EP2457629A1 - Evaporation device - Google Patents
Evaporation device Download PDFInfo
- Publication number
- EP2457629A1 EP2457629A1 EP20110188935 EP11188935A EP2457629A1 EP 2457629 A1 EP2457629 A1 EP 2457629A1 EP 20110188935 EP20110188935 EP 20110188935 EP 11188935 A EP11188935 A EP 11188935A EP 2457629 A1 EP2457629 A1 EP 2457629A1
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- EP
- European Patent Office
- Prior art keywords
- liquid
- capillary
- wetting
- porous
- component
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
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- 230000008020 evaporation Effects 0.000 title description 21
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- 238000010438 heat treatment Methods 0.000 claims abstract description 59
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- 230000004858 capillary barrier Effects 0.000 claims abstract description 37
- 238000005086 pumping Methods 0.000 claims abstract description 33
- 238000009834 vaporization Methods 0.000 claims abstract description 26
- 238000009736 wetting Methods 0.000 claims description 100
- 239000000463 material Substances 0.000 claims description 21
- 239000002245 particle Substances 0.000 claims description 14
- 239000007921 spray Substances 0.000 claims description 7
- 238000005507 spraying Methods 0.000 claims description 7
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Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01B—BOILING; BOILING APPARATUS ; EVAPORATION; EVAPORATION APPARATUS
- B01B1/00—Boiling; Boiling apparatus for physical or chemical purposes ; Evaporation in general
- B01B1/005—Evaporation for physical or chemical purposes; Evaporation apparatus therefor, e.g. evaporation of liquids for gas phase reactions
Definitions
- the present invention relates to an evaporation device comprising an improved capillary pump for the production of steam for a variety of applications and, more particularly, a device for the vaporization of a liquid, comprising a reservoir capable of containing a liquid to vaporizing, a heating element capable of heating liquid in order to vaporize it, and a capillary pump capable of pumping liquid contained in said reservoir towards said heating element by capillary pumping.
- International demand WO 2005/049185 describes such a vaporization device comprising a capillary pump for producing and emitting pressurized and non-pressurized steam from a liquid to be vaporized.
- international demand WO 2005/049185 discloses a device using a capillary pump having for capillary pumping a wetting porous medium for passively pumping a liquid to be vaporized from a reservoir to a heating or heated element.
- this device comprises a liquid inlet to vaporize, a porous vaporization element and an element for thermal transfer.
- an insulating element such as an insulating element, an element for preheating the liquid to be sprayed, a liquid supply tank and / or a supply system, an integrated or associated heating element, a storage chamber for steam, a heat distributor, an orifice and / or a steam emission element, can also be associated or integrated with this device.
- the vaporization devices comprising a capillary pump according to the prior art have numerous drawbacks.
- the capillary pumping carried out by the capillary pump provided in the device according to the international application WO 2005/049185 is independent of the orientation of said device, a leak will take place and the liquid contained in the tank will flow in the case where the device is used upside down, that is to say with the supply tank in liquid flipped over the capillary pump.
- Such leakage will occur because the wetting porous medium performing said capillary pump may limit flow rate, but it can not stop it.
- the purpose of the present invention is therefore to overcome these disadvantages by providing a device for the vaporization of a liquid comprising a capillary pump capable of operating without leakage regardless of the orientation of the pump while consuming a minimum electrical power during its operation.
- the devices for vaporizing a liquid according to the present invention are provided for the emission of vapor produced from a liquid to be vaporized.
- a liquid to be vaporized generally having a first temperature and being provided in a low pressure liquid supply tank, is sucked by a capillary pump through capillary forces.
- the liquid thus sucked is transported to an area of the device serving as a vaporizer.
- This zone is provided with a capillary barrier, impervious to the liquid and permeable to vapor, thus defining a liquid / vapor or liquid / gas interface.
- the liquid migrating to this interface is heated to a second temperature, higher than the first temperature and vaporizes.
- the capillary barrier impervious to liquid and permeable to the vapor allows the expulsion of the latter from the device.
- the devices for vaporizing a liquid to be vaporized comprise a reservoir capable of containing a liquid to be vaporized, a heating element capable of heating liquid in order to vaporize it, a capillary pump capable of pumping liquid. contained in said reservoir to said heating element by capillary pumping, and a capillary barrier disposed in a direction of capillary pumping of the liquid to be vaporized downstream of the capillary pump, said capillary barrier being able to prevent non-vaporized liquid from escaping of the device.
- the present invention thus makes it possible to propose compact devices, allowing a strong integration, and preventing leakage of liquid regardless of the orientation of the devices when in use.
- said capillary barrier comprises at least one non-wetting porous component.
- the at least one non-wetting porous component is preferably impervious to said vapor permeable liquid generated from said liquid to be vaporized.
- a desired seal of the devices according to the present invention can be achieved by using a simple and inexpensive component.
- Said at least one non-wetting porous component preferably comprises a membrane of polymeric material.
- said at least one non-wetting porous component is comparatively little heat conductor required for the vaporization of said liquid to be vaporized.
- said at least one porous non-wetting component is adapted to withstand temperatures higher than the vaporization temperature of the liquid, for example 100 Ā° C for water at atmospheric pressure, and / or comprises a thermally insulating material.
- the present invention thus provides the capillary barrier close to the heating element, allowing a strong integration of the device for the vaporization of a liquid to vaporize and the provision of a compact device, resistant and solid.
- Said capillary barrier is preferably arranged in a removable manner.
- the capillary barrier can be exchanged or cleaned easily and quickly thus allowing improved healthiness of the device.
- the capillary barrier may be located inside the system. analysis and in contact with the air to be treated, while being exchangeable between two successive analyzes thanks to its removability.
- the risk of a contamination of the analysis system that could distort the results obtained can easily and effectively be ruled out.
- said reservoir, said capillary pump and said capillary barrier are provided in the form of stacked disks.
- at least said capillary pump may be provided in cylindrical form and said capillary barrier in annular form, said capillary barrier surrounding said capillary pump at least partially.
- Said tank, said capillary pump and said capillary barrier are preferably arranged in an external support.
- Said outer support preferably comprises glass, ceramic and / or plastic adapted to withstand the heat required for the vaporization of said liquid to be vaporized.
- such materials have a low thermal conductivity, which minimizes thermal energy losses: the energy consumption of the device is then minimized.
- an inexpensive external support can be proposed, adapted to maintain the constituent components of the device for the vaporization of a liquid to be vaporized according to the present invention in a predefined structure in a safe and solid manner.
- said heating element comprises at least one stainless material.
- said heating element is disposed in a capillary pumping direction of said liquid to be vaporized between said capillary pump and said capillary barrier.
- said heating element may be disposed in a capillary pumping direction of said liquid to be vaporized downstream of said capillary barrier.
- the present invention thus provides a reliable heating element at a location of the device for the vaporization of a liquid to vaporize, in the vicinity of which the vaporization of the liquid will take place.
- the heat required for the vaporization can be produced exactly at the point of vaporization, thus allowing a minimized consumption of electrical power by the heating element and, therefore, by the device during its operation.
- Said heating element is preferably provided in the form of an electrically conductive grid.
- said capillary pump comprises at least one porous wetting component permeable to said liquid to be vaporized.
- the porosity of said at least one non-wetting porous component may be greater than the porosity of said at least one porous wetting component. This allows easy evacuation of steam. But the porosity of said at least one non-wetting porous component may also be lower than the porosity of said at least one porous wetting component. This will be particularly the case if it is desired that the non-wetting porous component constitutes a barrier preventing pollution of the device by the external environment, for example a bacteriological pollution.
- the at least one porous wetting component may be provided with a porosity gradient, or comprise at least a first porous component and a second porous component, the porosity of said first porous component being greater than the porosity of said second porous component. It is known that a decreasing porosity gradient, obtained by a reduction of the pore diameters, according to the pumping direction of the liquid, increases the pumping pressure.
- devices for spraying a liquid spray according to the present invention can vaporize any type of liquid, provided that it can be vaporized under appropriate conditions, for example a required heat of vaporization and an associated boiling point.
- Sprayable liquids may include water, ethanol, perfume compounds, crop treatments, insect repellants and / or attractants, antiseptics, inhalants, and other medical compositions, as well as other liquids for which the Spraying is desirable and / or necessary in order, for example, to accurately measure a vapor such as in a process of producing or depositing a chemical vapor.
- the advantages of using devices for spraying a liquid spray according to the present invention for vaporizing liquids are that the steam can be produced from the top to the bottom of the device and driven by the airflow.
- the reservoir containing the liquid can be located above an associated evaporation zone, so that the hydrostatic pressure is substituted for the mechanical pumps and pressurization systems.
