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ES2178778T3 - PROCEDURE FOR OBTAINING A DETERGENT COMPOSITION BY A TOWER-FREE PROCESS. - Google Patents

PROCEDURE FOR OBTAINING A DETERGENT COMPOSITION BY A TOWER-FREE PROCESS.

Info

Publication number
ES2178778T3
ES2178778T3 ES97928871T ES97928871T ES2178778T3 ES 2178778 T3 ES2178778 T3 ES 2178778T3 ES 97928871 T ES97928871 T ES 97928871T ES 97928871 T ES97928871 T ES 97928871T ES 2178778 T3 ES2178778 T3 ES 2178778T3
Authority
ES
Spain
Prior art keywords
procedure
tower
obtaining
phase
detergent composition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97928871T
Other languages
Spanish (es)
Inventor
Greco Angela Gloria Del
Wayne Edward Beimesch
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Procter and Gamble Co
Original Assignee
Procter and Gamble Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co
Application granted granted Critical
Publication of ES2178778T3 publication Critical patent/ES2178778T3/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/02—Preparation in the form of powder by spray drying
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C11D17/065—High-density particulate detergent compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/146—Sulfuric acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/29—Sulfates of polyoxyalkylene ethers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCEDIMIENTO QUE NO UTILIZA UNA TORRE, PARA PREPARAR DE FORMA CONTINUA UNA COMPOSICION DETERGENTE GRANULAR DE DENSIDAD APROX. DE 600 G/L. DICHO PROCEDIMIENTO COMPRENDE LAS SIGUIENTES FASES: (A) (I) DISPERSAR UN TENSIOACTIVO Y REVESTIR DICHO TENSIOACTIVO CON POLVO FINO, CUYO DIAMETRO ESTE COMPRENDIDO ENTRE 0,1 Y 500 MICRONES, EN UN MEZCLADOR Y (B) GRANULAR LOS AGLOMERADOS EN UNO O MAS APARATOS DE FLUIDIFICACION. DICHO PROCEDIMIENTO PUEDE COMPRENDER ASIMISMO UNA FASE ADICIONAL (A'') QUE CONSISTE EN PULVERIZAR UN LIQUIDO FINAMENTE ATOMIZADO SOBRE LOS PRIMEROS AGLOMERADOS, EN UN MEZCLADOR, ENTRE LA FASE (A) Y LA FASE (B).THE INVENTION REFERS TO A PROCEDURE THAT DOES NOT USE A TOWER, TO PREPARE A DETERGENT GRANULAR COMPOSITION OF APPROX DENSITY CONTINUOUSLY. OF 600 G / L. SUCH PROCEDURE UNDERSTAND THE FOLLOWING PHASES: (A) (I) DISPERSE A TENSIOACTIVE AND COVER SUCH TENSIOACTIVE WITH FINE POWDER, WHOSE DIAMETER THIS UNDERSTANDED BETWEEN 0.1 AND 500 MICRONS, IN A MIXER AND (B) GRANULAR AG FLUIDIFICATION DEVICES. SUCH PROCEDURE CAN ALSO UNDERSTAND AN ADDITIONAL PHASE (A '') THAT CONSISTS OF SPRAYING A FINALLY ATOMIZED LIQUID ON THE FIRST AGLOMERATED, IN A MIXER, BETWEEN PHASE (A) AND PHASE (B).

ES97928871T 1996-10-04 1997-06-05 PROCEDURE FOR OBTAINING A DETERGENT COMPOSITION BY A TOWER-FREE PROCESS. Expired - Lifetime ES2178778T3 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/US1996/015881 WO1998014549A1 (en) 1996-10-04 1996-10-04 Process for making a low density detergent composition by non-tower process

Publications (1)

Publication Number Publication Date
ES2178778T3 true ES2178778T3 (en) 2003-01-01

Family

ID=22255901

Family Applications (5)

Application Number Title Priority Date Filing Date
ES97928871T Expired - Lifetime ES2178778T3 (en) 1996-10-04 1997-06-05 PROCEDURE FOR OBTAINING A DETERGENT COMPOSITION BY A TOWER-FREE PROCESS.
ES97929815T Expired - Lifetime ES2201305T3 (en) 1996-10-04 1997-06-05 PROCEDURE FOR MANUFACTURING A DETERGENT COMPOSITION WITHOUT USING TOWERS.
ES97931058T Expired - Lifetime ES2193386T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO PRODUCE A DETERGENT COMPOSITION WITHOUT USING A TOWER.
ES97931056T Expired - Lifetime ES2210544T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO PRODUCE A DETERGENT COMPOSITION THROUGH A PROCEDURE WITHOUT TOWERS.
ES97928872T Expired - Lifetime ES2212109T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO MANUFACTURE A DETERGENT COMPOSITION BY A TOWER-FREE PROCEDURE.

