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EP1381557B1 - Filling head - Google Patents

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Publication number
EP1381557B1
EP1381557B1 EP02718238A EP02718238A EP1381557B1 EP 1381557 B1 EP1381557 B1 EP 1381557B1 EP 02718238 A EP02718238 A EP 02718238A EP 02718238 A EP02718238 A EP 02718238A EP 1381557 B1 EP1381557 B1 EP 1381557B1
Authority
EP
European Patent Office
Prior art keywords
product
liquid
dispensing
semiliquid
valve
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP02718238A
Other languages
German (de)
French (fr)
Other versions
EP1381557A1 (en
Inventor
Jean Pierre Solignac
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Individual
Original Assignee
Individual
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Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of EP1381557A1 publication Critical patent/EP1381557A1/en
Application granted granted Critical
Publication of EP1381557B1 publication Critical patent/EP1381557B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65BMACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B39/00Nozzles, funnels or guides for introducing articles or materials into containers or wrappers
    • B65B39/001Nozzles, funnels or guides for introducing articles or materials into containers or wrappers with flow cut-off means, e.g. valves
    • B65B39/004Nozzles, funnels or guides for introducing articles or materials into containers or wrappers with flow cut-off means, e.g. valves moving linearly
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B67OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
    • B67CCLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
    • B67C3/00Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
    • B67C3/02Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
    • B67C3/22Details
    • B67C3/26Filling-heads; Means for engaging filling-heads with bottle necks
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B67OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
    • B67CCLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
    • B67C3/00Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
    • B67C3/02Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
    • B67C3/22Details
    • B67C3/26Filling-heads; Means for engaging filling-heads with bottle necks
    • B67C3/2608Filling-heads; Means for engaging filling-heads with bottle necks comprising anti-dripping means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B67OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
    • B67CCLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
    • B67C3/00Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
    • B67C3/02Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
    • B67C3/22Details
    • B67C3/28Flow-control devices, e.g. using valves