- the wetting porous components provide uniform supply of the heating element if the device is inclined.
- the outer body of the device is of simple geometry so that it is easy to clean.
- An exemplary embodiment and application of a device for vaporizing a liquid to be vaporized according to the present invention as described above is a counter and / or collector of particles included in a gas to be treated, such as air, for example a meter and / or particle collector by semi-wet electrostatic collection.
- a gas to be treated such as air
- the air to be treated is sometimes enriched, or even saturated, with steam so as to cause a magnification of the particles by nucleation, either for meters for counting by optical means, or for collectors for collection purposes.
- the present invention can be integrated in such devices and improve them by its advantages on the devices of the state of the prior art.
- An electrostatic collecting device is for example described in the application WO 2007/012447 .
- the generator The steam according to the invention can be used as a means for producing steam from such an electrostatic collector.
- the use of the device for the vaporization of a liquid to be sprayed according to the present invention for the production of a counter and / or particle collector has only been described for illustration without limiting the device to such use.
- a use of the device in many different applications is conceivable, such as for example a use for the production of an apparatus for treatment of the respiratory tract with humidified air.
- the figure 1 shows a counter and / or particle collector by semi-wet electrostatic collection 150 comprising a device for the vaporization of a liquid spray 100 according to a first embodiment of the present invention.
- An exemplary configuration of a counter and / or particle collector by semi-wet electrostatic collection is described in the international application WO 2007/012447 , the content of which is explicitly referred to and considered to be an integral part of this application.
- the meter and / or collector 150 is different from the meter and / or collector of the international application WO 2007/012447 essentially by the constitution of its device for the vaporization of a liquid spray 100. Thus, thereafter only the device 100 is described in greater detail, for the sake of brevity and simplicity of the description.
- the device for vaporizing a liquid to be vaporized 100 comprises, by way of example, a configuration in the form of stacked disks. During operation of the device 100, a liquid is sucked by one or more capillary pumping layers and then vaporized. The vapor produced is expelled or emitted under pressurized or essentially non-pressurized conditions and can be used directly.
- the device 100 is hereinafter also designated as "evaporation device".
- the evaporation device 100 comprises for the illustration a reservoir 101 capable of containing a liquid to be vaporized 111, a heating element 105 capable of heating liquid in order to vaporize it, a capillary pump 110 capable of pumping liquid contained in the reservoir 101 to the heating element 105 by capillary pumping, and a capillary barrier 106 disposed in a capillary pumping direction 102 of the liquid to be vaporized 111 downstream of the capillary pump 110.
- the capillary barrier 106 is capable of preventing non-vaporized liquid from escaping from the device 100 and preferably comprises at least one non-wetting porous component 116.
- the capillary pump 110 is permeable to the liquid to be vaporized 111 and has at least one wetting porous component 103, 104.
- the pore diameter of this wetting porous component 103, 104 may be larger than the pore diameter of the non-wetting porous component.
- the capillary pump 110 comprises a first porous component 103 and a second porous component 104.
- the porosity of the first porous component 103 is greater than the porosity of the second porous component 104.
- the pores of the second Wet porous component 104 is preferably much smaller than that of the first wetting porous component 103.
- the first porous wetting component 103 is preferably thick with respect to the second wetting porous component 104 to provide good thermal insulation between the heating element 105. and the reservoir 101 of the liquid to be vaporized 111.
- the pumping function of the liquid 111 can be ensured by capillarity p provided that the capillaries or pores of the porous wetting components 103, 104 are of a sufficiently small diameter, preferably less than a millimeter, of a few tenths of a micron to a few hundred microns.
- the first wetting porous component 103 is provided with a porosity of a few tens of microns or even hundreds of microns and the second porous wetting component 104 is provided with a porosity of a few tenths of a micron to a few microns.
- the second wetting porous component 104 is purely optional.
- the evaporation device 100 can therefore be produced according to an embodiment of the present invention without the second wetting porous component 104.
- the first wetting porous component 103 constitutes, for example, in itself only the capillary pump 110 according to the invention. the present invention and is then preferably provided with a porosity gradient.
- the first wetting porous component 103 and the second wetting porous component 104 provide a capillary pumping of the spraying liquid 111 from the reservoir 101.
- a liquid path is established in the direction of the arrow 102, and a heat circulation path is established in the zone comprising the heating element 105.
- the evaporation device 100 operates passively with respect to capillary pumping and without any leakage regardless of its orientation in use.
- a wetting porous medium can not stop the flow of a liquid.
- the evaporation device 100 is turned over, the liquid reservoir 101 then being above the wetting porous components 103, 104, the tank 101 would be emptied drop by drop.
- the wetting porous components 103, 104 would only serve to limit the flow rate by introducing a high pressure drop.
- the evaporation device 100 according to the present invention comprises the non-wetting porous component 116.
- This non-wetting porous component 116 is impervious to said vapor-permeable liquid 111 generated from said liquid to be vaporized. 111. In this configuration, a liquid / vapor or liquid / air interface is blocked at the interface between the two wetting porous media 103, 104 and non-wetting 116.
- a material is said to be "wetting" when a drop placed on it leads to a contact angle of the triple line less than 90 Ā° according to a commonly accepted definition.
- a wetting and porous material is permeable to a liquid, for example the spraying liquid 111.
- the term āhydrophilicā is reserved for wetting materials with respect to water.
- a material is said to be ānon-wettingā when a drop placed on it leads to a contact angle of the triple line greater than 90 Ā°.
- a non-wetting material is generally impermeable (or poorly permeable) to a liquid, for example the spraying liquid 111, and may be vapor permeable if porous.
- hydrophobic is reserved for non-wetting materials with respect to water.
- the non-wetting porous component 116 comprises a membrane made of a polymer material, such as, for example, Teflon.
- the non-wetting porous component 116 is comparatively little heat conductor required for the vaporization of said liquid spray 111 and adapted to withstand the vaporization temperatures, for example 100 Ā° C for water.
- the non-wetting porous component 116 may comprise a thermally insulating material.
- the heating element 105 Located between the first wetting porous component 103 and the nonwetting porous component 116, the heating element 105 directly heats the liquid / vapor or liquid / air interface.
- the liquid / vapor interface is not necessarily located at the level of the heating element, but can move in the porous medium 103, 104 to the tank 101.
- the heating element 105 located at this interface or in the immediate vicinity of this interface, can vaporize the pumped liquid to this interface.
- This heating element 105 is advantageously a grid, electrically conductive and preferably made of a stainless material.
- the heating element 105 may be provided with and electrically connected to a power source (not shown).
- the heating element 105 may for example consist of a grid consisting of stainless steel son diameter 100 microns, the distance between each wire being of the order of magnitude of the diameter, powered by a voltage of a few volts.
- a heating element that can be heated by electrical energy can be used to provide the heating element 105 to provide the thermal energy required for vaporization.
- Heating elements based on electrical resistors or having a thermistor or other resistive heating material suitable and suitable for heating, when traversed by an electric current, may be used.
- the resistive heating material may be designed as a wire, a porous material, a perforated plate or a disc, or may be deposited as a thin or thick film.
- it is incorporated so that the vapor permeability at the vapor emission surface of the vaporizer component, i.e., non-wetting porous component 116, is substantially maintained.
- the heat can be applied directly to the surface of the non-wetting porous component 116 by means of a resistive heating material in direct contact with or deposited directly on the porous non-wetting component 116.
- the constituent components of the evaporation device 100 described above are sufficiently aligned to produce and maintain the liquid flow pathways so that liquid and vapor can travel in or on associated surfaces of different components by capillary pumping.
- the various wetting porous components 103, 104 constituting the pump are in contact with each other, and are also in contact with the tank 101. In some embodiments, each of the surfaces of the various components comes into close contact with one another. adjacent surface substantially without gaps or voids.
- the relative thickness, or the volume, of the different components depends on the function that the component provides and the application for capillary pumping.
- the components constituting the evaporation device 100 according to the present invention described above may be selected from different materials.
- the wetting porous components 103, 104 are preferably made using materials with low heat conductivity such as, for example, a glass sinter, glass beads, glass fibers, sintered or porous stainless steel.
- Other exemplary porous materials that may be used include porous ceramic, such as alumina grinding material (as provided, for example, by Abrasives Unlimited Inc., San Leandro, Calif.).
- Other types of absorbents and / or porous materials including cotton, fiberglass (such as EI Dupont de Nemours & Co., Nomextm, Wilmington, Delaware) and the like, known to those skilled in the art, can alternatively be used. These materials have a maximum thermal conductivity of about 0.03 to 3 W / m-K.
