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EP1570899A2 - Method and apparatus for the preparation of diluted solutions - Google Patents

Method and apparatus for the preparation of diluted solutions Download PDF

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Publication number
EP1570899A2
EP1570899A2 EP05004665A EP05004665A EP1570899A2 EP 1570899 A2 EP1570899 A2 EP 1570899A2 EP 05004665 A EP05004665 A EP 05004665A EP 05004665 A EP05004665 A EP 05004665A EP 1570899 A2 EP1570899 A2 EP 1570899A2
Authority
EP
European Patent Office
Prior art keywords
amount
different
concentrate
different concentrations
concentrates
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP05004665A
Other languages
German (de)
French (fr)
Other versions
EP1570899A3 (en
Inventor
Hans Georg Hagleitner
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Individual
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Individual
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Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of EP1570899A2 publication Critical patent/EP1570899A2/en
Publication of EP1570899A3 publication Critical patent/EP1570899A3/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/405Methods of mixing liquids with liquids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/20Measuring; Control or regulation
    • B01F35/22Control or regulation
    • B01F35/221Control or regulation of operational parameters, e.g. level of material in the mixer, temperature or pressure
    • B01F35/2216Time, i.e. duration, of at least one parameter during the operation
    • B01F35/22162Time of feeding of at least one of the components to be mixed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/80Forming a predetermined ratio of the substances to be mixed
    • B01F35/83Forming a predetermined ratio of the substances to be mixed by controlling the ratio of two or more flows, e.g. using flow sensing or flow controlling devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/80Forming a predetermined ratio of the substances to be mixed
    • B01F35/88Forming a predetermined ratio of the substances to be mixed by feeding the materials batchwise
    • B01F35/883Forming a predetermined ratio of the substances to be mixed by feeding the materials batchwise using flow rate controls for feeding the substances
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/24Mixing of ingredients for cleaning compositions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/48Mixing liquids with liquids; Emulsifying characterised by the nature of the liquids
    • B01F23/483Mixing liquids with liquids; Emulsifying characterised by the nature of the liquids using water for diluting a liquid ingredient, obtaining a predetermined concentration or making an aqueous solution of a concentrate
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/20Measuring; Control or regulation

Definitions

  • the invention relates to a method and an apparatus for producing dilute Solutions in different concentrations of especially diverse Concentrates, each containing an amount of a concentrate and an amount of one Diluent are mixed.
  • the Proceeding the same i. for more dilute solutions will be more volume units a diluent mixed.
  • one liter of a ten percent solution can be made thereby that 10 centiliters of concentrate and 90 centiliters of diluent are mixed.
  • suitable portioning device has two containers with said space contents on. This portioning device may also be used to prepare a five percent solution which must contain 95 centiliters of diluent. In this case will a half vorverPolntes concentrate used because of the Portioning device already spent 10 centiliters of prediluted concentrate contain 5 centiliters of the diluent missing on 95 centiliters.
  • metering devices with constant Flow rates selected per unit time. Twenty liters of the above ten percent Solution are by metering devices with flow rates of two liters and eighteen liters per minute in one minute. Twenty liters of a five percent Solution are also prepared in one minute by means of these dosing devices, if the concentrate is prediluted by half and already one liter of diluent contains.
  • the inventive method is especially because in one and the same Dosing or portioning device can be diluted different means that usually not used in the same dilution. It is only necessary that various means in the same, can be used in the device, interchangeable bottles or containers.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Accessories For Mixers (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The method involves providing an amount of diverse concentrate and an amount of diluents. The concentrate and the diluents are mixed. A ratio between the amount of concentrate and amount of diluents is kept constant by actuating two metering apparatuses with different flow rates per unit time for an equal length of time. Different concentrations of the solutions are produced by using concentrates with different concentrations. An independent claim is also included for an apparatus for producing diluted solutions in different concentrations.

