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ES2033378T3 - Procedimiento para la hidrogenacion de mezclas de esteres metilicos de acidos grasos. - Google Patents

Procedimiento para la hidrogenacion de mezclas de esteres metilicos de acidos grasos.

Info

Publication number
ES2033378T3
ES2033378T3 ES198888111205T ES88111205T ES2033378T3 ES 2033378 T3 ES2033378 T3 ES 2033378T3 ES 198888111205 T ES198888111205 T ES 198888111205T ES 88111205 T ES88111205 T ES 88111205T ES 2033378 T3 ES2033378 T3 ES 2033378T3
Authority
ES
Spain
Prior art keywords
weight
methyl esters
mixtures
fatty acid
acid methyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES198888111205T
Other languages
English (en)
Inventor
Theo Dr. Fleckenstein
Joachim Dr. Pohl
Franz-Josef Dr. Carduck
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Application granted granted Critical
Publication of ES2033378T3 publication Critical patent/ES2033378T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/02—Monohydroxylic acyclic alcohols
    • C07C31/125—Monohydroxylic acyclic alcohols containing five to twenty-two carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
    • C07C29/149—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof with hydrogen or hydrogen-containing gases
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Fats And Perfumes (AREA)

Abstract

EN UNA HIDROGENACION CATALITICA DE MEZCLAS DE ESTERES METILICOS DE ACIDOS GRASOS, LOS ESTERES METILICOS SE TRANSFORMAN CON HIDROGENO, A UNA PRESION ENTRE 100 Y 300 BAR, A UNA TEMPERATURA ENTRE 160 Y 270 C, CON RELACION MOLAR DE HIDROGENO / MEZCLA DE ESTER METILICO DE 10:1 A 500:1 Y EN PRESENCIA DE CATALIZADORES. EL CATALIZADOR CONTIENE DE 30 A 40% EN PESO DE COBRE, DE 23 A 30% EN PESO DE CROMO, DE 1 A 10% EN PESO DE SILICIO Y DE 1 A 7% EN PESO DE BARIO Y ADEMAS UN OXIDO DE METAL DE TRANSICION. PARA EL CALCINADO DE LOS COMPONENTES FORMADORES DE LA MASA DEL CATALIZADOR SE TRANSFORMAN CON 1 A 10% EN PESO DE UNOS LIGANTES Y CON UN 1 A 10% EN PESO DE GRAFITO RESPECTO A LA MASA DEL CATALIZADOR EN GRANOS Y / O TROZOS Y SE ACTIVAN CON HIDROGENO O MEZCLA DE GAS CONTENIENDO HIDROGENO.
ES198888111205T 1987-07-22 1988-07-13 Procedimiento para la hidrogenacion de mezclas de esteres metilicos de acidos grasos. Expired - Lifetime ES2033378T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19873724257 DE3724257A1 (de) 1987-07-22 1987-07-22 Verfahren zur hydrierung von fettsaeuremethylestergemischen

Publications (1)

Publication Number Publication Date
ES2033378T3 true ES2033378T3 (es) 1993-03-16

Family

ID=6332119

Family Applications (1)

Application Number Title Priority Date Filing Date
ES198888111205T Expired - Lifetime ES2033378T3 (es) 1987-07-22 1988-07-13 Procedimiento para la hidrogenacion de mezclas de esteres metilicos de acidos grasos.

Country Status (12)

Country Link
US (1) US5043485A (es)
EP (1) EP0300347B1 (es)
JP (1) JPS6447725A (es)
KR (1) KR890001921A (es)
AT (1) ATE78013T1 (es)
BR (1) BR8803656A (es)
DE (2) DE3724257A1 (es)
DK (1) DK414288A (es)
ES (1) ES2033378T3 (es)
GR (1) GR3005750T3 (es)
MY (1) MY103743A (es)
PH (1) PH25603A (es)

Families Citing this family (40)