- the figure 2 shows a sectional view of a second embodiment of the invention of an evaporation device 200.
- the evaporation device 200 is essentially identical to that described in FIG. figure 1 and comprises a reservoir 201 capable of containing a vaporizing liquid 211, a capillary pump 210 having a first porous wetting component 203 and a second wetting porous component 204, a heating element 206 and a capillary barrier 205 having a porous non-wetting component 215.
- a capillary pumping associated up to the capillary barrier 205 is designated by an arrow 202.
- the difference between the device 200 and the device 100 of the figure 1 consists in arranging the non-wetting porous component 215 below the heating element 206.
- the non-wetting porous component 215 is positioned just above the second wetting porous component 204 and between the latter and the element heating 206.
- the arrangement according to the figure 2 allows the heating element 206 to be used to mechanically maintain the various layers of the evaporation device 200 in the form of disks, established by the various constituent components of the device 200, between them.
- the heating element 206 mechanically holds the reservoir 201, the first wetting porous component 203, the second wetting porous component 204 and the non-wetting porous component 205.
- the figure 3 shows a sectional view of an evaporation device 300 according to a third embodiment of the present invention.
- the device 300 consists of an assembly of materials in the form of stacked disks, as illustrated in FIG. figure 1 , and comprises for example a reservoir 301 capable of containing a liquid to vaporize 311.
- the reservoir 301 is arranged adjacent to a capillary pump 310 having a first wetting and thermally insulating porous medium 304 itself arranged by adjacent to a second wetting and thermally insulating porous medium 305.
- the capillary pump 310 is arranged below a heating element 307 which is covered by a non-wetting porous component 316 forming a capillary barrier 306. Pumping associated capillary to the capillary barrier 306 is designated by an arrow 302.
- the assembly is held by a support 308.
- the latter comprises an annular upper support 309 (illustrated in FIG. figure 3 on the right and left sides of the device 300 above the porous non-wetting component 316) and an annular lower support 303 (illustrated at the bottom of the figure 3 between the reservoir 301 and the first wetting porous component 304).
- the figure 4 shows a sectional view of an evaporation device 400 according to a fourth embodiment of the present invention.
- the device 400 consists of an assembly of materials and components in a cylindrical geometry and comprises by way of example a reservoir 401 capable of containing a liquid to be sprayed 411, a capillary pump 410 with a first wetting and thermally insulating porous component 403 and a second wetting and thermally insulating porous component 407, a heating element 408 and a capillary barrier 409, which includes, by way of example, a non-wetting porous component 419.
- Associated capillary pumping to the capillary barrier 409 is designated by arrows 402 and 406.
- the first wetting porous component 403 has a cylindrical shape and is held with the cylindrical reservoir 401 by an annular support 404, and a disc-shaped support 405.
- the reservoir 401 is held by the support 404, which has an annular configuration and illustratively surrounds the end of the reservoir 401.
- the first wetting porous component 403 is covered by the disc-shaped support 405.
- first wetting porous component 403 is surrounded by the second wetting porous component 407 having as an example a tube shape and also held by the support 404, 405.
- the second wetting porous component 407 is surrounded by the element 408, provided in the form of a spiral and which can serve to maintain the arrangement of the figure 4 in a cylindrical geometry.
- the heating element 408 is surrounded by the non-wetting porous component 419 in the form of a tube.
- the figure 5 shows a sectional view of a particle analysis system 550 having an evaporation device 500 according to a fifth embodiment of the present invention.
- the device 500 consists of an assembly of materials in the form of stacked disks, as illustrated in FIG. figure 3 but in comparison with it, turned upside down.
- the device 500 comprises, by way of example, a tank 501 capable of containing a liquid to be vaporized 521, the tank 501 being arranged in the figure 5 above a first wetting and thermally insulating porous component 504, which is itself arranged in the figure 5 on top of a second porous wetting and thermally insulating component 505.
- the two wetting porous components 504, 505 provide for illustration a capillary pump 520, arranged in the figure 5 above a heating element 506 preferably provided in the form of a grid.
- first annular lower support 509 and a second annular lower support 507 in the form of a flange illustrated in FIG. figure 5 on the right and left sides of the device 500 below the heating element 506)
- annular medium support 503 illustrated in the middle of the figure 5 between the reservoir 501 and the first wetting porous component 504
- annular upper support 512 having an orifice 511 and being placed or fixed on the device 500 as a cover.
- the second symmetrical lower support 507 is provided to hold the reservoir 501, the first and second wetting porous components 504, 505 and the heating element 506 in the form of stacked disks, as illustrated in FIG. figure 3 . Between this second symmetrical lower support 507 and the first symmetrical lower support 509 is provided a removable non-wetting porous component 518 producing a capillary barrier 508.
- a capillary pumping associated up to the capillary barrier 508 is designated by an arrow 502.
- the first symmetrical lower support 509 is removable and allows quick and easy replacement and / or cleaning of the removable non-wetting porous component 518, while the other components are maintained during these replacement operations and / or cleaning the component 518 by the second symmetrical lower support 507.
- the non-wetting porous component 518 is located inside the analysis system 550 is in contact with the air to be treated.
- the porous non-wetting component 518 is changeable and / or cleanable between two analyzes.
- the invention may for example be achieved by stacking various components, described above with reference to the figure 1 in a support that is both thermally and electrically insulating and capable of withstanding a temperature of use greater than 100 Ā° C.
- a support comprising polycarbonate can be made, resistant to operating temperatures up to approximately 130 Ā° C max.
- the first wetting porous component 103 consists of a glass frit 1 mm thick and with a porosity of about 100 to 200 ā m.
- the second wetting porous component 104 consists of a 260 ā m thick fiberglass filtration membrane having a filtration threshold of 1.6 ā m.
- the heating element 105 is a wire cloth made of stainless steel wires 97 ā m in diameter, and spaced a distance close to this diameter. These stainless steel son are traversed by an electric current and thus constitute the heating element 105.
- the non-wetting porous component 116 consists of a teflon filtration membrane having a filtration threshold of 20 .mu.m.
- the membranes used may be, for example, commercially available filters. Their diameters are commonly 25, 47 or 90 mm. The diameter of the evaporation devices is generally between 3 and 20 cm, and their height is between 2 and 20 cm.
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
La prĆ©sente invention concerne un dispositif (100) pour la vaporisation d'un liquide, ledit dispositif (100) comportant: un rĆ©servoir (101) susceptible de contenir un liquide Ć vaporiser (111), un Ć©lĆ©ment chauffant (105) susceptible de chauffer du liquide afin de le vaporiser, une pompe capillaire (110) susceptible de pomper du liquide contenu dans ledit rĆ©servoir (101) vers ledit Ć©lĆ©ment chauffant (105) par pompage capillaire, et une barriĆØre capillaire (106) disposĆ©e dans une direction (102) de pompage capillaire du liquide Ć vaporiser (111) en aval de la pompe capillaire (110), ladite barriĆØre capillaire (106) Ć©tant susceptible d'empĆŖcher du liquide non vaporisĆ© de s'Ć©chapper du dispositif (100).The present invention relates to a device (100) for the vaporization of a liquid, said device (100) comprising: a reservoir (101) capable of containing a liquid to be vaporized (111), a heating element (105) capable of heating the liquid, liquid for vaporizing it, a capillary pump (110) capable of pumping liquid contained in said reservoir (101) to said heating element (105) by capillary pumping, and a capillary barrier (106) disposed in a direction (102) of capillary pumping of the liquid to be vaporized (111) downstream of the capillary pump (110), said capillary barrier (106) being able to prevent non-vaporized liquid from escaping from the device (100).
Description
La prĆ©sente invention concerne un dispositif d'Ć©vaporation comportant une pompe capillaire amĆ©liorĆ©e pour la production de vapeur destinĆ©e Ć une variĆ©tĆ© d'applications et, plus particuliĆØrement, un dispositif pour la vaporisation d'un liquide, comportant un rĆ©servoir susceptible de contenir un liquide Ć vaporiser, un Ć©lĆ©ment chauffant susceptible de chauffer du liquide afin de le vaporiser, et une pompe capillaire susceptible de pomper du liquide contenu dans ledit rĆ©servoir vers ledit Ć©lĆ©ment chauffant par pompage capillaire.The present invention relates to an evaporation device comprising an improved capillary pump for the production of steam for a variety of applications and, more particularly, a device for the vaporization of a liquid, comprising a reservoir capable of containing a liquid to vaporizing, a heating element capable of heating liquid in order to vaporize it, and a capillary pump capable of pumping liquid contained in said reservoir towards said heating element by capillary pumping.