Definitions

  • the present invention relates to a device for dispensing and precision dosing pasty products with high or low surface tension, which can also be used for the dosed dispensing of liquid or semi-liquid products with high or low surface tension or still pulverulent products with high or low agglomeration power.
  • the same problems are found to a lesser degree for the dosed distribution of liquid or semi-liquid products.
  • the dose tails are generally in the form of more or less large drops.
  • patent application US 5,150,743A discloses a dispensing and dosing device according to the preamble of claim 1.
  • the actuating mechanism of the valve, to function properly is periodically lubricated.
  • the actuating mechanism is mounted in a chamber separated from the product passageway in the device by sealing elements.
  • Valve devices that is to say shutter member movable perpendicular to the seat
  • valve devices are well suited if is preferred the possibility of a precise adjustment of the flow while maintaining a laminar flow
  • corollary valve arrangements known imply a product passageway, bent in particular at the seat.
  • These elbows are factors of loss of loads and for pasty products can constitute niches of product retention.
  • Such a disadvantage is not found in valve devices (that is to say shutter member movable parallel to the seat) which allow the realization of a rectilinear passageway.
  • this type of configuration can generate turbulence downstream of the valve that can transform a laminar flow turbulent flow, likely to affect the accuracy of the assay.
  • the present invention aims to solve the aforementioned problems by providing a universal device that can be used for the metered dispensing of all types of products they are pasty, liquid, semi-liquid or powder with which it is possible to to obtain a very high degree of precision in the metering with simple mechanical means, robust and machined with the tolerances of the current mechanics.
  • Another object of the present invention is the implementation of a device for dispensing and dosing of pasty products which allows to combine the precision of the dosage and the speed of distribution of the product.
  • Another object of the present invention is the production of a device for dispensing and dosing pasty products whose closure member is constituted by a valve and for which the pressure losses have been reduced.
  • Another object of the present invention is the production of a device for dispensing and dosing pasty, liquid or semi-liquid products with a high surface tension or pulverulent products with high agglomeration power.
  • Another objective of the present invention is to obtain a very high degree of precision in the determination of pasty, liquid, semi-liquid and powdery products, this degree of precision being able to reach a tenth of a milligram.
  • Another object of the present invention is the production of a device for the dispensing and dosing of pasty, liquid or semi-liquid products with a high surface tension or of pulverulent products with a high agglomeration power which, on the one hand, ensures separation of the dose tail without use of mechanical organs such as doctor blades and others coming into contact with the product and secondly the fall of this dose tail in the container in which is dispensed the dose.
  • the device for the dosed dispensing of pasty or liquid or semi-liquid or powdery products comprises a device body in which is formed a conduit for the passage of the product from an introduction orifice to a delivery nozzle of the product. in metered quantities.
  • a valve seat is formed in said conduit and a valve is mounted therein so as to be slidable thereon and can be applied against the valve seat or be spaced from the valve seat to either prohibit the delivery of the product or allow this deliverance.
  • the valve is provided with a valve stem which is slidably mounted in a guide bore and cooperates with a drive mechanism for actuating the valve away from the seat or towards the valve seat
  • the product passageway comprises a straight segment of passage of the product in which segment is disposed the valve seat and extend axially and in all the valve and the valve stem and in which segment at least partially penetrates the actuating mechanism of the valve, this the mechanism being in contact with the product so that the mechanical connection between the valve stem and the actuating mechanism is also in contact with the product and is lubricated by the product itself
  • the actuating mechanism of the valve comprises, at least one elastic member acting as a thrust on the valve and biasing the latter towards the seat and thus towards a closed position and on the other hand actuating geometry, guided axially in a bore of the device body, which bore is transverse to the rectilinear segment of conduit and opens into said segment, said rod coming into contact with the valve stem to act in thrust on the latter, the contact between the valve stem and the actuating
  • This provides a particularly simple and inexpensive actuation mechanism.
  • the oblique sliding surface forms with the geometric axis of displacement of the actuating rod, an acute angle of value less than 45 degrees. Thanks to this characteristic, a given displacement of the actuating rod will be accompanied by a less displacement of the valve. This results in a reduction effect of the movement of the valve leading to a better positional accuracy of the latter.
  • the guide bore of the actuating rod is perpendicular to the passage section of the product.
  • the straight section of passage of the product is vertical.
  • the product passage is vertical and extends rectilinearly from an inlet of the product to a delivery port of the latter.
  • the motor member ensuring the displacement of the actuating rod is external to the device and independent of the latter.
  • the dispensing nozzle of the product is associated with a device for blowing a fluid under pressure to detach, under the effect of the blast or under the effect of the depression or the pressure resulting, the dose tail suspended from the delivery nozzle and promote the fall of this dose tail to the container in which was dispensed the dose.