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Publication number Priority date Publication date Assignee Title
DE3913387A1 (de) * 1989-04-24 1990-10-25 Henkel Kgaa Verfahren zur katalytischen hydrierung von fluessigen fettsaeure-methylestern
DE3942064A1 (de) * 1989-10-04 1991-04-11 Henkel Kgaa Verfahren zur herstellung von saeurefesten katalysatoren fuer die direkte hydrierung von carbonsaeuren zu alkoholen
DE4005629A1 (de) * 1990-02-22 1991-08-29 Henkel Kgaa Verfahren zum hydrieren
DE4028295A1 (de) * 1990-09-06 1992-03-12 Henkel Kgaa Cupfer-mangan-katalysatoren
MY107920A (en) * 1990-12-27 1996-06-29 Kao Corp Process for producing alcohol
US5409621A (en) * 1991-03-25 1995-04-25 Lever Brothers Company, Division Of Conopco, Inc. Fabric softening composition
US5243095A (en) * 1992-04-24 1993-09-07 Engelhard Corporation Hydrogenation catalyst, process for preparing and process for using said catalyst
DE4335781C2 (de) * 1993-10-20 1998-02-19 Henkel Kgaa Fettalkohole auf pflanzlicher Basis und Verfahren zu Ihrer Herstellung
US5475159A (en) * 1994-11-07 1995-12-12 Shell Oil Company Process for the direct hydrogenation of methyl esters
US5475160A (en) * 1994-11-07 1995-12-12 Shell Oil Company Process for the direct hydrogenation of triglycerides
US5463143A (en) * 1994-11-07 1995-10-31 Shell Oil Company Process for the direct hydrogenation of wax esters
US5536889A (en) * 1995-09-29 1996-07-16 Shell Oil Company Process for the two-stage hydrogenation of methyl esters
EP1566372B1 (en) * 2002-11-27 2018-01-10 New Japan Chemical Co., Ltd. Method of hydrogenation reaction
EP2292697A1 (en) 2005-01-10 2011-03-09 Elevance Renewable Sciences, Inc. Candle and candle wax containing metathesis and metathesis-like products
WO2007081987A2 (en) 2006-01-10 2007-07-19 Elevance Renewable Sciences, Inc. Method of making hydrogenated metathesis products
WO2007103460A2 (en) * 2006-03-07 2007-09-13 Elevance Renewable Sciences, Inc. Colorant compositions comprising metathesized unsaturated polyol esters
CN102525829B (zh) 2006-03-07 2014-08-06 埃莱文斯可更新科学公司 含有复分解不饱和多元醇酯的组合物
EP2046719B1 (en) * 2006-07-12 2013-09-04 Elevance Renewable Sciences, Inc. Ring opening cross-metathesis reaction of cyclic olefins with seed oils and the like
US8067610B2 (en) 2006-07-13 2011-11-29 Yann Schrodi Synthesis of terminal alkenes from internal alkenes and ethylene via olefin metathesis
EP2074079B1 (en) * 2006-10-13 2011-08-10 Elevance Renewable Sciences, Inc. Metathesis methods involving hydrogenation and compositions relating to same
CA2723568A1 (en) * 2008-05-06 2009-11-12 Archer Daniels Midland Company Lubricant additives
WO2010062932A1 (en) * 2008-11-26 2010-06-03 Elevance Renewable Sciences, Inc. Methods of producing jet fuel from natural oil feedstocks through oxygen-cleaved reactions
WO2010062958A1 (en) 2008-11-26 2010-06-03 Elevance Renewable Sciences, Inc. Methods of producing jet fuel from natural oil feedstocks through metathesis reactions
CA3035015C (en) * 2009-10-12 2021-03-16 Elevance Renewable Sciences, Inc. Methods of refining and producing fuel from natural oil feedstocks
US9175231B2 (en) 2009-10-12 2015-11-03 Elevance Renewable Sciences, Inc. Methods of refining natural oils and methods of producing fuel compositions
US9365487B2 (en) 2009-10-12 2016-06-14 Elevance Renewable Sciences, Inc. Methods of refining and producing dibasic esters and acids from natural oil feedstocks
US9382502B2 (en) 2009-10-12 2016-07-05 Elevance Renewable Sciences, Inc. Methods of refining and producing isomerized fatty acid esters and fatty acids from natural oil feedstocks
US9169447B2 (en) 2009-10-12 2015-10-27 Elevance Renewable Sciences, Inc. Methods of refining natural oils, and methods of producing fuel compositions
US9051519B2 (en) 2009-10-12 2015-06-09 Elevance Renewable Sciences, Inc. Diene-selective hydrogenation of metathesis derived olefins and unsaturated esters
US9000246B2 (en) 2009-10-12 2015-04-07 Elevance Renewable Sciences, Inc. Methods of refining and producing dibasic esters and acids from natural oil feedstocks
US9222056B2 (en) 2009-10-12 2015-12-29 Elevance Renewable Sciences, Inc. Methods of refining natural oils, and methods of producing fuel compositions
US8735640B2 (en) 2009-10-12 2014-05-27 Elevance Renewable Sciences, Inc. Methods of refining and producing fuel and specialty chemicals from natural oil feedstocks
WO2012074841A2 (en) * 2010-11-30 2012-06-07 Basf Corporation Copper chromite hydrogenation catalysts for production of fatty alcohols
US9169174B2 (en) 2011-12-22 2015-10-27 Elevance Renewable Sciences, Inc. Methods for suppressing isomerization of olefin metathesis products
US9139493B2 (en) 2011-12-22 2015-09-22 Elevance Renewable Sciences, Inc. Methods for suppressing isomerization of olefin metathesis products
US9133416B2 (en) 2011-12-22 2015-09-15 Elevance Renewable Sciences, Inc. Methods for suppressing isomerization of olefin metathesis products
US9388098B2 (en) 2012-10-09 2016-07-12 Elevance Renewable Sciences, Inc. Methods of making high-weight esters, acids, and derivatives thereof
CN103980090B (zh) * 2014-05-28 2016-03-16 灯塔北方化工有限公司 天然脂肪醇的生产方法
CN106622379A (zh) * 2016-12-20 2017-05-10 江苏金马油脂科技发展有限公司 一种脂肪酸甲酯加氢铜基催化剂的制备方法及应用
KR102354488B1 (ko) * 2020-07-31 2022-02-07 최성호 펠릿 숯 제조시스템