La demande internationale
D'autres Ć©lĆ©ments tels qu'un Ć©lĆ©ment isolant, un Ć©lĆ©ment permettant le prĆ©chauffage du liquide Ć vaporiser, un rĆ©servoir d'alimentation en liquide et/ou un systĆØme d'alimentation, un Ć©lĆ©ment chauffant intĆ©grĆ© ou associĆ©, une chambre d'accumulation de vapeur, un rĆ©partiteur de chaleur, un orifice et/ou un Ć©lĆ©ment d'Ć©mission de vapeur, peuvent aussi ĆŖtre associĆ©s ou intĆ©grĆ©s Ć ce dispositif.Other elements such as an insulating element, an element for preheating the liquid to be sprayed, a liquid supply tank and / or a supply system, an integrated or associated heating element, a storage chamber for steam, a heat distributor, an orifice and / or a steam emission element, can also be associated or integrated with this device.
NĆ©anmoins les dispositifs de vaporisation comportant une pompe capillaire selon l'art antĆ©rieur prĆ©sentent de nombreux inconvĆ©nients. Par exemple, mĆŖme si le pompage capillaire effectuĆ© par la pompe capillaire prĆ©vu dans le dispositif selon la demande internationale
Le but de la prĆ©sente invention est donc de remĆ©dier Ć ces inconvĆ©nients en proposant un dispositif pour la vaporisation d'un liquide comportant une pompe capillaire susceptible de fonctionner sans fuite quelque soit l'orientation de la pompe tout en consommant une puissance Ć©lectrique minimisĆ©e lors de son fonctionnement.The purpose of the present invention is therefore to overcome these disadvantages by providing a device for the vaporization of a liquid comprising a capillary pump capable of operating without leakage regardless of the orientation of the pump while consuming a minimum electrical power during its operation.
Les dispositifs pour la vaporisation d'un liquide selon la prĆ©sente invention sont prĆ©vus pour l'Ć©mission de vapeur produite Ć partir d'un liquide Ć vaporiser. Lors du fonctionnement d'un tel dispositif, un liquide Ć vaporiser, ayant gĆ©nĆ©ralement une premiĆØre tempĆ©rature et Ć©tant prĆ©vu dans un rĆ©servoir d'alimentation en liquide de basse pression, est aspirĆ© par une pompe capillaire par le biais de forces capillaires. Le liquide ainsi aspirĆ© est transportĆ© vers une zone du dispositif servant de vaporisateur. Cette zone est pourvue d'une barriĆØre capillaire, impermĆ©able au liquide et permĆ©able Ć la vapeur, dĆ©finissant alors une interface liquide/vapeur ou liquide/gaz. Le liquide migrant vers cette interface est chauffĆ© Ć une deuxiĆØme tempĆ©rature, plus Ć©levĆ©e que la premiĆØre tempĆ©rature et se vaporise. La barriĆØre capillaire impermĆ©able au liquide et permĆ©able Ć la vapeur permet l'expulsion de cette derniĆØre du dispositif.The devices for vaporizing a liquid according to the present invention are provided for the emission of vapor produced from a liquid to be vaporized. In operation of such a device, a liquid to be vaporized, generally having a first temperature and being provided in a low pressure liquid supply tank, is sucked by a capillary pump through capillary forces. The liquid thus sucked is transported to an area of the device serving as a vaporizer. This zone is provided with a capillary barrier, impervious to the liquid and permeable to vapor, thus defining a liquid / vapor or liquid / gas interface. The liquid migrating to this interface is heated to a second temperature, higher than the first temperature and vaporizes. The capillary barrier impervious to liquid and permeable to the vapor allows the expulsion of the latter from the device.
Plus particuliĆØrement, les dispositifs pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention comportent un rĆ©servoir susceptible de contenir un liquide Ć vaporiser, un Ć©lĆ©ment chauffant susceptible de chauffer du liquide afin de le vaporiser, une pompe capillaire susceptible de pomper du liquide contenu dans ledit rĆ©servoir vers ledit Ć©lĆ©ment chauffant par pompage capillaire, et une barriĆØre capillaire disposĆ©e selon une direction de pompage capillaire du liquide Ć vaporiser en aval de la pompe capillaire, ladite barriĆØre capillaire Ć©tant susceptible d'empĆŖcher du liquide non vaporisĆ© de s'Ć©chapper du dispositif.More particularly, the devices for vaporizing a liquid to be vaporized according to the present invention comprise a reservoir capable of containing a liquid to be vaporized, a heating element capable of heating liquid in order to vaporize it, a capillary pump capable of pumping liquid. contained in said reservoir to said heating element by capillary pumping, and a capillary barrier disposed in a direction of capillary pumping of the liquid to be vaporized downstream of the capillary pump, said capillary barrier being able to prevent non-vaporized liquid from escaping of the device.
La prĆ©sente invention permet ainsi de proposer des dispositifs compacts, permettant une forte intĆ©gration, et empĆŖchant toute fuite de liquide indĆ©pendamment de l'orientation des dispositifs lors de leur utilisation.The present invention thus makes it possible to propose compact devices, allowing a strong integration, and preventing leakage of liquid regardless of the orientation of the devices when in use.
Selon un mode d'exĆ©cution, ladite barriĆØre capillaire comporte au moins un composant poreux non mouillant. Ledit au moins un composant poreux non mouillant est prĆ©fĆ©rablement impermĆ©able au dit liquide Ć vaporiser et permĆ©able Ć la vapeur gĆ©nĆ©rĆ©e Ć partir dudit liquide Ć vaporiser.According to one embodiment, said capillary barrier comprises at least one non-wetting porous component. The at least one non-wetting porous component is preferably impervious to said vapor permeable liquid generated from said liquid to be vaporized.
Ainsi, une Ć©tanchĆ©itĆ© dĆ©sirĆ©e des dispositifs selon la prĆ©sente invention peut ĆŖtre obtenue en utilisant un composant simple et peu onĆ©reux.Thus, a desired seal of the devices according to the present invention can be achieved by using a simple and inexpensive component.
Ledit au moins un composant poreux non mouillant comporte prĆ©fĆ©rablement une membrane en matĆ©riau polymĆØre.Said at least one non-wetting porous component preferably comprises a membrane of polymeric material.
Ainsi, un composant poreux non mouillant robuste et fiable peut ĆŖtre proposĆ©.Thus, a robust and reliable non-wetting porous component can be provided.
Selon un mode d'exĆ©cution, ledit au moins un composant poreux non mouillant est comparativement peu conducteur de chaleur requise pour la vaporisation dudit liquide Ć vaporiser. De prĆ©fĆ©rence, ledit au moins un composant poreux non mouillant est adaptĆ© Ć rĆ©sister aux tempĆ©ratures supĆ©rieures Ć la tempĆ©rature de vaporisation du liquide , par exemple 100Ā°C pour l'eau Ć la pression atmosphĆ©rique, et/ou comporte un matĆ©riau thermiquement isolant.According to one embodiment, said at least one non-wetting porous component is comparatively little heat conductor required for the vaporization of said liquid to be vaporized. Preferably, said at least one porous non-wetting component is adapted to withstand temperatures higher than the vaporization temperature of the liquid, for example 100 Ā° C for water at atmospheric pressure, and / or comprises a thermally insulating material.
La prĆ©sente invention permet ainsi de disposer la barriĆØre capillaire proche de l'Ć©lĆ©ment chauffant, permettant alors une forte intĆ©gration du dispositif pour la vaporisation d'un liquide Ć vaporiser et la mise Ć disposition d'un dispositif compact, rĆ©sistant et solide.The present invention thus provides the capillary barrier close to the heating element, allowing a strong integration of the device for the vaporization of a liquid to vaporize and the provision of a compact device, resistant and solid.
Ladite barriĆØre capillaire est prĆ©fĆ©rablement disposĆ©e de maniĆØre amovible.Said capillary barrier is preferably arranged in a removable manner.
Ainsi, la barriĆØre capillaire peut ĆŖtre Ć©changĆ©e ou nettoyĆ©e facilement et rapidement permettant alors une salubritĆ© amĆ©liorĆ©e du dispositif. Plus en dĆ©tail, lors d'une utilisation du dispositif pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention par exemple dans un systĆØme d'analyse d'air, la barriĆØre capillaire peut ĆŖtre situĆ©e Ć l'intĆ©rieur du systĆØme d'analyse et au contact de l'air Ć traiter, tout en Ć©tant Ć©changeable entre deux analyses successives grĆ¢ce Ć son amovibilitĆ©. Ainsi, le risque d'une contamination du systĆØme d'analyse qui pourrait fausser des rĆ©sultats obtenus peut facilement et efficacement ĆŖtre Ć©cartĆ©.Thus, the capillary barrier can be exchanged or cleaned easily and quickly thus allowing improved healthiness of the device. In more detail, when using the device for vaporizing a liquid to be vaporized according to the present invention, for example in an air analysis system, the capillary barrier may be located inside the system. analysis and in contact with the air to be treated, while being exchangeable between two successive analyzes thanks to its removability. Thus, the risk of a contamination of the analysis system that could distort the results obtained can easily and effectively be ruled out.
