ES2131311T3 - PROCEDURE FOR PREPARING POLYOLES OF POLYOLES WITH LOW LEVELS OF TRIGLYCERIDES. - Google Patents
PROCEDURE FOR PREPARING POLYOLES OF POLYOLES WITH LOW LEVELS OF TRIGLYCERIDES.Info
- Publication number
- ES2131311T3 ES2131311T3 ES95912772T ES95912772T ES2131311T3 ES 2131311 T3 ES2131311 T3 ES 2131311T3 ES 95912772 T ES95912772 T ES 95912772T ES 95912772 T ES95912772 T ES 95912772T ES 2131311 T3 ES2131311 T3 ES 2131311T3
- Authority
- ES
- Spain
- Prior art keywords
- polyoles
- triglycerides
- procedure
- preparing
- low levels
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 150000003626 triacylglycerols Chemical class 0.000 title abstract 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract 2
- -1 POLYOL FATTY ACID Chemical class 0.000 abstract 2
- 235000014113 dietary fatty acids Nutrition 0.000 abstract 2
- 229930195729 fatty acid Natural products 0.000 abstract 2
- 239000000194 fatty acid Substances 0.000 abstract 2
- 229920005862 polyol Polymers 0.000 abstract 2
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical compound CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 abstract 1
- 235000011187 glycerol Nutrition 0.000 abstract 1
- 150000004702 methyl esters Chemical class 0.000 abstract 1
- 229920000728 polyester Polymers 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C07H13/06—Fatty acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyesters Or Polycarbonates (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Fats And Perfumes (AREA)
- Medicinal Preparation (AREA)
- Saccharide Compounds (AREA)
Abstract
SE DESCRIBE UN PROCEDIMIENTO PARA PREPARAR POLIESTERES DE ACIDO GRASO DE POLIOL CON NIVELES DE TRIGLICERIDOS POR DEBAJO DEL 0.5%. SE PREPARAN METILESTERES QUE TIENEN UN NIVEL DE MONOGLICERIDOS POR DEBAJO DE 500 PPM, UN NIVEL DE DIGLICERIDOS Y TRIGLICERIDOS NO DETECTABLE Y UN NIVEL DE GLICERINA INFERIOR A 200 PPM Y DESPUES SE USAN EN UNA REACCION DE TRANSESTERIFICACION EN DOS ETAPAS LIBRE DE DISOLVENTE PARA PREPARAR LOS POLIESTERES DE ACIDO GRASO DE POLIOL.A PROCEDURE FOR PREPARING POLYOL FATTY ACID POLYESTERS WITH TRIGLYCERIDES LEVELS BELOW 0.5% IS DESCRIBED. METHYLESTERS ARE PREPARED THAT HAVE A MONOGLYCERIDES LEVEL BELOW 500 PPM, A NON-DETECTABLE DIGLYCERIDES AND TRIGLYCERIDES LEVEL AND A LEVEL OF GLYCERIN LESS THAN 200 PPM AND THEN THEY ARE USED IN A TRANSPARATION REACTION IN TWO STAGES POLYOLES OF POLYOL FATTY ACID.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/223,624 US5491226A (en) | 1994-04-06 | 1994-04-06 | Process for preparing polyol polyesters having low levels of triglycerides |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2131311T3 true ES2131311T3 (en) | 1999-07-16 |
Family
ID=22837321
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES95912772T Expired - Lifetime ES2131311T3 (en) | 1994-04-06 | 1995-03-06 | PROCEDURE FOR PREPARING POLYOLES OF POLYOLES WITH LOW LEVELS OF TRIGLYCERIDES. |
Country Status (15)
Country | Link |
---|---|
US (1) | US5491226A (en) |
EP (1) | EP0754186B1 (en) |
JP (1) | JPH09511522A (en) |
CN (1) | CN1045092C (en) |
AT (1) | ATE180260T1 (en) |
BR (1) | BR9507344A (en) |
CA (1) | CA2186464C (en) |
DE (1) | DE69509768T2 (en) |
DK (1) | DK0754186T3 (en) |
ES (1) | ES2131311T3 (en) |
FI (1) | FI963997A0 (en) |
GR (1) | GR3030270T3 (en) |
MY (1) | MY112718A (en) |