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3173959A (en) * 1965-03-16 Process for the production of saturated fatty alcohols
US2091800A (en) * 1931-09-15 1937-08-31 Rohm & Haas Method of hydrogenating esters
US2094127A (en) * 1932-01-02 1937-09-28 Du Pont Mixed higher alcohols
US2109844A (en) * 1932-02-27 1938-03-01 Du Pont Catalytic hydrogenation of glycerides of aliphatic carboxylic acids
US2080419A (en) * 1934-02-16 1937-05-18 Green Stanley Joseph Process for producing higher fatty alcohols
DE965236C (de) * 1955-08-22 1957-06-06 Dehydag Gmbh Verfahren zur kontinuierlichen Herstellung einfach ungesaettigter, hoehermolekularerFettalkohole
FR1276722A (fr) * 1960-10-11 1961-11-24 Eastman Kodak Co Procédé de préparation d'un catalyseur en vue de la réduction des esters en alcools
US3180898A (en) * 1961-04-17 1965-04-27 Metallgesellschaft Ag Process for the production of fatty alcohols by catalytic hydrogenation of fatty acids and their derivatives
DE2513377C3 (de) * 1975-03-26 1985-08-29 Henkel KGaA, 4000 Düsseldorf Verfahren zur Herstellung einfach ungesättigter höhermolekularer Fettalkohole
DE2613226B2 (de) * 1976-03-27 1978-12-14 Henkel Kgaa, 4000 Duesseldorf Verfahren zur kontinuierlichen Herstellung von Fettalkoholen
US4113662A (en) * 1976-08-05 1978-09-12 Chevron Research Company Catalyst for ester hydrogenation
US4199479A (en) * 1978-02-24 1980-04-22 Chevron Research Company Hydrogenation catalyst
DE3146493A1 (de) * 1981-11-24 1983-06-01 Chemische Werke Hüls AG, 4370 Marl Verfahren zur herstellung von reinem neohexanol
DE3221307A1 (de) * 1982-06-05 1983-12-08 Metallgesellschaft Ag, 6000 Frankfurt Verfahren zur abtrennung und reinigung von katalysatoren
GB8310797D0 (en) * 1983-04-21 1983-05-25 British Petroleum Co Plc Vapour phase hydrogenation of esters
US4652685A (en) * 1985-11-15 1987-03-24 General Electric Company Hydrogenation of lactones to glycols
EP0254189B1 (de) * 1986-07-23 1992-03-04 Henkel Kommanditgesellschaft auf Aktien Verfahren zur Direkthydrierung von Glyceridölen

Also Published As

Publication number Publication date
EP0300347B1 (de) 1992-07-08
JPS6447725A (en) 1989-02-22
EP0300347A3 (en) 1989-07-05
PH25603A (en) 1991-08-08
DE3724257A1 (de) 1989-02-02
US5043485A (en) 1991-08-27
KR890001921A (ko) 1989-04-06
DE3872616D1 (de) 1992-08-13
DK414288A (da) 1989-01-23
ATE78013T1 (de) 1992-07-15
GR3005750T3 (es) 1993-06-07
MY103743A (en) 1993-09-30
EP0300347A2 (de) 1989-01-25
BR8803656A (pt) 1989-02-14
DK414288D0 (da) 1988-07-22

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