Selon un mode d'exĆ©cution, ledit rĆ©servoir, ladite pompe capillaire et ladite barriĆØre capillaire sont prĆ©vus sous forme de disques empilĆ©s. Alternativement, au moins ladite pompe capillaire peut ĆŖtre prĆ©vue sous forme cylindrique et ladite barriĆØre capillaire sous forme annulaire, ladite barriĆØre capillaire entourant ladite pompe capillaire au moins partiellement.According to one embodiment, said reservoir, said capillary pump and said capillary barrier are provided in the form of stacked disks. Alternatively, at least said capillary pump may be provided in cylindrical form and said capillary barrier in annular form, said capillary barrier surrounding said capillary pump at least partially.
Ainsi, un dispositif compact et rigide pour la vaporisation d'un liquide Ć vaporiser peut ĆŖtre obtenu.Thus, a compact and rigid device for vaporizing a liquid to be vaporized can be obtained.
Ledit rĆ©servoir, ladite pompe capillaire et ladite barriĆØre capillaire sont prĆ©fĆ©rablement disposĆ©s dans un support extĆ©rieur. Ledit support extĆ©rieur comporte prĆ©fĆ©rablement du verre, de la cĆ©ramique et/ou du plastique adaptĆ©s Ć rĆ©sister Ć la chaleur requise pour la vaporisation dudit liquide Ć vaporiser. De plus, de tels matĆ©riaux prĆ©sentent une conductivitĆ© thermique faible, ce qui minimise les pertes d'Ć©nergie thermiques: on minimise alors la consommation Ć©nergĆ©tique du dispositif.Said tank, said capillary pump and said capillary barrier are preferably arranged in an external support. Said outer support preferably comprises glass, ceramic and / or plastic adapted to withstand the heat required for the vaporization of said liquid to be vaporized. In addition, such materials have a low thermal conductivity, which minimizes thermal energy losses: the energy consumption of the device is then minimized.
Ainsi, un support extĆ©rieur peu coĆ»teux peut ĆŖtre proposĆ©, adaptĆ© Ć maintenir les composants constitutifs du dispositif pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention dans une structure prĆ©dĆ©finie de maniĆØre sĆ»re et solide.Thus, an inexpensive external support can be proposed, adapted to maintain the constituent components of the device for the vaporization of a liquid to be vaporized according to the present invention in a predefined structure in a safe and solid manner.
Selon un mode d'exĆ©cution, ledit Ć©lĆ©ment chauffant comporte au moins un matĆ©riau inoxydable. De prĆ©fĆ©rence, ledit Ć©lĆ©ment chauffant est disposĆ© dans une direction de pompage capillaire dudit liquide Ć vaporiser entre ladite pompe capillaire et ladite barriĆØre capillaire. Alternativement, ledit Ć©lĆ©ment chauffant peut ĆŖtre disposĆ© dans une direction de pompage capillaire dudit liquide Ć vaporiser en aval de ladite barriĆØre capillaire.According to one embodiment, said heating element comprises at least one stainless material. Preferably, said heating element is disposed in a capillary pumping direction of said liquid to be vaporized between said capillary pump and said capillary barrier. Alternatively, said heating element may be disposed in a capillary pumping direction of said liquid to be vaporized downstream of said capillary barrier.
La prĆ©sente invention permet ainsi de disposer un Ć©lĆ©ment chauffant fiable Ć un endroit du dispositif pour la vaporisation d'un liquide Ć vaporiser, au voisinage duquel la vaporisation du liquide aura lieu. Ainsi, la chaleur requise pour la vaporisation peut ĆŖtre produite exactement Ć l'endroit de la vaporisation, permettant alors une consommation minimisĆ©e en puissance Ć©lectrique par l'Ć©lĆ©ment chauffant et, donc, par le dispositif lors de son fonctionnement.The present invention thus provides a reliable heating element at a location of the device for the vaporization of a liquid to vaporize, in the vicinity of which the vaporization of the liquid will take place. Thus, the heat required for the vaporization can be produced exactly at the point of vaporization, thus allowing a minimized consumption of electrical power by the heating element and, therefore, by the device during its operation.
Ledit ƩlƩment chauffant est prƩfƩrablement prƩvu sous forme d'une grille Ʃlectriquement conductrice.Said heating element is preferably provided in the form of an electrically conductive grid.
Ainsi, un Ć©lĆ©ment chauffant simple et efficace peut ĆŖtre rĆ©alisĆ©.Thus, a simple and effective heating element can be realized.
Selon un mode d'exĆ©cution, ladite pompe capillaire comporte au moins un composant poreux mouillant permĆ©able au dit liquide Ć vaporiser. La porositĆ© dudit au moins un composant poreux non mouillant peut ĆŖtre plus grande que la porositĆ© dudit au moins un composant poreux mouillant. Cela permet une Ć©vacuation facilitĆ©e de la vapeur. Mais la porositĆ© dudit au moins un composant poreux non mouillant peut aussi ĆŖtre plus faible que la porositĆ© dudit au moins un composant poreux mouillant. Cela sera notamment le cas si on souhaite que le composant poreux non mouillant constitue une barriĆØre prĆ©venant une pollution du dispositif par l'environnement extĆ©rieur, par exemple une pollution bactĆ©riologique.According to one embodiment, said capillary pump comprises at least one porous wetting component permeable to said liquid to be vaporized. The porosity of said at least one non-wetting porous component may be greater than the porosity of said at least one porous wetting component. This allows easy evacuation of steam. But the porosity of said at least one non-wetting porous component may also be lower than the porosity of said at least one porous wetting component. This will be particularly the case if it is desired that the non-wetting porous component constitutes a barrier preventing pollution of the device by the external environment, for example a bacteriological pollution.
Ainsi, une pompe capillaire fonctionnelle et fiable peut ĆŖtre proposĆ©e.Thus, a functional and reliable capillary pump can be proposed.
Ledit au moins un composant poreux mouillant peut ĆŖtre pourvu d'un gradient de porositĆ©, ou comporte au moins un premier composant poreux et un second composant poreux, la porositĆ© dudit premier composant poreux Ć©tant plus grande que la porositĆ© dudit second composant poreux. On sait qu'un gradient de porositĆ© dĆ©croissant, obtenu par une rĆ©duction des diamĆØtres des pores, selon la direction de pompage du liquide, augmente la pression de pompage.The at least one porous wetting component may be provided with a porosity gradient, or comprise at least a first porous component and a second porous component, the porosity of said first porous component being greater than the porosity of said second porous component. It is known that a decreasing porosity gradient, obtained by a reduction of the pore diameters, according to the pumping direction of the liquid, increases the pumping pressure.
Ainsi, un composant poreux mouillant simple, robuste et efficace peut ĆŖtre rĆ©alisĆ©.Thus, a simple, robust and efficient wetting porous component can be realized.
Il est Ć noter que les dispositifs pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention peuvent vaporiser n'importe quel type de liquide, pourvu qu'il puisse ĆŖtre vaporisĆ© dans des conditions appropriĆ©es, par exemple une chaleur de vaporisation requise et un point d'Ć©bullition associĆ©. Des liquides Ć vaporiser peuvent comprendre l'eau, l'Ć©thanol, des composĆ©s de parfum, des traitements de rĆ©colte, des produits rĆ©pulsifs et/ou attractants d'insectes, des antiseptiques, des inhalants et autres compositions mĆ©dicales, ainsi que d'autres liquides pour lesquels la vaporisation est dĆ©sirable et/ou nĆ©cessaire afin de permettre par exemple de doser prĆ©cisĆ©ment une vapeur telle que dans un processus de production ou de dĆ©pĆ“t d'une vapeur chimique. Les avantages d'une utilisation des dispositifs pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention pour vaporiser des liquides, sont que la vapeur peut ĆŖtre produite du haut vers le bas du dispositif et entraĆ®nĆ©e par l'Ć©coulement d'air. Ainsi, le rĆ©servoir contenant le liquide peut ĆŖtre situĆ© au-dessus d'une zone d'Ć©vaporation associĆ©e, si bien que la pression hydrostatique se substitue aux pompes mĆ©caniques et systĆØmes de pressurisation. De plus, les composants poreux mouillants assurent l'alimentation uniforme de l'Ć©lĆ©ment chauffant si le dispositif est inclinĆ©. Finalement, le corps externe du dispositif est d'une gĆ©omĆ©trie simple si bien qu'il est facile Ć nettoyer.It should be noted that devices for spraying a liquid spray according to the present invention can vaporize any type of liquid, provided that it can be vaporized under appropriate conditions, for example a required heat of vaporization and an associated boiling point. Sprayable liquids may include water, ethanol, perfume compounds, crop treatments, insect repellants and / or attractants, antiseptics, inhalants, and other medical compositions, as well as other liquids for which the Spraying is desirable and / or necessary in order, for example, to accurately measure a vapor such as in a process of producing or depositing a chemical vapor. The advantages of using devices for spraying a liquid spray according to the present invention for vaporizing liquids are that the steam can be produced from the top to the bottom of the device and driven by the airflow. Thus, the reservoir containing the liquid can be located above an associated evaporation zone, so that the hydrostatic pressure is substituted for the mechanical pumps and pressurization systems. In addition, the wetting porous components provide uniform supply of the heating element if the device is inclined. Finally, the outer body of the device is of simple geometry so that it is easy to clean.