Description

Die Erfindung betrifft ein Verfahren und eine Vorrichtung zur Herstellung verdünnter Lösungen in unterschiedlichen Konzentrationen aus insbesondere verschiedenartigen Konzentraten, wobei jeweils eine Menge eines Konzentrates und eine Menge eines Verdünnungsmittels vermischt werden.The invention relates to a method and an apparatus for producing dilute Solutions in different concentrations of especially diverse Concentrates, each containing an amount of a concentrate and an amount of one Diluent are mixed.

Bei der Herstellung verdünnter Lösungen wird üblicherweise auf eine Volumseinheit des Konzentrates eine dem Verdünnungsfaktor entsprechende Vielzahl von Volumseinheiten des Verdünnungsmittels zugegeben.In the preparation of dilute solutions is usually based on a volume of the Concentrate a plurality of volume units corresponding to the dilution factor Diluent added.

Falls die verdünnten Lösungen unterschiedliche Konzentrationen aufweisen sollen, bleibt die Vorgangsweise dieselbe, d.h. für stärker verdünnte Lösungen werden mehr Volumseinheiten eines Verdünnungsmittels zugemischt.If the dilute solutions should have different concentrations, the Proceeding the same, i. for more dilute solutions will be more volume units a diluent mixed.

Diese im Prinzip völlig zufriedenstellende Vorgangsweise weist Nachteile auf, da Bemessungsfehler auftreten können. Diese bestehen hauptsächlich darin, dass das Volumen des Verdünnungsmittels falsch bestimmt, oder die Anzahl der Volumseinheiten falsch berechnet wird.This in principle completely satisfactory approach has disadvantages because Design errors can occur. These consist mainly in that the Volume of diluent incorrectly determined, or the number of volume units calculated incorrectly.

Die Fehler einer falschen Mengenbemessung treten wesentlich häufiger auf, als Fehler bei Herstellung von Konzentraten mit unterschiedlichen Konzentrationen, da die Mengenbemessung durch den Konsumenten bzw. Benützer erfolgt, während die Konzentrationseinstellung üblicherweise beim Hersteller des Konzentrates vorgenommen wird.The errors of a wrong quantity measurement occur much more frequently than errors Production of concentrates with different concentrations, as the Quantity measurement by the consumer or user takes place while the Concentration adjustment usually made by the manufacturer of the concentrate becomes.

So ist beispielsweise bei Reinigungs- oder Desinfektionsmitteln durch eine Zugabe einer Verschlusskappe des Mittels zu einem Eimer Wasser eine gleichbleibende Konzentration nahezu unmöglich, da weder der Wassereimer noch die Verschlusskappe immer mit gleichbleibenden Mengen gefüllt werden.For example, in cleaning or disinfecting agents by adding a Cap of the agent to a bucket of water a constant concentration almost impossible, since neither the water bucket nor the cap always with constant amounts are filled.

Zusätzlich tritt noch der Effekt auf, dass oft eine zusätzliche Portion des Konzentrates zugegeben wird, um die Wirkung sicherzustellen, was aber nicht erforderlich ist.In addition, the effect still occurs that often an additional portion of the concentrate is added to ensure the effect, but this is not required.

Die Falschdosierung wird beim enfindungsgemäßen Verfahren dadurch vermieden, dass das Verhältnis der beiden Mengen konstant gehalten wird und die unterschiedlichen Konzentrationen der verdünnten Lösungen dadurch hergestellt werden, dass Konzentrate mit unterschiedlichen Konzentrationen eingesetzt werden. Für den Benützer ergibt sich daher der Vorteil, dass die beiden Mengen von Konzentrat und Lösungsmittel in fixen Größen zur Verfügung gestellt werden, und er immer nur diese beiden Mengen vereinigen muss.The incorrect dosage is avoided in the inventive method in that the Ratio of the two quantities is kept constant and the different Concentrations of the dilute solutions are prepared by concentrates be used with different concentrations. For the user results Therefore, the advantage that the two amounts of concentrate and solvent in fixed Sizes are provided, and he always consolidates only these two quantities got to.

