ES2123053T3 - APPARATUS AND METHOD OF EXTRACTION OF COMPOUNDS FROM A SOLUTION. - Google Patents
APPARATUS AND METHOD OF EXTRACTION OF COMPOUNDS FROM A SOLUTION.Info
- Publication number
- ES2123053T3 ES2123053T3 ES93911036T ES93911036T ES2123053T3 ES 2123053 T3 ES2123053 T3 ES 2123053T3 ES 93911036 T ES93911036 T ES 93911036T ES 93911036 T ES93911036 T ES 93911036T ES 2123053 T3 ES2123053 T3 ES 2123053T3
- Authority
- ES
- Spain
- Prior art keywords
- permeate
- column
- wine
- retentate
- anion exchange
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 150000001875 compounds Chemical class 0.000 title abstract 2
- 238000000605 extraction Methods 0.000 title 1
- 239000012466 permeate Substances 0.000 abstract 7
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 abstract 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 5
- 238000005349 anion exchange Methods 0.000 abstract 4
- 238000004821 distillation Methods 0.000 abstract 4
- 239000012465 retentate Substances 0.000 abstract 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 3
- 239000000126 substance Substances 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Natural products CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 abstract 1
- IKHGUXGNUITLKF-XPULMUKRSA-N acetaldehyde Chemical compound [14CH]([14CH3])=O IKHGUXGNUITLKF-XPULMUKRSA-N 0.000 abstract 1
- 235000013334 alcoholic beverage Nutrition 0.000 abstract 1
- 239000012530 fluid Substances 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 239000012528 membrane Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000001223 reverse osmosis Methods 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
- B01D61/025—Reverse osmosis; Hyperfiltration
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/08—Preparation of other alcoholic beverages by methods for altering the composition of fermented solutions or alcoholic beverages not provided for in groups C12G3/02 - C12G3/07
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H3/00—Methods for reducing the alcohol content of fermented solutions or alcoholic beverage to obtain low alcohol or non-alcoholic beverages
- C12H3/02—Methods for reducing the alcohol content of fermented solutions or alcoholic beverage to obtain low alcohol or non-alcoholic beverages by evaporating
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H3/00—Methods for reducing the alcohol content of fermented solutions or alcoholic beverage to obtain low alcohol or non-alcoholic beverages
- C12H3/04—Methods for reducing the alcohol content of fermented solutions or alcoholic beverage to obtain low alcohol or non-alcoholic beverages using semi-permeable membranes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Zoology (AREA)
- Biochemistry (AREA)
- Water Supply & Treatment (AREA)
- Food Science & Technology (AREA)
- Nanotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Electrical Discharge Machining, Electrochemical Machining, And Combined Machining (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
Method and apparatus for the treatment of fluids, particularly wine, to remove unwanted substances. The wine is treated in a reverse osmosis (R.O.) treatment unit, generating a retentate and a raw permeate. The membrane for the R.O. unit is selected to pass in the permeate the unwanted substances, such as volatile acidity (ethyl acetate and acetic acid). The raw permeate is subjected to a treatment column. In the case of volatile acidity, this is an anion exchange column, which removes the acetic acid from the permeate by anion exchange and removes the ethyl acetate by base hydrolysis. This produces a purified permeate, which is depleted in volatile acidity, but contains other components desirable for the wine. The purified permeate is then recombined with the retentate from the R.O. column, and the result is wine with the volatile acidity and little else removed. This wine may be recirculated through the system to remove yet more of the volatile acidity. Before the anion exchange step, a low-energy distillation may be used to remove CO2, H2S, or other relatively volatile compounds. To remove acetaldehyde, a low-energy distillation column is used instead of the anion exchange column, and the distillation residue constitutes the purified permeate that is recombined with the retentate from the R.O. column. A high-energy distillation column may be used to separate out alcohol and water, and then add either the alcohol or the water back to the R.O. retentate, thus producing either a higher alcohol or a lower alcohol beverage.