Un exemple de rĆ©alisation et d'application d'un dispositif pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention tel que dĆ©crit ci-dessus est un compteur et/ou collecteur de particules comprises dans un gaz Ć traiter, tel que l'air, par exemple un compteur et/ou collecteur de particules par collection Ć©lectrostatique semi-humide. Dans de tels compteurs et/ou collecteurs, l'air Ć traiter est parfois enrichi, voire mĆŖme saturĆ©, en vapeur de faƧon Ć provoquer un grossissement des particules par nuclĆ©ation, soit pour des compteurs Ć des fins de comptage via des moyens optiques, soit pour des collecteurs Ć des fins de collecte. La prĆ©sente invention peut ĆŖtre intĆ©grĆ©e dans de tels appareils et les amĆ©liorerait par ses avantages sur les appareils de l'Ć©tat de l'art antĆ©rieur. Un dispositif collecteur Ć©lectrostatique est par exemple dĆ©crit dans la demande
Par exemple, un collecteur de particules semi-humide requiert l'enrichissement de l'air en vapeur d'eau pour:
- faire grossir des particules Ć collecter et ainsi faciliter leur collecte dans un champ Ć©lectrique intense,
- former un film liquide sur une paroi, qui s'Ć©coule par gravitĆ© et entraĆ®ne des particules Ć collecter vers un systĆØme d'analyse.
- make particles to collect collect and thus facilitate their collection in an intense electric field,
- forming a liquid film on a wall, which flows by gravity and causes particles to be collected to an analysis system.
En associant un dispositif pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention tel que dĆ©crit ci-dessus avec un tel collecteur de particules semi-humide, il serait possible d'exploiter l'Ć©coulement de l'air pour forcer l'Ć©coulement du film liquide sur la paroi et donc orienter le collecteur diffĆ©remment. Autrement dit, au lieu d'avoir un flux d'air et de vapeur du bas vers le haut, il serait possible d'orienter les flux d'air et de vapeur du haut vers le bas en utilisant un dispositif pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention.By associating a device for the vaporization of a liquid to vaporize according to the present invention as described above with such a semi-wet particle collector, it would be possible to exploit the flow of air to force the flow of the liquid film on the wall and thus orient the collector differently. In other words, instead of having a flow of air and steam from bottom to top, it would be possible to direct the flow of air and steam from top to bottom using a device for the vaporization of a liquid to be vaporized according to the present invention.
Il est nĆ©anmoins Ć noter, que l'utilisation du dispositif pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention pour la rĆ©alisation d'un compteur et/ou collecteur de particules a seulement Ć©tĆ© dĆ©crit pour l'illustration sans vouloir restreindre le dispositif Ć une telle utilisation. Au contraire, une utilisation du dispositif dans de nombreuses diffĆ©rentes applications est envisageable, telle que par exemple une utilisation pour la rĆ©alisation d'un appareil de traitement des voies respiratoires par de l'air humidifiĆ©.It should nevertheless be noted that the use of the device for the vaporization of a liquid to be sprayed according to the present invention for the production of a counter and / or particle collector has only been described for illustration without limiting the device to such use. On the contrary, a use of the device in many different applications is conceivable, such as for example a use for the production of an apparatus for treatment of the respiratory tract with humidified air.
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La
figure 1 est un diagramme schĆ©matique en vue de cĆ“tĆ© illustrant un compteur et/ou collecteur de particules par collection Ć©lectrostatique semi-humide comportant un dispositif pour la vaporisation d'un liquide Ć vaporiser selon un mode de rĆ©alisation de la prĆ©sente invention.Thefigure 1 is a schematic side view diagram illustrating a semi-wet electrostatic collection particle counter and / or collector including a device for vaporizing a liquid to be vaporized according to an embodiment of the present invention. -
La
figure 2 est un diagramme schĆ©matique en vue de cĆ“tĆ© illustrant un dispositif pour la vaporisation d'un liquide Ć vaporiser comportant une pompe capillaire selon un autre mode de rĆ©alisation de la prĆ©sente invention.Thefigure 2 is a schematic side view diagram illustrating a device for vaporizing a vaporizing liquid having a capillary pump according to another embodiment of the present invention. -
La
figure 3 est un diagramme schĆ©matique en vue de cĆ“tĆ© illustrant un dispositif pour la vaporisation d'un liquide Ć vaporiser comportant une pompe capillaire selon encore un autre mode de rĆ©alisation de la prĆ©sente invention avec un assemblage de composants sous forme de disques.Thefigure 3 is a schematic side view diagram illustrating a device for vaporizing a vaporizing liquid having a capillary pump according to yet another embodiment of the present invention with an assembly of disc components. -
La
figure 4 est un diagramme schĆ©matique en vue de cĆ“tĆ© illustrant un dispositif pour la vaporisation d'un liquide Ć vaporiser comportant une pompe capillaire selon encore un autre mode de rĆ©alisation de la prĆ©sente invention avec un assemblage de composants ayant une gĆ©omĆ©trie cylindrique.Thefigure 4 is a schematic side view diagram illustrating a device for vaporizing a vaporizing liquid having a capillary pump according to yet another embodiment of the present invention with an assembly of components having a cylindrical geometry. -
La
figure 5 est un diagramme schĆ©matique en vue de cĆ“tĆ© illustrant un systĆØme d'analyse de particules comportant un dispositif pour la vaporisation d'un liquide Ć vaporiser selon la prĆ©sente invention.Thefigure 5 is a schematic side view diagram illustrating a particle analysis system having a device for vaporizing a liquid to be vaporized according to the present invention.