Des weiteren können für die Herstellung der unterschiedlich konzentrierten verdünnten Lösungen einfachere Dosier- bzw. Portioniervorrichtungen verwendet werden, die konstante Durchflussraten bzw. Portionen mit konstanten Volumina abgeben.Furthermore, for the preparation of the differently concentrated dilute Solutions simpler dosing or portioning devices are used, the constant Release flow rates or portions with constant volumes.

Beispielsweise kann ein Liter einer zehnprozentigen Lösung dadurch hergestellt werden, dass 10 Zentiliter Konzentrat und 90 Zentiliter Verdünnungsmittel vermischt werden. Eine hiefür geeignete Portioniervorrichtung weist zwei Behälter mit den genannten Rauminhalten auf. Diese Portioniervorrichtung kann ebenso zur Herstellung einer fünfprozentigen Lösung verwendet werden, die 95 Zentiliter Verdünnungsmittel enthalten muss. In diesem Fall wird ein um die Hälfte vorverdünntes Konzentrat eingesetzt, da die durch die Portioniervorrichtung ausgegebenen 10 Zentiliter des vorverdünnten Konzentrates bereits die auf 95 Zentiliter fehlenden 5 Zentiliter des Verdünnungsmittels enthalten.For example, one liter of a ten percent solution can be made thereby that 10 centiliters of concentrate and 90 centiliters of diluent are mixed. A For this purpose, suitable portioning device has two containers with said space contents on. This portioning device may also be used to prepare a five percent solution which must contain 95 centiliters of diluent. In this case will a half vorverdünntes concentrate used because of the Portioning device already spent 10 centiliters of prediluted concentrate contain 5 centiliters of the diluent missing on 95 centiliters.

Für größere Mengen werden bevorzugt, wie erwähnt, Dosiervorrichtungen mit konstanten Durchflussmengen pro Zeiteinheit gewählt. Zwanzig Liter der oben angegebenen zehnprozentigen Lösung werden durch Dosiervorrichtungen mit Durchflussraten von zwei Litern und achtzehn Litern pro Minute in einer Minute abgefüllt. Zwanzig Liter einer fünfprozentigen Lösung werden ebenfalls in einer Minute mittels dieser Dosiervorrichtungen hergestellt, wenn das Konzentrat um die Hälfte vorverdünnt ist und bereits ein ein Liter Verdünnungsmittel enthält.For larger quantities it is preferred, as mentioned, to have metering devices with constant Flow rates selected per unit time. Twenty liters of the above ten percent Solution are by metering devices with flow rates of two liters and eighteen liters per minute in one minute. Twenty liters of a five percent Solution are also prepared in one minute by means of these dosing devices, if the concentrate is prediluted by half and already one liter of diluent contains.

Von Bedeutung ist das erfindungsgemäße Verfahren vor allem, da in ein- und derselben Dosier- oder Portioniervorrichtung unterschiedliche Mittel verdünnt werden Können, die üblicherweise nicht in derselben Verdünnung angewendet werden. Es ist nur notwendig, die verschiedenen Mittel in gleichen, in die Vorrichtung einsetzbaren, austauschbaren Flaschen oder Behältern anzubieten.Of importance, the inventive method is especially because in one and the same Dosing or portioning device can be diluted different means that usually not used in the same dilution. It is only necessary that various means in the same, can be used in the device, interchangeable bottles or containers.