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US88065992A | 1992-05-08 | 1992-05-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2123053T3 true ES2123053T3 (en) | 1999-01-01 |
Family
ID=25376789
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES93911036T Expired - Lifetime ES2123053T3 (en) | 1992-05-08 | 1993-05-04 | APPARATUS AND METHOD OF EXTRACTION OF COMPOUNDS FROM A SOLUTION. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US5480665A (en) |
| EP (1) | EP0639105B1 (en) |
| AT (1) | ATE171390T1 (en) |
| AU (1) | AU661912B2 (en) |
| BG (1) | BG62318B1 (en) |
| CA (1) | CA2135305C (en) |
| DE (1) | DE69321229T2 (en) |
| DK (1) | DK0639105T3 (en) |
| ES (1) | ES2123053T3 (en) |
| HU (1) | HU219319B (en) |
| WO (1) | WO1993023151A1 (en) |
| ZA (1) | ZA933213B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008092982A1 (en) * | 2007-02-02 | 2008-08-07 | Consejo Superior De Investigaciones Científicas | Reduction of volatile acidity in hydroalcoholic liquids for food use |
Families Citing this family (49)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0690124A3 (en) * | 1994-06-02 | 2000-04-26 | Bodegas Y Vinedos Santa Ana S.A. | Alcohol removal procedure for alcoholic beverages and low alcoholic grading beverages obtained thereby |
| EP1146115B1 (en) | 2000-04-14 | 2005-05-11 | Enologica Vason S.r.l. | A method for the tartaric stabilisation of wine and apparatus for its implementation |
| AU781154B2 (en) * | 2000-04-14 | 2005-05-12 | Bryan Richard Tudhope | Apparatus and method for isolating and/or eliminating solutes from a solution |
| ITVI20010161A1 (en) | 2001-07-31 | 2003-01-31 | Enologica Vason Srl | PROCEDURE AND PLANT FOR THE SEPARATION OF UNDESIRABLE SUBSTANCES FROM FOOD LIQUIDS, IN PARTICULAR FROM WINES |
| EP1481051A1 (en) * | 2002-03-05 | 2004-12-01 | VELO Spa | Process and apparatus for wine treatment to reduce its contents of volatile acidity |
| FR2845096B1 (en) * | 2002-09-30 | 2004-10-29 | Vaslin Bucher | PROCESS FOR DEACIDIFYING BEVERAGES |
| BRPI0315698B1 (en) * | 2002-11-18 | 2017-05-09 | Goel Prayas | reducing the pollution rate of wastewater from distilleries to zero% |
| CA2523099C (en) * | 2003-04-25 | 2012-01-17 | 2S-Sophisticated Systems Limited | Distillation method |
| DE10336926A1 (en) * | 2003-08-07 | 2005-03-03 | Eau De Vin Ag | Tasty beverage obtained from reverse osmosis, ultrafiltration or microfiltration |
| AU2004201949A1 (en) * | 2004-05-07 | 2005-11-24 | Wine Network Technology Pty. Ltd. | Taint Removal from Wine |
| NZ551931A (en) * | 2004-06-09 | 2010-08-27 | Memstar Pty Ltd | Alcohol reduction in beverages |
| US7455777B2 (en) * | 2004-12-14 | 2008-11-25 | Itt Manufacturing Enterprises, Inc. | Method of adjusting levels of dissolved compounds in beverages |
| AU2006201593B2 (en) * | 2005-04-13 | 2011-02-03 | United Distillers Pty Ltd | Process for alcohol production |
| US8460405B2 (en) * | 2010-02-02 | 2013-06-11 | Celanese International Corporation | Ethanol compositions |
| US8747492B2 (en) | 2010-02-02 | 2014-06-10 | Celanese International Corporation | Ethanol/fuel blends for use as motor fuels |
| US8575403B2 (en) | 2010-05-07 | 2013-11-05 | Celanese International Corporation | Hydrolysis of ethyl acetate in ethanol separation process |
| US8932372B2 (en) | 2010-02-02 | 2015-01-13 | Celanese International Corporation | Integrated process for producing alcohols from a mixed acid feed |
| US8668750B2 (en) | 2010-02-02 | 2014-03-11 | Celanese International Corporation | Denatured fuel ethanol compositions for blending with gasoline or diesel fuel for use as motor fuels |