  • the dose tail is separated from the dispensing nozzle, without the use of mechanical means, solely by fluids which may be inert with respect to the product to be dispensed but which may, if appropriate, react with them if this effect is research. It is also understood that the dose tail is systematically included in the dose which guarantees the accuracy of the dosage. Moreover, it is ensured, after each distribution, the cleaning of the outer faces around the dispensing nozzle, this avoids any breakable deposit at this level which could possibly obstruct the nozzle or pollute subsequent distributions.
  • the fluid under pressure is blown towards the dose tail in the form of a pulse or a short jet, of an appropriate intensity, to ensure a rapid separation, compatible with rates of high distribution.
  • the power of the jet combined with an appropriate orientation in the direction of flow of the product or slightly inclined relative to the latter, creates a depression around the tail of the dose generating a suction phenomenon of this last leading first to its separation from the dispensing nozzle and its controlled drop towards the container.
  • the direction of the jet will be radial to the nozzle or slightly inclined relative to a radial plane to provide shear separation.
  • the separation jet is no longer pulsed, but continuously.
  • the blowing device is provided with a nozzle for delivering a fluid under pressure and said nozzle is formed around the product delivery nozzle.
  • the fluid is thus distributed around the dose tail, and this distribution limits the deviation of the drop of the dose tail towards the container.
  • the device according to the invention for the precise dispensing and dosing, of the order of one-tenth of a milligram, of pasty products that may have a high surface tension or of liquid, semi-liquid products or products pulverulent materials that can exhibit a high agglomeration power, comprises a device body 1 of parallelepiped shape, in which is formed a conduit 2 for the passage of the product from an introduction orifice 3, to a nozzle 4 of product delivery in metered quantities , under which is disposed a not shown container, provided to collect the dose delivered by the device.
  • the introduction orifice 3 will be connected by a suitable conduit to a supply of product to be dispensed, this reserve may be arranged at a higher level relative to the device to allow a gravity flow of the product to said device. This reserve may also be pressurized to force the movement of the product to the device, it may also provide a pump between the reserve and the device for drawing the product into the reserve and back in the device.
  • the duct 2 has a rectilinear segment of the product passage which segment by considering the direction of passage of the product, a rectilinear vertical downstream product passage section, a rectilinear vertical cross section of product passage.
  • a rectilinear upright vertical section of product passage connects to said rectilinear segment.
  • This upstream section may be laterally offset from the median section and be connected thereto by a bend section.
  • the sections, median and downstream, extend mutually axially aligned.
  • the upstream section as can be seen in Figure 1 may also be located in the axial extension of the middle section. In this case, the three sections are axially aligned, which minimizes the pressure losses in the product passage duct. It may be noted that this duct extends vertically between the inlet orifice and the delivery orifice which facilitates the gravity flow of the product through the device.
  • valve seat 5 At low spacing of the delivery nozzle 4 is formed in the downstream section of the conduit 2, a valve seat 5. This seat, of frustoconical shape, is crossed by the downstream section of the duct. As can be seen, the downstream section downstream of the seat 5 has a reduced diameter relative to the diameter of the upstream section.
  • a valve 6, hemispherical or conical is mounted in the duct 2 so as to slide to be applied against the seat 5 and prohibit the delivery of the product or be removed from this seat and allow this delivery.
  • the duct immediately upstream of the seat 5 may have a frustoconical shape. The valve, between its closed position and opening moves in this frustoconical shape.
  • valve 6 is provided with a straight vertical valve stem 7, extending axially in the middle section of the duct 2, this valve stem cooperating with a mechanism for actuating the valve 6 in spacing from the seat 5 or towards the seat 5, this actuating mechanism penetrating at least partly into the rectilinear segment of product passage and coming into contact with the product so that the mechanical connection between the valve stem and the mechanism the actuator is also in contact with the product and is lubricated by the product itself.
  • the valve stem 7 has a diameter smaller than the diameter of the conduit 2.
  • valve stem 7 is slidably mounted in the axial through bore of a guide sleeve 19 in the form of a disc, mounted in blocking in the middle section of the passage conduit.
  • guide sleeve 19 extends transversely in the passage section and comprises, around the guide bore, through-holes for the passage of the product.
  • valve stem 7 is slidably mounted in a bore 7a formed in the device body 1, in the axial extension of the middle section of the conduit 2.
  • the guide bore will be long enough to avoid any risk of jamming at this level.
  • a seal may be disposed in the bore 7a around the valve stem to prevent product backflow into the bore and ensure sealing but preferably the bore is blind, the quality of the guide of the tail of valve in the bore is of the type H7-g6 for example and no seal is used. It is thus allowed to flow back deliberately to the bottom of the bore 7a, this reflux occurring in the form of a film whose interest is to ensure the lubrication of the guide.
  • Pollution of the product to be distributed by the amount of product contained in the bore 7a is not to be feared because, firstly, because the device is used only for the distribution of a single product and on the other hand, that it undergoes a complete cleaning after each distribution cycle.
  • the mechanism for actuating the valve comprises, on the one hand, at least one spring-like elastic member 8 acting in thrust on the valve 6 and urging the latter towards the seat 5, therefore to a closed position and on the other hand an actuating rod 9, guided axially in a bore 10 of the device body, which bore is transverse to the straight segment of conduit and opens into said segment.