Claims (6)

Verfahren zur Herstellung verdünnter Lösungen in unterschiedlichen Konzentrationen aus insbesondere verschiedenartigen Konzentraten, wobei jeweils eine Menge eines Konzentrates und eine Menge eines Verdünnungsmittels vermischt werden, dadurch gekennzeichnet, dass das Verhältnis der beiden Mengen konstant gehalten wird und die unterschiedlichen Konzentrationen der verdünnten Lösungen dadurch hergestellt werden, dass Konzentrate mit unterschiedlichen Konzentrationen eingesetzt werden.Process for the preparation of dilute solutions in different concentrations of, in particular, different concentrates, in which in each case an amount of a concentrate and an amount of a diluent are mixed, characterized in that the ratio of the two quantities is kept constant and the different concentrations of the dilute solutions are produced thereby, that concentrates with different concentrations are used. Verfahren zur Herstellung nach Anspruch 1, dadurch gekennzeichnet, dass die Konzentrate mit unterschiedlichen Konzentrationen durch eine Vorverdünnung der Konzentrate hergestellt werden.A process for the preparation according to claim 1, characterized in that the concentrates are prepared with different concentrations by a predilution of the concentrates. Verfahren zur Herstellung nach Anspruch 1 oder 2, dadurch gekennzeichnet, dass die beiden Mengen durch eine gleich lange Betätigung zweier Dosiervorrichtungen mit unterschiedlichen Durchflussmengen pro Zeiteinheit konstant gehalten werden.Process for the preparation according to claim 1 or 2, characterized in that the two quantities are kept constant by an equally long operation of two metering devices with different flow rates per unit time. Verfahren zur Herstellung nach Anspruch 1 oder 2, dadurch gekennzeichnet, dass die beiden Mengen durch eine zumindest einmalige Betätigung zweier Portioniervorrichtungen mit unterschiedlichen Volumina konstant gehalten werden.Process for the preparation according to claim 1 or 2, characterized in that the two quantities are kept constant by an at least one operation of two portioning devices with different volumes. Vorrichtung zur Herstellung verdünnter Lösungen in unterschiedlichen Konzentrationen aus insbesondere verschiedenartigen Konzentraten, wobei jeweils eine Menge eines Konzentrates und eine Menge eines Verdünnungsmittels vermischt werden, dadurch gekennzeichnet, dass zwei Dosiervorrichtungen mit unterschiedlichen Durchlassmengen pro Zeiteinheit vorgesehen sind.Device for the preparation of dilute solutions in different concentrations of particular different concentrates, wherein in each case an amount of a concentrate and an amount of a diluent are mixed, characterized in that two metering devices are provided with different flow rates per unit time. Vorrichtung zur Herstellung verdünnter Lösungen in unterschiedlichen Konzentrationen aus insbesondere verschiedenartigen Konzentraten, wobei jeweils eine Menge eines Konzentrates und eine Menge eines Verdünnungsmittels vermischt werden, dadurch gekennzeichnet, dass zwei Portioniervorrichtungen mit unterschiedlichen Volumina vorgesehen sind.Device for producing dilute solutions in different concentrations, in particular different concentrates, wherein in each case an amount of a concentrate and an amount of a diluent are mixed, characterized in that two portioning devices are provided with different volumes.
EP05004665A 2004-03-05 2005-03-03 Method and apparatus for the preparation of diluted solutions Withdrawn EP1570899A3 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AT3782004 2004-03-05
AT0037804A AT500486B1 (en) 2004-03-05 2004-03-05 METHOD FOR PRODUCING DILUTED SOLUTIONS

Publications (2)

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EP1570899A2 true EP1570899A2 (en) 2005-09-07
EP1570899A3 EP1570899A3 (en) 2006-01-04

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EP05004665A Withdrawn EP1570899A3 (en) 2004-03-05 2005-03-03 Method and apparatus for the preparation of diluted solutions

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EP (1) EP1570899A3 (en)
AT (1) AT500486B1 (en)

Families Citing this family (1)

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EP2401502B1 (en) * 2009-02-27 2018-10-31 Waters Technologies Corporation Automated dilution for liquid chromatography

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Also Published As

Publication number Publication date
EP1570899A3 (en) 2006-01-04
US20090057337A1 (en) 2009-03-05
AT500486A1 (en) 2006-01-15
AT500486B1 (en) 2006-11-15
US20050194007A1 (en) 2005-09-08

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