NO (1) | NO305208B1 (en) |
WO (1) | WO1995027719A1 (en) |
Families Citing this family (32)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FI95367C (en) * | 1994-09-07 | 1996-01-25 | Raision Tehtaat Oy Ab | Method for preparing a synthetic ester from vegetable oil |
US5648483A (en) * | 1995-06-07 | 1997-07-15 | The Procter & Gamble Company | Continuous transesterification method for preparing polyol polyesters |
FR2752850A1 (en) * | 1996-08-27 | 1998-03-06 | Inst Francais Du Petrole | COMPOSITIONS OF ADDITIVES IMPROVING THE LUBRICATING POWER OF FUELS AND FUELS CONTAINING THEM |
US6143801A (en) * | 1996-12-20 | 2000-11-07 | The University Of North Carolina At Chapel Hill | Catalyst for ester metathesis |
US6465642B1 (en) | 1997-02-07 | 2002-10-15 | The Procter & Gamble Company | Lower alkyl ester recycling in polyol fatty acid polyester synthesis |
DE19742097C1 (en) * | 1997-09-24 | 1998-12-10 | Henkel Kgaa | Recovery of light-coloured fatty acid lower alkyl especially methyl ester with low glycerol content |
US6965043B1 (en) * | 1997-11-10 | 2005-11-15 | Procter + Gamble Co. | Process for making high purity fatty acid lower alkyl esters |
WO2000009528A1 (en) * | 1998-08-13 | 2000-02-24 | The Procter & Gamble Company | Lower alkyl ester recycling synthesis |
US20020058774A1 (en) * | 2000-09-06 | 2002-05-16 | Kurth Thomas M. | Transesterified polyol having selectable and increased functionality and urethane material products formed using the polyol |
US7063877B2 (en) | 1998-09-17 | 2006-06-20 | Urethane Soy Systems Company, Inc. | Bio-based carpet material |
US6180686B1 (en) | 1998-09-17 | 2001-01-30 | Thomas M. Kurth | Cellular plastic material |
US8575226B2 (en) * | 1998-09-17 | 2013-11-05 | Rhino Linings Corporation | Vegetable oil-based coating and method for application |
US6979477B2 (en) | 2000-09-06 | 2005-12-27 | Urethane Soy Systems Company | Vegetable oil-based coating and method for application |
US6962636B2 (en) * | 1998-09-17 | 2005-11-08 | Urethane Soy Systems Company, Inc. | Method of producing a bio-based carpet material |
US20030191274A1 (en) * | 2001-10-10 | 2003-10-09 | Kurth Thomas M. | Oxylated vegetable-based polyol having increased functionality and urethane material formed using the polyol |
CA2388296A1 (en) | 1999-10-15 | 2001-04-26 | Danisco Cultor America, Inc. | Method for the direct esterification of sorbitol with fatty acids |
WO2002060975A1 (en) | 2001-01-31 | 2002-08-08 | The Procter & Gamble Company | Synthesis of polyol medium fatty acid polyesters |
US6723863B2 (en) * | 2001-08-09 | 2004-04-20 | Archer-Daniels-Midland Company | Methods for the preparation of propylene glycol fatty acid esters |
US20040086621A1 (en) * | 2002-11-06 | 2004-05-06 | Kraft Foods Holdings, Inc. | Reduced calorie fat |
US20090127499A1 (en) * | 2004-05-14 | 2009-05-21 | Tran Bo L | Methods and compositions for dust control and freeze conditioning |
GB0423972D0 (en) * | 2004-10-28 | 2004-12-01 | Vincent Processes Ltd | Process for the production of esters of sugars and sugar derivatives |
AU2006218395A1 (en) | 2005-03-03 | 2006-09-08 | South Dakota Soybean Processors, Llc | Novel polyols derived from a vegetable oil using an oxidation process |
CN1696100B (en) * | 2005-06-01 | 2010-11-24 | 黑龙江福和华星制药集团股份有限公司 | Now short cutting method for synthcsizing Adpalin dryg trcatubg acnc |