| US8728179B2 (en) | 2010-02-02 | 2014-05-20 | Celanese International Corporation | Ethanol compositions |
| US8858659B2 (en) * | 2010-02-02 | 2014-10-14 | Celanese International Corporation | Processes for producing denatured ethanol |
| US8541633B2 (en) * | 2010-02-02 | 2013-09-24 | Celanese International Corporation | Processes for producing anhydrous ethanol compositions |
| US8569551B2 (en) | 2010-05-07 | 2013-10-29 | Celanese International Corporation | Alcohol production process integrating acetic acid feed stream comprising water from carbonylation process |
| US8664454B2 (en) | 2010-07-09 | 2014-03-04 | Celanese International Corporation | Process for production of ethanol using a mixed feed using copper containing catalyst |
| US8859827B2 (en) | 2011-11-18 | 2014-10-14 | Celanese International Corporation | Esterifying acetic acid to produce ester feed for hydrogenolysis |
| US9272970B2 (en) | 2010-07-09 | 2016-03-01 | Celanese International Corporation | Hydrogenolysis of ethyl acetate in alcohol separation processes |
| US8710279B2 (en) | 2010-07-09 | 2014-04-29 | Celanese International Corporation | Hydrogenolysis of ethyl acetate in alcohol separation processes |
| US9073816B2 (en) | 2011-04-26 | 2015-07-07 | Celanese International Corporation | Reducing ethyl acetate concentration in recycle streams for ethanol production processes |
| CN103080053B (en) | 2011-04-26 | 2015-08-12 | 国际人造丝公司 | Stacked bed bioreactor is used to produce the method for ethanol |
| US8754268B2 (en) | 2011-04-26 | 2014-06-17 | Celanese International Corporation | Process for removing water from alcohol mixtures |
| US8592635B2 (en) | 2011-04-26 | 2013-11-26 | Celanese International Corporation | Integrated ethanol production by extracting halides from acetic acid |
| US8895786B2 (en) | 2011-08-03 | 2014-11-25 | Celanese International Corporation | Processes for increasing alcohol production |
| US8829249B2 (en) | 2011-11-18 | 2014-09-09 | Celanese International Corporation | Integrated esterification and hydrogenolysis process for producing ethanol |
| US8829251B2 (en) | 2011-11-18 | 2014-09-09 | Celanese International Corporation | Liquid esterification method to produce ester feed for hydrogenolysis |
| US8802901B2 (en) | 2011-11-18 | 2014-08-12 | Celanese International Corporation | Continuous ethyl acetate production and hydrogenolysis thereof |
| US8853468B2 (en) | 2011-11-18 | 2014-10-07 | Celanese International Corporation | Vapor esterification method to produce ester feed for hydrogenolysis |
| US9024089B2 (en) | 2011-11-18 | 2015-05-05 | Celanese International Corporation | Esterification process using extractive separation to produce feed for hydrogenolysis |
| US8748673B2 (en) | 2011-11-18 | 2014-06-10 | Celanese International Corporation | Process of recovery of ethanol from hydrogenolysis process |
| US8927790B2 (en) | 2011-12-15 | 2015-01-06 | Celanese International Corporation | Multiple vapor feeds for hydrogenation process to produce alcohol |
| ITPD20120332A1 (en) | 2012-11-07 | 2014-05-08 | Enologica Vason S P A | PROCEDURE AND PLANT FOR THE EXTRACTION OF COMPOUNDS ACIDS UNDESIDED BY A FOOD LIQUID AND IN PARTICULAR BY A WINE |
| US8975451B2 (en) | 2013-03-15 | 2015-03-10 | Celanese International Corporation | Single phase ester feed for hydrogenolysis |
| PT3303543T (en) | 2015-05-28 | 2019-12-18 | Jorge Ferreira Cameira Dos Santos Paulo | Method for extracting unwanted very weak acidic compounds from a drinkable liquid, in particular from a wine |
| DE102015109344A1 (en) * | 2015-06-11 | 2016-12-15 | Martin Schmitt | Process and apparatus for removing or reducing nitrogen or sulfur compounds from liquid foods or precursors thereof |
| TWI746500B (en) * | 2016-01-22 | 2021-11-21 | 美商愛克瑪公司 | Purification of mercaptans or thiophenes using dividing wall column distillation |
| US10745658B2 (en) | 2017-08-11 | 2020-08-18 | Mark Anthony International Srl | Clarified fermented beverages, and a method thereof |
| US12152224B2 (en) | 2017-08-11 | 2024-11-26 | Mark Anthony International Srl | Refined fermented beverages, and a method thereof |