  • this guide bore 10 is perpendicular to the median section of the conduit 2 and opens into the latter.
  • the actuating rod 9 comes into contact with the valve stem 7 and acts in thrust on the latter, the contact between the valve stem and the actuating mechanism being established by two sliding surfaces 11, 20 of which one 11 is formed on the valve stem 7 and the other 20 on the actuating rod 9, both said surfaces 11, 20 being located in the rectilinear segment of the product and being in contact with said product.
  • At least one of these surfaces is flat and oblique with respect to the geometric axis of displacement of the valve 6 between its open and closed positions so that when the actuating rod 9 is moved in the direction of insertion into the device body, the valve 9 is spaced from its seat under the effect of the thrust exerted by the sliding surface 20 of the rod 9 on the sliding surface 11 of the valve stem and of course under the effect of the sliding movement of the two surfaces 11, 20 one over the other. It should be noted that the spacing movement of the valve 6 takes place against the thrust action exerted by the elastic member 8 on the valve 7. On the other hand, during the reverse movement of the rod 11, the thrust of the spring 8 causes the valve to move towards the valve seat 5.
  • the elastic member 8 is mounted around the valve stem, in compression between the valve and the centering sleeve.
  • the resilient member 8 is mounted in compression between the bottom of the bore 7a and the tail 7 valve.
  • the oblique sliding surface may be provided on the actuating rod 9 or on the valve stem, the other surface may or may not have the same obliqueness in order to to obtain a contact and a sliding plan on plane less subject to wear than a contact and a slip, line on plan.
  • both surfaces 11, 20 are both oblique.
  • the rod 9 is actuated in axial sliding by a motor member 9a external to the body of the device.
  • This rod 9 thus has a portion external to the body of the device with which cooperates in axial thrust the motor member 9a.
  • This drive member 9a can be fixed to the body of the device or be independent of the device and not attached thereto.
  • This drive member 9a thus controls the movement of the rod 9 and its degree of depression in the bore 9.
  • the drive member 9a controls the movement of the valve and the degree of opening of the latter.
  • the valve by these means can be placed in a position of total opening allowing the flow of the product at a maximum flow rate but also in an intermediate position, between the open position and closing, chosen according to the desired flow rate .
  • the motor member also controls the return movement of the rod 9 and thus the way the valve is brought into the closed position.
  • This motor unit will be controlled and controlled by a control unit.
  • the driving movement of the rod 9 in the bore 10 towards the valve stem takes place against the action of an elastic return member 12 mounted in compression in the bore 10 between a shoulder of the latter and a shoulder of the rod 9.
  • the rod 9 has a shape of push pin 9b of reduced diameter.
  • This form of thrust finger 9b is provided at the end portion of one of the two sliding surfaces, and the resilient return member 12, in the form of a coil spring, is mounted around this thrust pin shape.
  • the bore 10 is formed in part by the through bore of a removable piece 9c for abutment and sealing, engaged in screwing in a tapping of the device body 1.
  • the bore of this piece forms a stop shoulder 9d against which abuts an abutment shoulder 9e of the rod 9.
  • the oblique sliding surface forms with the geometric axis of displacement of the actuator, an acute angle of less than 45 degrees. Thanks to this characteristic, a given displacement of the actuating rod will be accompanied by a less displacement of the valve. This gives a reduction effect of the movement of the valve. Thanks to this reduction effect, a better positional accuracy of the valve is obtained as well as a better control of the flow of the product. It goes without saying that the inclination of the sliding surfaces is compatible with the coefficient of friction of one over the other. It should be recalled that these two surfaces are in contact with the product so that the latter by being deposited on these surfaces forms a film capable of reducing this coefficient of friction and consequently the wear of the two sliding surfaces.
  • the valve stem 7 is provided with a through-hole in a diametrical direction, the sliding surface 11 specific to the valve stem being constituted by the upper face (upstream face, considering the direction of the valve). product flow) from this light.
  • This light is further delimited by two plane faces parallel to each other and parallel to the longitudinal axis of the valve stem and by a lower face perpendicular or oblique to said axis.
  • the thrust finger shape 9b has two parallel flats, coming opposite the lateral faces of the through-light.
  • the push pin shape 9b of the latter is constrained by the stop shoulders 9d, 9th, to remain always in the crossing light.
  • the flats of this form of thrust finger 9b and the lateral faces of the light together constitute the angular setting.
  • the sliding surface 20 that the finger has is oblique and is opposite the sliding surface 11.
  • the sliding surface 11 is formed in a wear piece 22 made of PTFE locked in the valve stem 7.
  • this valve stem is tubular and presents in a diametrical plane. two opposite lights offset in height.
  • the wear part 22 is intended to be forced into the valve stem and is in the form of a cylinder.
  • This wear part according to one of its diameters will be equipped with the above-mentioned through-light, the sliding surface 11 will always be constituted by the upper face (upstream face considering the direction of flow of the product) of this light .
  • the light of the wear part 22 will be brought opposite the slots of the valve stem.
  • a device 13 for blowing a fluid under pressure To separate from the delivery nozzle 4, the dose tail which could adhere under the effect of the action of the surface tension forces, is provided a device 13 for blowing a fluid under pressure.
  • the pressurized fluid can be introduced into the conduit 2 downstream of the seat 5 so as to push the dose tail by pushing but preferably, the pressurized fluid jet delivered by the device 13 is external to the conduit 4.
  • the blowing device 13 is external to the duct 2 and to the nozzle 4.