GB0608512D0 (en) * | 2006-04-28 | 2006-06-07 | Vincent Processes Ltd | Process for the production of esters of sugars and sugar derivatives |
CN101195572B (en) * | 2006-12-08 | 2010-06-09 | 四川古杉油脂化学有限公司 | Method for synthesizing fatty acid methyl ester |
US20090005583A1 (en) * | 2007-06-29 | 2009-01-01 | Benecke Herman P | Preparation of Propylene Glycol Fatty Acid Ester or Other Glycol or Polyol Fatty Acid Esters |
GB0724721D0 (en) * | 2007-12-19 | 2008-01-30 | Ici Plc | A method of making triglyceride macromonomers |
WO2010058918A2 (en) * | 2008-11-19 | 2010-05-27 | (주)에스엠피오티 | Method for preparing polyol ester |
WO2011007361A1 (en) * | 2009-07-17 | 2011-01-20 | Tata Chemicals Ltd . | A process for production of biolubricant using fly ash as a catalyst |
CN104171973A (en) * | 2014-07-08 | 2014-12-03 | 北京市营养源研究所 | Healthy sugar-free popcorn with function of relaxing bowel |
US9493608B1 (en) * | 2015-12-21 | 2016-11-15 | Covestro Llc | DMC catalyzed alkoxylation of esters |
CN107698447B (en) * | 2016-08-09 | 2021-10-29 | 浙江医药股份有限公司新昌制药厂 | Method for preparing fatty glyceride |
Family Cites Families (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2177407A (en) * | 1936-09-21 | 1939-10-24 | Du Pont | Alcoholysis of glycerides |
US2290609A (en) * | 1940-09-10 | 1942-07-21 | Henry A Wallace | Process for producing fatty acid polyhydric esters from glycerides |
US2360844A (en) * | 1941-11-26 | 1944-10-24 | Du Pont | Preparation of detergents |
US2383614A (en) * | 1942-10-17 | 1945-08-28 | Colgate Palmolive Peet Co | Treatment of fatty glycerides |
US2383596A (en) * | 1943-01-30 | 1945-08-28 | Colgate Palmolive Peet Co | Method of treating fatty glycerides |
US2383633A (en) * | 1943-01-30 | 1945-08-28 | Colgate Palmolive Peet Co | Process for treating fatty glycerides |
US2383580A (en) * | 1943-03-20 | 1945-08-28 | Colgate Palmolive Peet Co | Treating fatty materials |
US3054789A (en) * | 1959-02-06 | 1962-09-18 | Ledoga Spa | Process for the preparation of pure sucrose esters |
US3349081A (en) * | 1963-06-26 | 1967-10-24 | Ledoga Spa | Process for preparing sucrose esters of high molecular weight fatty acids |
GB1399053A (en) * | 1973-03-16 | 1975-06-25 | Tate & Lyle Ltd | Process for the production of surface active agents comprising sucrose esters |
NL158165B (en) * | 1973-05-15 | 1978-10-16 | Amsterdam Chem Comb | PROCESS FOR THE PREPARATION OF CARBONIC ACID ESTERS FROM LINEAR ALIPHATIC SUGAR ALCOHOLS. |
NO142306C (en) * | 1975-04-18 | 1980-07-30 | Tate & Lyle Ltd | PROCEDURE FOR CLEANING A SOLID SUBSTANCE IN THE FORM OF A TRANSFER PRODUCT PRODUCT BY REACTION BETWEEN SUCROSE AND AT LEAST ONE FATTY ACID TRIGLYCERIDE |
WO1980002156A1 (en) * | 1979-04-05 | 1980-10-16 | Mitsui Toatsu Chemicals | Process for purifying sugar fatty acid ester |
US4582946A (en) * | 1979-10-04 | 1986-04-15 | Henkel Corporation | Polyhydric alcohols |
JPS56120799A (en) * | 1980-02-28 | 1981-09-22 | Lion Corp | Manufacture of high quality fatty ester |
DE3128696A1 (en) * | 1981-07-21 | 1983-02-10 | Hoechst Ag, 6000 Frankfurt | "PROCESS FOR CLEANING ESTERS" |
DE3421217A1 (en) * | 1984-06-07 | 1985-09-05 | Hoechst Ag, 6230 Frankfurt | METHOD FOR PRODUCING FATTY ACID ESTERS OF SHORT-CHAIN ALCOHOLS |
NL8601904A (en) * | 1986-07-23 | 1988-02-16 | Unilever Nv | PROCESS FOR THE PREPARATION OF POLYOL FATTY ACID POLYESTERS. |