| AU2019321503A1 (en) * | 2019-07-31 | 2022-03-03 | Mark Anthony International Srl | Refined fermented beverages, and a method thereof |
| US20230271102A1 (en) * | 2020-07-27 | 2023-08-31 | Matthew J. Rubin | Systems and methods for rehabilitating alcohol compositions and rehabilitated alcoholic products |
| US11213766B1 (en) * | 2020-07-27 | 2022-01-04 | Matthew Rubin | Systems and methods for rehabilitating alcohol |
| IT202100032066A1 (en) * | 2021-12-21 | 2023-06-21 | Progetto Ecosoluzioni S R L | METHOD AND RELATED SYSTEM FOR THE CONTROL OF QUERCETIN IN WINE PRODUCTION |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT1027551B (en) * | 1973-09-28 | 1978-12-20 | Henkell & Co | PROCEDURE FOR THE ACCELERATION OF CRYSTALLIZATION IN SPECIES FOR THE PRECIPITATION OF TARARO IN THE WINE AS WELL AS SUITABLE DEVICES FOR THIS PROCEDURE |
| US4205092A (en) * | 1978-08-04 | 1980-05-27 | Cornell Research Foundation, Inc. | Acid reduction in wine by ion exchange |
| FR2497825A1 (en) * | 1981-01-13 | 1982-07-16 | Bonneau Marc | PROCESS FOR THE PREPARATION OF NATURAL BEVERAGES WITH A LOW ALCOHOLIC CONTENT, BEVERAGES AND VARIOUS PRODUCTS OBTAINED BY CARRYING OUT SAID METHOD |
| DD204493A1 (en) * | 1982-02-15 | 1983-11-30 | Zoltan Sziranyi | PROCESS FOR REDUCING THE VOLATILE SAUCE IN WINE OR MOST |
| FR2524000A1 (en) * | 1982-03-24 | 1983-09-30 | Union Brasseries | PROCESS FOR THE MANUFACTURE AND TREATMENT OF ALCOHOLIC BEVERAGES |
| GB8303611D0 (en) * | 1983-02-09 | 1983-03-16 | Ag Patents Ltd | Concentration of alcoholic beverages |
| DE3413085A1 (en) * | 1984-04-06 | 1985-10-24 | Henkell & Co, 6200 Wiesbaden | METHOD FOR REDUCING THE ALCOHOL CONTENT OF BEVERAGES CONTAINING ALCOHOL, IN PARTICULAR WINE AND SPARKLING WINE |
| US4617127A (en) * | 1985-05-20 | 1986-10-14 | Allied Corporation | Production of low alcoholic content beverages |
| IL86319A0 (en) * | 1988-05-09 | 1988-11-15 | Weizmann Kiryat Membrane Prod | Process and apparatus for the removal of undesired components from aqueous feedstocks |
-
1993
- 1993-05-04 ES ES93911036T patent/ES2123053T3/en not_active Expired - Lifetime
- 1993-05-04 WO PCT/US1993/004197 patent/WO1993023151A1/en active IP Right Grant
- 1993-05-04 DK DK93911036T patent/DK0639105T3/en active
- 1993-05-04 HU HU9403192A patent/HU219319B/en not_active IP Right Cessation
- 1993-05-04 AT AT93911036T patent/ATE171390T1/en not_active IP Right Cessation
- 1993-05-04 AU AU42319/93A patent/AU661912B2/en not_active Ceased
- 1993-05-04 EP EP93911036A patent/EP0639105B1/en not_active Expired - Lifetime
- 1993-05-04 CA CA002135305A patent/CA2135305C/en not_active Expired - Fee Related
- 1993-05-04 DE DE69321229T patent/DE69321229T2/en not_active Expired - Fee Related
- 1993-05-07 ZA ZA933213A patent/ZA933213B/en unknown
-
1994
- 1994-03-28 US US08/218,920 patent/US5480665A/en not_active Expired - Lifetime
- 1994-11-04 BG BG99165A patent/BG62318B1/en unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008092982A1 (en) * | 2007-02-02 | 2008-08-07 | Consejo Superior De Investigaciones Científicas | Reduction of volatile acidity in hydroalcoholic liquids for food use |
| ES2303781A1 (en) * | 2007-02-02 | 2008-08-16 | Consejo Superior Invest. Cientificas | REDUCTION OF VOLATILE ACIDITY IN HYDROALCOHOLIC LIQUIDS FOR FOOD USE. |
Also Published As
| Publication number | Publication date |
|---|---|
| AU4231993A (en) | 1993-12-13 |
| ZA933213B (en) | 1994-06-14 |
| AU661912B2 (en) | 1995-08-10 |
| EP0639105A1 (en) | 1995-02-22 |
| CA2135305C (en) | 2001-07-24 |
| DE69321229T2 (en) | 1999-02-18 |
| HU219319B (en) | 2001-03-28 |
| WO1993023151A1 (en) | 1993-11-25 |
| BG99165A (en) | 1995-08-28 |
| BG62318B1 (en) | 1999-08-31 |
| ATE171390T1 (en) | 1998-10-15 |
| CA2135305A1 (en) | 1993-11-25 |
| HUT70805A (en) | 1995-11-28 |
| EP0639105B1 (en) | 1998-09-23 |
| US5480665A (en) | 1996-01-02 |
| DE69321229D1 (en) | 1998-10-29 |
| DK0639105T3 (en) | 1999-06-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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