  • the fluid under pressure is blown towards the dose tail in the form of a pulse of relatively high intensity.
  • the blowing device 13 is equipped with a nozzle 14 for delivering the fluid under pressure.
  • This nozzle is formed around the delivery nozzle of the product so that the fluid output of this nozzle can be distributed around the dose tail.
  • the delivery nozzle 4 of the product is preferably formed in a nozzle 15, this nozzle is provided with the seat 5.
  • the nozzle 15 is removably attached to the device body 1.
  • the nozzle 15 will be equipped with a threaded cylindrical portion and will be engaged by this threaded cylindrical portion in a suitable thread, made in the device body around the middle section of the conduit 2. This arrangement allows the disassembly of the valve 6 for cleaning.
  • Figure 1 it can be seen that the nozzle 15 bears against the guide sleeve 19 and maintains the latter against a shoulder formed in the middle section of the conduit.
  • the nozzle 15 upstream of the delivery port may receive a gate 21 adapted to retain drops of liquids that may disturb the assay.
  • the nozzle 15, upstream of this grid may have a flare to "quiet" the flow.
  • the nozzle 14 for delivering the fluid is formed by the lower, circular opening of a chamber 16 formed around the nozzle 15 and delimited by an envelope 16a fixed with respect to said nozzle.
  • the envelope 16a and the nozzle 15 are coaxial.
  • the casing 16 is equipped with at least one piercing 17 for introducing the fluid under pressure into the chamber 16.
  • This piercing is connected, by a suitable conduit of the device 13, to a source of pressure fluid installed remotely or proximity of the device.
  • On this pipe may be installed a solenoid valve controlled by a programmable controller or any other equivalent means.
  • the outer surface of the nozzle 15 is frustoconical in shape, the small base of the truncated cone and the nozzle 14 for delivering the fluid under pressure being arranged close to each other.
  • the outer surface of the nozzle 15 is cylindro-conical, the delivery nozzle 14 of the pressurized fluid being located in this case in the immediate vicinity of the free end of the cylindrical portion.
  • This cylindrical surface allows to a certain extent the orientation of the pressurized fluid jet substantially in the product flow axis and limits the shearing effect that the fluid can produce on the dose tail.
  • the delivery nozzle of the product is formed at the end of the cylindrical portion.
  • the inner face of the casing 16a has a frustoconical portion whose small base is formed by the nozzle 14 for delivering the fluid under pressure.
  • the frustoconical portion of the inner face of the envelope 16a has an apex angle greater than the angle at the apex of the frustoconical portion of the outer surface of the nozzle 15. This provision allows to remove the internal face of the casing 16a of the outer face of the nozzle 15 to provide a chamber 16 of sufficient volume.
  • the top of the cone corresponding to the frustoconical shape that presents the inner face of the casing 16 is located on the axis of symmetry of the duct 2 near the nozzle 4 for delivering the product.
  • this vertex is located downstream of this nozzle in order to superimpose the driving effect of the dose tail a slight shearing effect.
  • the top of the cone may be located upstream of the delivery nozzle 4 of the product.
  • the envelope 16a has a cylindrical portion in the extension of the frustoconical portion.
  • This cylindrical portion may be provided with at least one through hole 17 for introducing the pressurized fluid into the chamber 16.
  • This drilling may also be performed in the frustoconical portion of the envelope.
  • In the accompanying figures is shown only one through hole, but alternatively may be provided several equidistributed holes, to better balance the jet of fluid output of the nozzle 14 and avoid any deviation of the latter.
  • the or each through bore 17 is disposed facing the conical portion of the outer surface of the nozzle 15. Still according to the preferred embodiment, the or each through hole occupies a radial position, but this position may be inclined by example to the delivery nozzle 14.
  • the respective positions of the product delivery nozzle and the delivery of the fluid under pressure are adjustable relative to each other.
  • the casing 16a of the blowing device 13 is fixed by screwing on the nozzle 15.
  • This arrangement makes it possible to adjust the position of the nozzles very precisely, in the embodiment shown in the figures, the nozzle 14 is slightly above the bore 4. This adjustment possibility allows a close adaptation of the blowing device to the particularities of the product to be dispensed. Thus, these respective positions may evolve according to the physical properties of the products to be dispensed, the desired effect being the separation of the dose tail.
  • this fluid may be air.
  • this fluid may be in the liquid state in this case, it may be liquid nitrogen.
  • This fluid may be in the gaseous state at room temperature but alternatively, it may be in the liquid state at room temperature.
  • the fluid used may be inert with respect to the product to be dispensed and possibly products already poured into the container or, conversely, it may react with this or these depending on the desired physical or chemical effect.
  • this device may be provided with several nozzles, mounted coaxially in one another spaced apart from each other to form annular chambers with circular opening forming nozzles. This arrangement allows the simultaneous distribution of several products to be associated in the same composition.
  • the casing 16a of the blowing device 13 is mounted around the outermost nozzle.
  • the device as described is provided with holes 18 for attachment to a suitable support, this support may be in the form of a tray.
  • This tray may receive several devices of the aforementioned kind.
  • the device may be equipped with indexing holes, not shown, for cooperating in shape interlocking with indexing fingers. Such a configuration requires only a single motor 9a.
  • the present invention provides a particularly simple solution to the problem of dosing pasty products with high surface tension, the tests carried out have demonstrated that accuracies of the order of a tenth of a milligram are perfectly conceivable.