Family Applications After (4)

Application Number Title Priority Date Filing Date
ES97929815T Expired - Lifetime ES2201305T3 (en) 1996-10-04 1997-06-05 PROCEDURE FOR MANUFACTURING A DETERGENT COMPOSITION WITHOUT USING TOWERS.
ES97931058T Expired - Lifetime ES2193386T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO PRODUCE A DETERGENT COMPOSITION WITHOUT USING A TOWER.
ES97931056T Expired - Lifetime ES2210544T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO PRODUCE A DETERGENT COMPOSITION THROUGH A PROCEDURE WITHOUT TOWERS.
ES97928872T Expired - Lifetime ES2212109T3 (en) 1996-10-04 1997-06-05 PROCEDURE TO MANUFACTURE A DETERGENT COMPOSITION BY A TOWER-FREE PROCEDURE.

Country Status (12)

Country Link
EP (9) EP0929645A1 (en)
JP (9) JP3305327B2 (en)
CN (8) CN1156561C (en)
AR (6) AR010729A1 (en)
AT (5) ATE223476T1 (en)
AU (9) AU7388196A (en)
BR (7) BR9612732A (en)
CA (9) CA2267291C (en)
DE (5) DE69726440T2 (en)
ES (5) ES2178778T3 (en)
MX (2) MX219077B (en)
WO (9) WO1998014549A1 (en)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4249804B2 (en) * 1995-04-03 2009-04-08 ノバルティス・アクチエンゲゼルシャフト Pyrazole derivative and process for producing the same
GB9526097D0 (en) * 1995-12-20 1996-02-21 Unilever Plc Process
GB9712583D0 (en) 1997-06-16 1997-08-20 Unilever Plc Production of detergent granulates
GB9712580D0 (en) * 1997-06-16 1997-08-20 Unilever Plc Production of detergent granulates
GB9713748D0 (en) * 1997-06-27 1997-09-03 Unilever Plc Production of detergent granulates
JP2002507629A (en) 1997-07-14 2002-03-12 ザ、プロクター、エンド、ギャンブル、カンパニー Method for making low-density detergent composition by controlling agglomeration by particle size
CN1218027C (en) 1997-07-14 2005-09-07 普罗格特-甘布尔公司 Process for making low density detergent composition by controlled agglomeration in fluid bed dryer
WO1999003965A1 (en) 1997-07-15 1999-01-28 The Procter & Gamble Company Process for making high-active detergent agglomerates by multi-stage surfactant paste injection
US6440342B1 (en) 1998-07-08 2002-08-27 The Procter & Gamble Company Process for making a low density detergent composition by controlling nozzle height in a fluid bed dryer
ATE336564T1 (en) 1998-08-20 2006-09-15 Procter & Gamble METHOD FOR PRODUCING DETERGENT USING A MEDIUM-SPEED MIXER/COMPRESSOR
US6794354B1 (en) * 1998-09-18 2004-09-21 The Procter & Gamble Company Continuous process for making detergent composition
BR9914809A (en) 1998-10-26 2001-07-03 Procter & Gamble Processes for preparing granular detergent composition having improved appearance and solubility
GB9825558D0 (en) * 1998-11-20 1999-01-13 Unilever Plc Granular detergent components and particulate detergent compositions containing them
GB9913546D0 (en) 1999-06-10 1999-08-11 Unilever Plc Granular detergent component containing zeolite map and laundry detergent compositions containing it
US6894018B1 (en) 1999-06-21 2005-05-17 The Procter & Gamble Company Process for making granular detergent in a fluidized bed granulator having recycling of improperly sized particles
CN1200999C (en) * 1999-06-21 2005-05-11 宝洁公司 Process for making granular detergent compsn.
GB0009877D0 (en) † 2000-04-20 2000-06-07 Unilever Plc Granular detergent component and process for its preparation
EP2123742A1 (en) 2008-05-14 2009-11-25 The Procter and Gamble Company A solid laundry detergent composition comprising light density silicate salt
WO2011061045A1 (en) 2009-11-20 2011-05-26 Unilever Nv Detergent granule and its manufacture
WO2015154277A1 (en) 2014-04-10 2015-10-15 The Procter & Gamble Company Composite detergent granules and laundry compositions comprising the same
EP4421156A1 (en) * 2018-01-26 2024-08-28 Ecolab USA Inc. Solidifying liquid anionic surfactants
EP3743495A1 (en) 2018-01-26 2020-12-02 Ecolab USA Inc. Solidifying liquid amine oxide, betaine, and/or sultaine surfactants with a carrier
MX2020007859A (en) 2018-01-26 2020-09-18 Ecolab Usa Inc Solidifying liquid amine oxide, betaine, and/or sultaine surfactants with a binder and optional carrier.