JPS63179884A (en) * | 1987-01-17 | 1988-07-23 | Mitsubishi Kasei Corp | Method for producing sucrose fatty acid ester |
US4973489A (en) * | 1987-05-13 | 1990-11-27 | Curtice Burns, Inc. | Polysaccaride fatty acid polyester fat substitutes |
US4968791A (en) * | 1987-07-23 | 1990-11-06 | Lever Brothers Company | Process for the preparation of polyol fatty acid esters |
GB8800087D0 (en) * | 1988-01-05 | 1988-02-10 | Unilever Plc | Process for synthesis of polyol fatty acid polyesters |
US4954621A (en) * | 1988-06-14 | 1990-09-04 | Mitsubushi Kasei Corporation | Process for producing sucrose fatty acid polyester |
US4927920A (en) * | 1988-11-15 | 1990-05-22 | Nebraska Department Of Economic Development, State Of Nebraska, U.S.A. | Sugar ester synthesis |
US5043438B1 (en) * | 1989-02-16 | 1998-04-28 | Lever Brothers Ltd | Process for the synthesis of polyol fatty-acid esters |
CA2012381C (en) * | 1989-03-28 | 1997-07-01 | Paul Seiden | Reduced calorie fat compositions containing polyol polyesters and reduced calorie triglycerides |
ATE99280T1 (en) * | 1989-04-05 | 1994-01-15 | Unilever Nv | PROCESS FOR PREPARING LOWER GALCYL FATTY ACID MONOESTER. |
AT394374B (en) * | 1990-06-29 | 1992-03-25 | Wimmer Theodor | METHOD FOR PRODUCING FATTY ACID ESTERS OF LOW ALCOHOLS |
-
1994
- 1994-04-06 US US08/223,624 patent/US5491226A/en not_active Expired - Lifetime
-
1995
- 1995-03-06 DK DK95912772T patent/DK0754186T3/en active
- 1995-03-06 DE DE69509768T patent/DE69509768T2/en not_active Expired - Fee Related
- 1995-03-06 EP EP95912772A patent/EP0754186B1/en not_active Expired - Lifetime
- 1995-03-06 AT AT95912772T patent/ATE180260T1/en not_active IP Right Cessation
- 1995-03-06 CA CA002186464A patent/CA2186464C/en not_active Expired - Fee Related
- 1995-03-06 JP JP7526328A patent/JPH09511522A/en not_active Ceased
- 1995-03-06 BR BR9507344A patent/BR9507344A/en not_active Application Discontinuation
- 1995-03-06 CN CN95192960A patent/CN1045092C/en not_active Expired - Fee Related
- 1995-03-06 ES ES95912772T patent/ES2131311T3/en not_active Expired - Lifetime
- 1995-03-06 WO PCT/US1995/002833 patent/WO1995027719A1/en active IP Right Grant
- 1995-04-07 MY MYPI95000894A patent/MY112718A/en unknown
-
1996
- 1996-10-04 FI FI963997A patent/FI963997A0/en unknown
- 1996-10-04 NO NO964218A patent/NO305208B1/en unknown
-
1999
- 1999-05-20 GR GR990401258T patent/GR3030270T3/en unknown
Also Published As
Publication number | Publication date |
---|---|
CA2186464A1 (en) | 1995-10-19 |
DE69509768T2 (en) | 1999-12-23 |
MY112718A (en) | 2001-08-30 |
BR9507344A (en) | 1997-09-23 |
CN1147814A (en) | 1997-04-16 |
NO305208B1 (en) | 1999-04-19 |
EP0754186A1 (en) | 1997-01-22 |
FI963997L (en) | 1996-10-04 |
DE69509768D1 (en) | 1999-06-24 |
EP0754186B1 (en) | 1999-05-19 |
DK0754186T3 (en) | 1999-11-22 |
FI963997A0 (en) | 1996-10-04 |
CN1045092C (en) | 1999-09-15 |
ATE180260T1 (en) | 1999-06-15 |
MX9604573A (en) | 1997-09-30 |
JPH09511522A (en) | 1997-11-18 |
NO964218D0 (en) | 1996-10-04 |
GR3030270T3 (en) | 1999-08-31 |
US5491226A (en) | 1996-02-13 |
NO964218L (en) | 1996-10-04 |
CA2186464C (en) | 1998-08-18 |
WO1995027719A1 (en) | 1995-10-19 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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