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Basic Packing Technique (AREA)
  • Containers And Packaging Bodies Having A Special Means To Remove Contents (AREA)
  • Supply Of Fluid Materials To The Packaging Location (AREA)
  • Devices For Dispensing Beverages (AREA)
  • Nozzles (AREA)
  • Formation And Processing Of Food Products (AREA)
  • Glass Compositions (AREA)
  • Vehicle Body Suspensions (AREA)
  • Manufacturing Of Electric Cables (AREA)
  • Coating Apparatus (AREA)

Abstract

A device for distributing and dosing pasty, liquid, semi-liquid or pulverulent products comprises a valve body which is provided with a through channel for moving the product from a feed opening to a delivery nozzle in dosed quantities. A valve seat is formed in the channel and a valve is mounted in the channel. The product through channel comprises a rectilinear product, passage segment in which the valve seat is disposed and in which the valve and the valve rod extend axially and in full. Moreover, the valve drive mechanism penetrates the product passage segment at least in part. The drive mechanism is in contact with the product such that the mechanical link between the valve rod and the drive mechanism is also in contact with the product and is lubricated by the product.

Description

La présente invention a pour objet un dispositif pour la distribution et le dosage de précision de produits pâteux à forte ou à faible tension superficielle, pouvant être utilisé aussi pour la distribution dosée de produits liquides ou semi-liquides à forte ou à faible tension superficielle ou encore de produits pulvérulents à fort ou faible pouvoir d'agglomération.The present invention relates to a device for dispensing and precision dosing pasty products with high or low surface tension, which can also be used for the dosed dispensing of liquid or semi-liquid products with high or low surface tension or still pulverulent products with high or low agglomeration power.

Les industries cosmétologiques, pharmaceutiques, chimiques et autres, exigent des degrés de précision très importants de l'ordre du demi-milligramme pour le dosage des différents constituants entrant dans les diverses compositions. La réalisation manuelle de ces compositions avec les précisions requises est particulièrement longue et fastidieuse et s'avère incompatible avec les productions en série. Un autre défaut des méthodes manuelles est qu'elles peuvent donner lieu à de multiples erreurs de dosage ou de compositions.Cosmetic, pharmaceutical, chemical and other industries require very high levels of precision of the order of half a milligram for the determination of the various constituents entering the various compositions. The manual production of these compositions with the required precision is particularly long and tedious and proves incompatible with mass production. Another defect of the manual methods is that they can give rise to multiple dosing errors or compositions.

L'état de la technique propose de nombreuses solutions pour l'automatisation de la fabrication des diverses compositions. Ainsi on connaît des dispositifs pour la distribution en quantités dosées de liquides avec lesquels il est possible de réaliser diverses compositions de manière automatisée. Ces dispositifs sont spécifiquement conçus pour la distribution et le dosage de produits liquides ou semi-liquides, et se prêtent peu à la distribution dosée de produits pâteux à forte tension superficielle ainsi qu'à la distribution dosée de produits pulvérulents. Un dispositif de ce genre est notamment connu du brevet EP 929 498 du demandeur. Ce dispositif présente l'avantage sur ceux de l'état de la technique de doser les produits avec une précision de l'ordre du demi-milligramme.The state of the art offers numerous solutions for automating the manufacture of the various compositions. Thus, there are known devices for dispensing dosed quantities of liquids with which it is possible to produce various compositions in an automated manner. These devices are specifically designed for the dispensing and dosing of liquid or semi-liquid products, and are not suitable for dosed dispensing of pasty products with a high surface tension and for the dosing of powdered products. A device of this type is known in particular from patent EP 929 498 of the applicant. This device has the advantage over those of the state of the art to dose the products with a precision of the order of half a milligram.

On connaît aussi des dispositifs pour la distribution en quantités dosées de produits pulvérulents. Un des inconvénients de ces dispositifs réside dans le fait qu'ils ne peuvent pas être utilisés pour le dosage de liquides ou de produits pâteux. Par ailleurs leur manque de précision limite leur champ d'application. La demande de brevet WO 98/35896 du demandeur apporte une solution efficace au manque de précision, cependant ce dispositif ne peut distribuer que des produits pulvérulents.Devices are also known for dispensing metered quantities of powdery products. One of the disadvantages of these devices lies in the fact that they can not be used for dosing liquids or pasty products. Moreover, their lack of precision limits their scope. The applicant's patent application WO 98/35896 provides an effective solution to the lack of precision, however this device can only distribute powdery products.