La
Le dispositif pour la vaporisation d'un liquide Ć vaporiser 100 comporte Ć titre d'exemple une configuration sous forme de disques empilĆ©s. Lors du fonctionnement du dispositif 100, un liquide est aspirĆ© par une ou plusieurs couches Ć pompage capillaire et ensuite vaporisĆ©. La vapeur produite est expulsĆ©e ou Ć©mise dans des conditions pressurisĆ©es ou essentiellement non pressurisĆ©es et peut ĆŖtre utilisĆ©e directement. Pour la simplicitĆ© de la description ci-aprĆØs, le dispositif 100 est par la suite aussi dĆ©signĆ© comme Ā« dispositif d'Ć©vaporation Ā».The device for vaporizing a liquid to be vaporized 100 comprises, by way of example, a configuration in the form of stacked disks. During operation of the
Le dispositif d'Ć©vaporation 100 comporte pour l'illustration un rĆ©servoir 101 susceptible de contenir un liquide Ć vaporiser 111, un Ć©lĆ©ment chauffant 105 susceptible de chauffer du liquide afin de le vaporiser, une pompe capillaire 110 susceptible de pomper du liquide contenu dans le rĆ©servoir 101 vers l'Ć©lĆ©ment chauffant 105 par pompage capillaire, et une barriĆØre capillaire 106 disposĆ©e dans une direction 102 de pompage capillaire du liquide Ć vaporiser 111 en aval de la pompe capillaire 110. Selon l'invention, la barriĆØre capillaire 106 est susceptible d'empĆŖcher du liquide non vaporisĆ© de s'Ć©chapper du dispositif 100 et comporte prĆ©fĆ©rablement au moins un composant poreux non mouillant 116.The
La pompe capillaire 110 est permĆ©able au liquide Ć vaporiser 111 et comporte au moins un composant poreux mouillant 103, 104. Le diamĆØtre des pores de ce composant poreux mouillant 103, 104 peut ĆŖtre plus grand que le diamĆØtre des pores du composant poreux non mouillant 116. A titre d'exemple, la pompe capillaire 110 comporte un premier composant poreux 103 et un second composant poreux 104. La porositĆ© du premier composant poreux 103 est plus grande que la porositĆ© du second composant poreux 104. Autrement dit, les pores du second composant poreux mouillant 104 sont prĆ©fĆ©rablement bien plus petits que ceux du premier composant poreux mouillant 103. De plus, le premier composant poreux mouillant 103 est prĆ©fĆ©rablement Ć©pais par rapport au second composant poreux mouillant 104 pour assurer une bonne isolation thermique entre l'Ć©lĆ©ment chauffant 105 et le rĆ©servoir 101 du liquide Ć vaporiser 111. La fonction de pompage du liquide 111 peut ĆŖtre assurĆ©e par capillaritĆ© pourvu que les capillaires ou pores des composants poreux mouillants 103, 104 soient d'un diamĆØtre suffisamment petit, prĆ©fĆ©rablement infĆ©rieur au millimĆØtre, de quelques dixiĆØmes de micron Ć quelques centaines de microns. Ainsi, dans un mode d'exĆ©cution prĆ©fĆ©rĆ© de l'invention, le premier composant poreux mouillant 103 est pourvu d'une porositĆ© de quelques dizaines de microns voire centaines de microns et le second composant poreux mouillant 104 est pourvu d'une porositĆ© de quelques dixiĆØmes de micron Ć quelques microns.The
Il est nĆ©anmoins Ć noter que le second composant poreux mouillant 104 est purement optionnel. Le dispositif d'Ć©vaporation 100 peut donc ĆŖtre rĆ©alisĆ© selon un mode d'exĆ©cution de la prĆ©sente invention sans le second composant poreux mouillant 104. Dans ce cas, le premier composant poreux mouillant 103 constitue par exemple en lui seul la pompe capillaire 110 selon la prĆ©sente invention et est alors, prĆ©fĆ©rablement, pourvu d'un gradient de porositĆ©.It should nevertheless be noted that the second wetting
Lors du fonctionnement du dispositif d'Ć©vaporation 100, le premier composant poreux mouillant 103 et le second composant poreux mouillant 104 assurent un pompage capillaire du liquide Ć vaporiser 111 depuis le rĆ©servoir 101. Une voie liquide est Ć©tablie dans la direction de la flĆØche 102, et une voie de circulation de chaleur est Ć©tablie dans la zone comportant l'Ć©lĆ©ment chauffant 105.During operation of the
Comme il a Ć©tĆ© prĆ©cisĆ© auparavant, un des avantages du dispositif d'Ć©vaporation 100 est qu'il fonctionne de faƧon passive en ce qui concerne le pompage capillaire et sans fuite quelconque indĆ©pendamment de son orientation lors de l'utilisation. Cependant, comme il a Ć©tĆ© mentionnĆ© plus haut, un milieu poreux mouillant ne peut arrĆŖter l'Ć©coulement d'un liquide. Dans la situation oĆ¹ le dispositif d'Ć©vaporation 100 est retournĆ©, le rĆ©servoir de liquide 101 se trouvant alors au-dessus des composants poreux mouillants 103, 104, le rĆ©servoir 101 se viderait goutte Ć goutte. Dans une telle situation, les composants poreux mouillants 103, 104 ne serviraient qu'Ć limiter le dĆ©bit d'Ć©coulement en introduisant une forte perte de charge. Pour pallier Ć ce problĆØme, le dispositif d'Ć©vaporation 100 selon la prĆ©sente invention comporte le composant poreux non mouillant 116. Ce composant poreux non mouillant 116 est impermĆ©able au dit liquide Ć vaporiser 111 et permĆ©able Ć la vapeur gĆ©nĆ©rĆ©e Ć partir dudit liquide Ć vaporiser 111. Dans cette configuration, une interface liquide/vapeur ou liquide/air est bloquĆ©e Ć l'interface entre les deux milieux poreux mouillants 103, 104 et non mouillant 116.As has been stated before, one of the advantages of the
Dans le contexte de la prĆ©sente invention, un matĆ©riau est dit Ā« mouillant Ā» lorsqu'une goutte posĆ©e dessus conduit Ć un angle de contact de la ligne triple infĆ©rieur Ć 90Ā° selon une dĆ©finition communĆ©ment admise. Ainsi, un matĆ©riau mouillant et poreux est permĆ©able Ć un liquide, par exemple le liquide Ć vaporiser 111. Le terme Ā« hydrophile Ā» est rĆ©servĆ© aux matĆ©riaux mouillants vis-Ć -vis de l'eau. Un matĆ©riau est dit Ā« non mouillant Ā» lorsqu'une goutte posĆ©e dessus conduit Ć un angle de contact de la ligne triple supĆ©rieur Ć 90Ā°. Un matĆ©riau non mouillant est gĆ©nĆ©ralement impermĆ©able (ou peu permĆ©able) Ć un liquide, par exemple le liquide Ć vaporiser 111, et peut ĆŖtre permĆ©able Ć la vapeur s'il est poreux. Le terme Ā« hydrophobe Ā» est rĆ©servĆ© aux matĆ©riaux non mouillants vis-Ć -vis de l'eau.In the context of the present invention, a material is said to be "wetting" when a drop placed on it leads to a contact angle of the triple line less than 90 Ā° according to a commonly accepted definition. Thus, a wetting and porous material is permeable to a liquid, for example the spraying
Selon un mode d'exĆ©cution, le composant poreux non mouillant 116 comporte une membrane en matĆ©riau polymĆØre, comme par exemple le tĆ©flon. De prĆ©fĆ©rence, le composant poreux non mouillant 116 est comparativement peu conducteur de chaleur requise pour la vaporisation dudit liquide Ć vaporiser 111 et adaptĆ© Ć rĆ©sister aux tempĆ©ratures de vaporisation, par exemple 100Ā°C pour de l'eau. Pour ce faire, le composant poreux non mouillant 116 peut comporter un matĆ©riau thermiquement isolant.According to one embodiment, the non-wetting
SituĆ© entre le premier composant poreux mouillant 103 et le composant poreux non mouillant 116, l'Ć©lĆ©ment chauffant 105 chauffe directement l'interface liquide/vapeur ou liquide/air. PrĆ©cisons que l'interface liquide/vapeur n'est pas nĆ©cessairement situĆ©e au niveau de l'Ć©lĆ©ment chauffant, mais peut se dĆ©placer, dans le milieu poreux 103, 104 vers le rĆ©servoir 101. Plus en dĆ©tail, l'Ć©lĆ©ment chauffant 105, situĆ© au niveau de cette interface ou bien dans le voisinage immĆ©diat de cette interface, permet de vaporiser le liquide pompĆ© vers cette interface. Cet Ć©lĆ©ment chauffant 105 est avantageusement une grille, Ć©lectriquement conductrice et prĆ©fĆ©rablement constituĆ©e d'un matĆ©riau inoxydable. L'Ć©lĆ©ment chauffant 105 peut ĆŖtre pourvu de, et Ć©lectriquement liĆ© Ć , une source d'Ć©nergie (non montrĆ©e). TraversĆ© par un courant Ć©lectrique de cette source, il s'Ć©chauffe par effet Joule et chauffe l'interface liquide/vapeur ou liquide/air oĆ¹ il se trouve. L'Ć©nergie fournie est ainsi transmise directement et uniquement Ć l'endroit oĆ¹ elle est nĆ©cessaire. De plus, en choisissant des composants poreux 103, 104 et/ou 116 dans des matĆ©riaux faiblement conducteurs de la chaleur, les pertes d'Ć©nergie thermique sont trĆØs faibles. L'Ć©lĆ©ment chauffant 105 peut par exemple ĆŖtre constituĆ© d'une grille constituĆ©e de fils d'acier inoxydable de diamĆØtre de 100 Āµm, la distance entre chaque fil Ć©tant de l'ordre de grandeur du diamĆØtre, alimentĆ© par une tension de quelques Volts.Located between the first wetting