Family Cites Families (15)

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Publication number Priority date Publication date Assignee Title
US3625902A (en) * 1968-10-11 1971-12-07 Stauffer Chemical Co Method of preparing agglomerated detergent composition
US4169806A (en) * 1978-08-09 1979-10-02 The Procter & Gamble Company Agglomeration process for making granular detergents
US4992079A (en) * 1986-11-07 1991-02-12 Fmc Corporation Process for preparing a nonphosphate laundry detergent
GB2209172A (en) * 1987-08-28 1989-05-04 Unilever Plc Preparation of solid particulate components for detergents
KR0170424B1 (en) * 1990-07-05 1999-01-15 호르스트 헤를레,요한 글라슬 Method for preparing surface active agent granules for detergents and cleaning agents
EP0557466B1 (en) * 1990-11-14 1995-04-12 The Procter & Gamble Company Process for the preparation of nonphosphated dishwashing compositions with oxygen bleach systems
DE69220773T2 (en) * 1992-02-14 1998-02-12 Procter & Gamble Process for the production of detergent granules by neutralization of sulfonic acids
KR100276030B1 (en) * 1992-06-15 2000-12-15 데이비드 엠 모이어 Manufacturing method of detergent granules and detergent granules prepared by such method
ATE172240T1 (en) * 1992-07-15 1998-10-15 Procter & Gamble DETERGENT COMPOSITIONS
CA2173108A1 (en) * 1993-10-15 1995-04-20 Scott William Capeci Continuous process for making high density detergent granules
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ATE195549T1 (en) * 1994-01-17 2000-09-15 Procter & Gamble METHOD FOR PRODUCING CLEANING AGENT GRANULES
US5489392A (en) * 1994-09-20 1996-02-06 The Procter & Gamble Company Process for making a high density detergent composition in a single mixer/densifier with selected recycle streams for improved agglomerate properties
US5516448A (en) * 1994-09-20 1996-05-14 The Procter & Gamble Company Process for making a high density detergent composition which includes selected recycle streams for improved agglomerate
US5554587A (en) * 1995-08-15 1996-09-10 The Procter & Gamble Company Process for making high density detergent composition using conditioned air