On connaît aussi des dispositifs pour la distribution de produits pâteux. S'il est possible d'utiliser certains d'entre eux pour la distribution de liquides, leur principal inconvénient réside dans leur manque de précision. Ceci tient essentiellement au fait que la tension superficielle que présentent les produits pâteux, s'oppose à l'écoulement libre des queues de doses, ces dernières se présentent généralement sous la forme de filaments plus ou moins longs et plus ou moins épais. Ces queues de dose, de valeurs pondérales variables d'une distribution à l'autre, demeurent, dans la plupart des cas, suspendues à la buse de distribution. Il est donc important de séparer la queue de dose de la buse de distribution pour compléter le dosage et assurer la précision de ce dernier. On a pensé utiliser des organes de coupe ou de raclage pour assurer cette séparation, mais l'utilisation de tels éléments ne résout en rien le problème, la tension superficielle du produit pâteux étant telle que la queue de dose reste accrochée à ces organes. On pourrait assurer le dosage par pesage du récipient dans lequel est déversé le produit. Mais en raison de l'adhérence aléatoire de la queue de dose à la buse de distribution, la précision du dosage pourrait se trouver anéantie par la chute inopinée de cette queue de dose dans le récipient. On pourrait aussi chasser par soufflage la queue de dose pour éviter sa chute dans le récipient, mais une telle solution ne peut être adoptée que pour des produits courants et de coûts réduits. Pour des produits particulièrement coûteux, comme ceux à base d'huiles essentielles, utilisés dans le domaine de la parfumerie ou contenant des principes actifs comme ceux utilisés dans le domaine de la cosmétologie ou de la pharmacologie, une telle solution entraînerait des pertes financières substantielles et avec certains types de produits, une pollution importante de l'environnement immédiat du poste de distribution.Devices for the distribution of pasty products are also known. If it is possible to use some of them for the distribution of liquids, their main drawback lies in their lack of precision. This is mainly because the surface tension of the pasty products, is opposed to the free flow of the tails of doses, the latter are generally in the form of more or less long filaments and more or less thick. These dose tails, weight values variable from one distribution to another, remain, in most cases, suspended from the dispensing nozzle. It is therefore important to separate the dose tail from the dispensing nozzle to complete the dosage and ensure the accuracy of the dispensing nozzle. It has been thought to use cutting or scraping members to ensure this separation, but the use of such elements does not solve the problem, the surface tension of the pasty product being such that the dose tail remains attached to these organs. We could ensure the dosing by weighing the container into which the product is poured. But because of the random adherence of the dose tail to the dispensing nozzle, the precision of the dosage could be annihilated by the unexpected fall of this tail of dose in the container. It would also be possible to blow blow the dose tail to prevent it from falling into the container, but such a solution can only be adopted for current products with reduced costs. For particularly expensive products, such as those based on essential oils, used in the field of perfumery or containing active ingredients such as those used in the field of cosmetology or pharmacology, such a solution would entail substantial financial losses and with certain types of products, significant pollution of the immediate environment of the distribution station.

On retrouve les mêmes problèmes dans un degré moindre pour la distribution dosée des produits liquides ou semi-liquides. Pour de tels produits, les queues de dose se présentent généralement sous la forme de gouttes plus ou moins grosses.The same problems are found to a lesser degree for the dosed distribution of liquid or semi-liquid products. For such products, the dose tails are generally in the form of more or less large drops.

Finalement, la demande de brevet US 5 150 743A décrit un dispositif de distribution et dosage selon le préambule de la revendication 1.Finally, patent application US 5,150,743A discloses a dispensing and dosing device according to the preamble of claim 1.

L'exigence d'une précision très élevée de l'ordre du demi milligramme, notamment pour le dosage de produits pâteux s'avère actuellement incompatible avec des cadences élevées de production. En effet le principal paramètre qui influe directement sur ces cadences est la valeur du débit de délivrance de ces produits. Un débit élevé implique avec les dispositifs actuels des vitesses d'écoulement élevées qui augmentent grandement l'énergie cinétique de l'écoulement. Il faut savoir que pour un dosage de précision, le récipient destiné à recevoir l'écoulement est placé sur une balance de précision dont la mesure peut se trouver fortement perturbée par la dissipation brusque de l'énergie cinétique de l'écoulement lors de l'impact de ce dernier avec le récipient ou avec le produit déjà contenu dans ce récipient. Le demandeur a déjà résolu ce problème pour le dosage de produits liquides et pulvérulents mais les solutions utilisées ne sont pas utilisables pour le dosage de produits pâteux.The requirement of a very high precision of the order of half milligram, especially for the dosage of pasty products is currently incompatible with high production rates. Indeed, the main parameter that directly influences these rates is the value of the delivery rate of these products. High flow rates imply high velocities with current devices that greatly increase the kinetic energy of the flow. It should be noted that for a precision dosing, the container intended to receive the flow is placed on a precision balance whose measurement can be greatly disturbed by the sudden dissipation of the kinetic energy of the flow during the flow. impact of the latter with the container or with the product already contained in this container. The applicant has already solved this problem for the dosing of liquid and powdery products, but the solutions used can not be used for the dosing of pasty products.