Plus gĆ©nĆ©ralement, lorsqu'une source d'Ć©nergie Ć©lectrique est disponible, un Ć©lĆ©ment de chauffage pouvant ĆŖtre chauffĆ© par l'Ć©nergie Ć©lectrique peut ĆŖtre utilisĆ© afin de rĆ©aliser l'Ć©lĆ©ment chauffant 105 pour fournir l'Ć©nergie thermique requise pour la vaporisation. Les Ć©lĆ©ments de chauffage Ć base de rĆ©sistances Ć©lectriques ou comportant un thermistor ou toute autre matiĆØre rĆ©sistive de chauffage appropriĆ©e et adaptĆ©e Ć se chauffer, lorsqu'ils sont traversĆ©s par un courant Ć©lectrique, peuvent ĆŖtre utilisĆ©s. La matiĆØre rĆ©sistive de chauffage peut ĆŖtre conƧue comme un fil, une matiĆØre poreuse, une tĆ“le perforĆ©e ou un disque, ou peut ĆŖtre dĆ©posĆ©e comme pellicule mince ou Ć©paisse. PrĆ©fĆ©rablement, elle est incorporĆ©e de faƧon Ć ce que la permĆ©abilitĆ© par rapport Ć la vapeur Ć la surface d'Ć©mission de vapeur du composant vaporisateur, c'est-Ć -dire du composant poreux non mouillant 116, soit sensiblement maintenue. Alternativement, la chaleur peut ĆŖtre appliquĆ©e directement sur la surface du composant poreux non mouillant 116 Ć l'aide d'une matiĆØre rĆ©sistive de chauffage, en contact direct avec ou dĆ©posĆ©e directement sur le composant poreux non mouillant 116.More generally, when a source of electric power is available, a heating element that can be heated by electrical energy can be used to provide the
Les composants constitutifs du dispositif d'Ʃvaporation 100 dƩcrit ci-dessus sont suffisamment alignƩs pour produire et entretenir les voies d'Ʃcoulement de liquide afin que le liquide et la vapeur puissent voyager dans ou sur des surfaces associƩes de diffƩrents composants par pompage capillaire. Les diffƩrents composants poreux mouillants 103, 104 constituant la pompe sont en contact l'un avec l'autre, et sont Ʃgalement en contact avec le rƩservoir 101. Dans quelques modes de rƩalisation, chacune des surfaces des diffƩrents composants entre Ʃtroitement en contact avec une surface adjacente sensiblement sans lacunes ou vides. L'Ʃpaisseur relative, ou le volume, des diffƩrents composants dƩpend de la fonction que le composant fournit et de l'application pour le pompage capillaire.The constituent components of the
Les composants constituant le dispositif d'Ć©vaporation 100 selon la prĆ©sente invention dĆ©crits ci-dessus peuvent ĆŖtre choisis dans diffĆ©rents matĆ©riaux. Ainsi, les composants poreux mouillants 103, 104 sont de prĆ©fĆ©rence rĆ©alisĆ©s en utilisant des matĆ©riaux peu conducteurs de la chaleur tels que par exemple un frittĆ© en verre, des billes de verre, des fibres de verre, des frittĆ©s ou poreux d'acier inox. D'autres matiĆØres poreuses exemplaires qui peuvent ĆŖtre utilisĆ©es comprennent la cĆ©ramique poreuse, telle que la matiĆØre de meule d'alumine (de la maniĆØre prĆ©vue, par exemple, par Abrasives Unlimited Inc., San Leandro, Californie). D'autres types d'absorbants et/ou matiĆØres poreuses comprenant le coton, la fibre de verre (telle que NOMEXTM d'E. I. Dupont de Nemours et Cie., Wilmington, Delaware) et semblables, connus par l'homme du mĆ©tier, peuvent alternativement ĆŖtre utilisĆ©s. Ces matiĆØres ont une conductivitĆ© thermique maximale d'environ 0.03 Ć 3 W/m-K.The components constituting the
La
La diffƩrence entre le dispositif 200 et le dispositif 100 de la
L'arrangement selon la
La
L'assemblage est maintenu par un support 308. Ce dernier comporte un support supƩrieur annulaire 309 (illustrƩ dans la
La
Le premier composant poreux mouillant 403 a une forme cylindrique et est maintenu avec le rƩservoir cylindrique 401 par un support annulaire 404, et un support en forme de disque 405. Plus en dƩtail, en bas de la
De plus, le premier composant poreux mouillant 403 est entourĆ© par le second composant poreux mouillant 407 possĆ©dant Ć titre d'exemple une forme de tube et Ć©galement maintenu par le support 404, 405. Le second composant poreux mouillant 407 est entourĆ© par l'Ć©lĆ©ment chauffant 408, prĆ©vu sous forme de spirale et pouvant servir Ć maintenir l'arrangement de la
La
Le dispositif 500 comporte Ć titre d'exemple un rĆ©servoir 501 susceptible de contenir un liquide Ć vaporiser 521, le rĆ©servoir 501 Ć©tant arrangĆ© dans la
Le rĆ©servoir 501, les premier et second composants poreux mouillants 504, 505 et l'Ć©lĆ©ment chauffant 506 sont maintenus par un support 510. Ce dernier comporte un premier support infĆ©rieur annulaire 509 et un deuxiĆØme support infĆ©rieur annulaire 507 sous forme d'un rebord (illustrĆ© dans la
Le deuxiĆØme support infĆ©rieur symĆ©trique 507 est prĆ©vu pour maintenir le rĆ©servoir 501, les premier et second composants poreux mouillants 504, 505 et l'Ć©lĆ©ment chauffant 506 sous forme de disques empilĆ©s, tel qu'illustrĆ© dans la
Selon un mode d'exĆ©cution, le premier support infĆ©rieur symĆ©trique 509 est amovible et permet un remplacement et/ou un nettoyage facile et rapide du composant poreux non mouillant 518 amovible, tandis que les autres composants sont maintenus pendant ces opĆ©rations de remplacement et/ou nettoyage du composant 518 par le deuxiĆØme support infĆ©rieur symĆ©trique 507. Comme dĆ©jĆ mentionnĆ© plus haut et comme visible dans la
La prĆ©sente invention a Ć©tĆ© dĆ©crite ci-dessus en dĆ©tail concernant des modes d'exĆ©cution et de rĆ©alisation spĆ©cifiques par rapport aux figures annexes. Ces modes spĆ©cifiques ne doivent pas ĆŖtre interprĆ©tĆ©s comme limitations de la portĆ©e de l'invention, mais en tant que modes d'exĆ©cution et de rĆ©alisation exemplaires. Il est Ć noter que des modifications et des substitutions peuvent ĆŖtre apportĆ©es aux dispositifs pour la vaporisation d'un liquide Ć vaporiser, aussi bien qu'Ć des procĆ©dĆ©s de leur utilisation, sans s'Ć©carter de la portĆ©e de l'invention.The present invention has been described above in detail concerning specific embodiments and embodiments with respect to the accompanying figures. These specific modes should not be interpreted as limitations of the scope of the invention, but as exemplary embodiments and embodiments. It should be noted that modifications and substitutions may be made to devices for vaporizing a liquid to be vaporized, as well as to methods of their use, without departing from the scope of the invention.
L'invention peut par exemple ĆŖtre rĆ©alisĆ©e par l'empilement de divers composants, dĆ©crits ci-dessus en faisant rĆ©fĆ©rence Ć la
Dans un exemple de rĆ©alisation, le premier composant poreux mouillant 103 est constituĆ© d'un frittĆ© en verre d'1mm d'Ć©paisseur et d'une porositĆ© d'environ 100 Ć 200Āµm. Le second composant poreux mouillant 104 est constituĆ© d'une membrane de filtration en fibre de verre Ć©paisse de 260Āµm ayant un seuil de filtration de 1,6Āµm. L'Ć©lĆ©ment chauffant 105 est une toile mĆ©tallique constituĆ©e de fils en inox de 97Āµm de diamĆØtre, et espacĆ©s d'une distance voisine de ce diamĆØtre. Ces fils en inox sont parcourus par un courant Ć©lectrique et constituent ainsi l'Ć©lĆ©ment chauffant 105. Le composant poreux non mouillant 116 est constituĆ© d'une membrane de filtration en tĆ©flon ayant un seuil de filtration de 20Āµm. Les membranes employĆ©es peuvent ĆŖtre par exemple des filtres disponibles dans le commerce. Leurs diamĆØtres sont couramment de 25, 47 ou 90 mm. Le diamĆØtre des dispositifs d'Ć©vaporation est gĆ©nĆ©ralement compris entre 3 et 20 cm, et leur hauteur est comprise entre 2 et 20 cm.In an exemplary embodiment, the first wetting
Claims (20)
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FR1004598A FR2967915B1 (en) | 2010-11-26 | 2010-11-26 | EVAPORATION DEVICE |
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EP2457629B1 (en) | 2019-01-09 |
FR2967915A1 (en) | 2012-06-01 |
US9352246B2 (en) | 2016-05-31 |
FR2967915B1 (en) | 2014-05-16 |
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