y se examinó visualmente el daño causado por las larvas recién nacidas de Diabrotica virgifera virgifera a las raíces nodales de maíz y la proporción del número de nódulos dañados y el número de todas las raíces nodales se calculó como una relación del daño conforme a siguiente ecuación (3). Ten (10) days after the release of the insects, the corn plants were collected and the damage caused by the newborn larvae of Diabrotica virgifera virgifera to the nodal roots of corn and the proportion of the number of damaged nodules and The number of all nodal roots was calculated as a ratio of damage according to the following equation (3).
Ec. (3) Relación de daños (%) = 100 × A/B en la que Eq. (3) Damage ratio (%) = 100 × A / B in which
14 14
A: Número de raíces nodales dañadas A: Number of damaged nodal roots
B: Número de todas las raíces nodales B: Number of all nodal roots
5 El valor preventivo se calculó de acuerdo con la siguiente ecuación (4) y se calculó entonces un valor preventivo promedio de 5 repeticiones. Ec. (4) Valor preventivo (%) = 100 × (1-C/D) 5 The preventive value was calculated according to the following equation (4) and an average preventive value of 5 repetitions was then calculated. Equ. (4) Preventive value (%) = 100 × (1-C / D)
10 en la que 10 in which
C: Relación de daño de la parcela tratada C: Damage ratio of the treated plot
D: Relación de daño del parcela no tratada D: Damage ratio of untreated plot
15 El resultado se muestra en la Tabla 1. 15 The result is shown in Table 1.
[Tabla 1] [Table 1]
- Formulación sólida agroquímica aplicada Solid agrochemical formulation applied
- Valor Preventivo (%) Preventive Value (%)
- Presente formulación (1) Present formulation (1)
- 73,5 73.5
- Presente formulación (2) Present formulation (2)
- 72,5 72.5
- Presente formulación (3) Present formulation (3)
- 65,3 65.3
- Presente formulación (4) Present formulation (4)
- 69,1 69.1
- Formulación comparativa (1) Comparative Formulation (1)
- 30,9 30.9
15 fifteen
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2016-026626 | 2016-02-16 | ||
| JP2016026626A JP2017145204A (en) | 2016-02-16 | 2016-02-16 | Agrochemical solid preparation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES2629996A1 true ES2629996A1 (en) | 2017-08-17 |
| ES2629996B1 ES2629996B1 (en) | 2018-02-28 |
Family
ID=59501660
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES201730178A Active ES2629996B1 (en) | 2016-02-16 | 2017-02-14 | AGROCHEMICAL SOLID FORMULATION |
Country Status (4)
| Country | Link |
|---|---|
| JP (1) | JP2017145204A (en) |
| ES (1) | ES2629996B1 (en) |
| FR (1) | FR3047639B1 (en) |
| HU (1) | HUP1700073A2 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20170231222A1 (en) | 2016-02-16 | 2017-08-17 | Sumitomo Chemical Company, Limited | Coated agrochemical granule |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111972228A (en) * | 2020-09-01 | 2020-11-24 | 广西大学 | Method for planting southern forage grass formula |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2002635A (en) * | 1977-08-05 | 1979-02-28 | Fumakilla Ltd | Method of enchancing the activity of fast evaporating insecticides |
| US20090263437A1 (en) * | 2008-04-16 | 2009-10-22 | Talmor Giora | Pesticide compositions |
| WO2012146887A1 (en) * | 2011-04-26 | 2012-11-01 | Syngenta Limited | Formulation component |
-
2016
- 2016-02-16 JP JP2016026626A patent/JP2017145204A/en active Pending
-
2017
- 2017-02-14 ES ES201730178A patent/ES2629996B1/en active Active
- 2017-02-15 FR FR1751228A patent/FR3047639B1/en active Active
- 2017-02-15 HU HU1700073A patent/HUP1700073A2/en unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2002635A (en) * | 1977-08-05 | 1979-02-28 | Fumakilla Ltd | Method of enchancing the activity of fast evaporating insecticides |
| US20090263437A1 (en) * | 2008-04-16 | 2009-10-22 | Talmor Giora | Pesticide compositions |
| WO2012146887A1 (en) * | 2011-04-26 | 2012-11-01 | Syngenta Limited | Formulation component |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20170231222A1 (en) | 2016-02-16 | 2017-08-17 | Sumitomo Chemical Company, Limited | Coated agrochemical granule |
| US10531661B2 (en) | 2016-02-16 | 2020-01-14 | Sumitomo Chemical Company, Limited | Coated agrochemical granule |
Also Published As
| Publication number | Publication date |
|---|---|
| FR3047639B1 (en) | 2020-03-06 |
| FR3047639A1 (en) | 2017-08-18 |
| JP2017145204A (en) | 2017-08-24 |
| HUP1700073A2 (en) | 2017-08-28 |
| ES2629996B1 (en) | 2018-02-28 |
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