Also Published As

Publication number Publication date
CA2268055C (en) 2004-02-03
AR010729A1 (en) 2000-07-12
AU3478597A (en) 1998-04-24
JP2000507632A (en) 2000-06-20
EP0929652A1 (en) 1999-07-21
CN1239507A (en) 1999-12-22
CA2267291A1 (en) 1998-04-09
DE69723986T2 (en) 2004-06-03
CA2268055A1 (en) 1998-04-09
WO1998014552A1 (en) 1998-04-09
AU3303097A (en) 1998-04-24
JP3305327B2 (en) 2002-07-22
WO1998014554A1 (en) 1998-04-09
EP0929649A1 (en) 1999-07-21
CA2267424A1 (en) 1998-04-09
BR9711861A (en) 1999-08-24
MX9903193A (en) 2000-01-31
CA2268063C (en) 2002-10-29
ES2212109T3 (en) 2004-07-16
JP2000503716A (en) 2000-03-28
BR9612732A (en) 1999-08-24
JP3299983B2 (en) 2002-07-08
AR010508A1 (en) 2000-06-28
ATE223476T1 (en) 2002-09-15
CA2268068A1 (en) 1998-04-09
BR9711865A (en) 1999-08-24
WO1998014556A1 (en) 1998-04-09
JP3299981B2 (en) 2002-07-08
JP3345022B2 (en) 2002-11-18
CA2268062C (en) 2002-11-12
BR9712490A (en) 1999-10-19
CA2268052C (en) 2003-12-30
EP0929655A1 (en) 1999-07-21
MX219077B (en) 2004-02-10
JP2000503717A (en) 2000-03-28
EP0929645A1 (en) 1999-07-21
EP0929654A1 (en) 1999-07-21
CN1156562C (en) 2004-07-07
ATE238409T1 (en) 2003-05-15
CN1239993A (en) 1999-12-29
CA2268052A1 (en) 1998-04-09
ATE255159T1 (en) 2003-12-15
CA2268062A1 (en) 1998-04-09
CN1156563C (en) 2004-07-07
EP0929653B1 (en) 2003-04-23
CA2268063A1 (en) 1998-04-09
DE69721287T2 (en) 2004-03-11
DE69726440T2 (en) 2004-09-09
DE69726439T2 (en) 2004-09-09
DE69726440D1 (en) 2004-01-08
AU7388196A (en) 1998-04-24
CA2267424C (en) 2004-01-06
EP0929648B1 (en) 2002-09-04
BR9712492A (en) 1999-10-19
JP2000503720A (en) 2000-03-28
JP2000503718A (en) 2000-03-28
CN1239508A (en) 1999-12-22
EP0929651B1 (en) 2003-11-26
EP0929650B1 (en) 2003-08-06
JP2000503719A (en) 2000-03-28
DE69723986D1 (en) 2003-09-11
CA2268067A1 (en) 1998-04-09
JP2000503715A (en) 2000-03-28
AU3568397A (en) 1998-04-24
AR010507A1 (en) 2000-06-28
EP0929651A1 (en) 1999-07-21
WO1998014549A1 (en) 1998-04-09
ATE255160T1 (en) 2003-12-15
CN1239991A (en) 1999-12-29
JP2000504062A (en) 2000-04-04
AR010511A1 (en) 2000-06-28
DE69715224D1 (en) 2002-10-10
CN1239506A (en) 1999-12-22
JP3299982B2 (en) 2002-07-08
AU3378597A (en) 1998-04-24
BR9713249A (en) 1999-11-03
BR9713246A (en) 1999-11-03
AR010509A1 (en) 2000-06-28
MX9903195A (en) 1999-09-30
CN1239992A (en) 1999-12-29
WO1998014555A1 (en) 1998-04-09
CA2268067C (en) 2004-01-06
DE69721287D1 (en) 2003-05-28
CA2267291C (en) 2002-12-10
ES2201305T3 (en) 2004-03-16
AU3478397A (en) 1998-04-24
ATE246726T1 (en) 2003-08-15
DE69726439D1 (en) 2004-01-08
AU3478497A (en) 1998-04-24
CN1239995A (en) 1999-12-29
CA2268060C (en) 2003-04-22
CA2268068C (en) 2003-06-03
ES2210544T3 (en) 2004-07-01
JP3299986B2 (en) 2002-07-08
JP2000503721A (en) 2000-03-28
EP0929653A1 (en) 1999-07-21
WO1998014557A1 (en) 1998-04-09
CN1133739C (en) 2004-01-07
ES2193386T3 (en) 2003-11-01
EP0929649B1 (en) 2003-11-26
WO1998014551A1 (en) 1998-04-09
JP3299985B2 (en) 2002-07-08
CN1133738C (en) 2004-01-07
CN1156560C (en) 2004-07-07
CN1156561C (en) 2004-07-07
EP0929648A1 (en) 1999-07-21
AU3303197A (en) 1998-04-24
EP0929650A1 (en) 1999-07-21
AU3478297A (en) 1998-04-24
CN1239994A (en) 1999-12-29
MX219076B (en) 2004-02-10
JP3299984B2 (en) 2002-07-08
JP3299987B2 (en) 2002-07-08
WO1998014553A1 (en) 1998-04-09
WO1998014558A1 (en) 1998-04-09
AR010510A1 (en) 2000-06-28
DE69715224T2 (en) 2003-08-07
CA2268060A1 (en) 1998-04-09

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