L'obtention d'un degré élevé de précision pour le dosage, suppose une parfaite maîtrise du degré d'ouverture de l'élément obturateur du dispositif de dosage. Typiquement dans les systèmes connus, cet élément obturateur est constitué par une soupape dont la queue coopère avec un mécanisme d'actionnement. Pour un contrôle rigoureux du degré d'ouverture de la soupape, l'état de la technique enseigne notamment l'utilisation de mécanisme d'actionnement sous forme de vis et écrou entraîné par l'arbre de sortie d'un moteur du genre électrique. De tels moyens bien que simples en soit compliquent la réalisation du dispositif de dosage.Obtaining a high degree of precision for the assay, assumes a perfect control of the degree of opening of the shutter element of the metering device. Typically in known systems, this shutter member is constituted by a valve whose tail cooperates with an actuating mechanism. For a rigorous control of the degree of opening of the valve, the state of the art teaches including the use of actuating mechanism in the form of screw and nut driven by the output shaft of a motor of the electric kind. Such means, although simple, are complicating the production of the metering device.

Le mécanisme d'actionnement de la soupape, pour fonctionner correctement est périodiquement lubrifié. Pour éviter toute pollution du produit à délivrer par les fluides de lubrification, le mécanisme d'actionnement est monté dans une chambre séparée de la voie de passage du produit dans le dispositif par des éléments d'étanchéité. Une telle solution communément utilisée complique la réalisation du dispositif sans écarter totalement le risque de pollution en raison de l'usure obligée des éléments d'étanchéité.The actuating mechanism of the valve, to function properly is periodically lubricated. To prevent any pollution of the product to be delivered by the lubricating fluids, the actuating mechanism is mounted in a chamber separated from the product passageway in the device by sealing elements. Such a commonly used solution complicates the realization of the device without completely eliminating the risk of pollution due to the wear required sealing elements.

Un autre facteur pouvant intervenir dans la précision du dosage est la facilité d'écoulement du produit au travers du dispositif. Des dispositifs à soupape (c'est-à-dire à organe d'obturation mobile perpendiculairement au siège) conviennent bien si est privilégiée la possibilité d'un réglage précis du débit tout en maintenant un écoulement laminaire, mais en corollaire les dispositions à soupapes connues impliquent une voie de passage du produit, coudée notamment au niveau du siège. Ces coudes sont facteurs de pertes de charges et pour des produits pâteux peuvent constituer des niches de rétention de produit. Un tel inconvénient ne se retrouve pas dans des dispositifs à vanne (c'est-à-dire à organe d'obturation déplaçable parallèlement au siège) qui permettent la réalisation d'une voie de passage rectiligne. Cependant bien que le débit puisse être ajusté par positionnement adapté de la vanne, ce type de configuration peut engendrer en aval de la vanne des turbulences pouvant transformer un écoulement laminaire en écoulement turbulent, susceptible d'altérer la précision du dosage.Another factor that may affect the accuracy of the assay is the ease of flow of the product through the device. Valve devices (that is to say shutter member movable perpendicular to the seat) are well suited if is preferred the possibility of a precise adjustment of the flow while maintaining a laminar flow, but corollary valve arrangements known imply a product passageway, bent in particular at the seat. These elbows are factors of loss of loads and for pasty products can constitute niches of product retention. Such a disadvantage is not found in valve devices (that is to say shutter member movable parallel to the seat) which allow the realization of a rectilinear passageway. However, although the flow rate can be adjusted by appropriate positioning of the valve, this type of configuration can generate turbulence downstream of the valve that can transform a laminar flow turbulent flow, likely to affect the accuracy of the assay.

Enfin, l'exigence d'un rendement élevé dans la production de compositions à partir de différents produits délivrés en quantités parfaitement dosées suppose que l'ensemble de ces produits et leurs dispositifs de distribution soient regroupés au sein d'une même unité. Ces dispositions, pour des dispositifs de délivrance de liquide et de poudre sont décrites dans les brevets antérieurs du demandeur. L'intérêt de ces dispositions antérieures est qu'elles ne prévoient qu'un seul moteur pour actionner les différents dispositifs de dosage, lesquels avec les réservoirs de produits associés, sont montés sur une structure mobile, par exemple un plateau tournant, pour être amené face au moteur d'actionnement. Cette façon de faire simplifie la réalisation de l'ensemble, et en facilite la commande. L'intérêt est de pouvoir utiliser une telle configuration pour des dispositifs de délivrance de produit pâteux, mais les dispositifs à soupape de l'art antérieur ne se prêtent pas à une telle organisation.Finally, the requirement of a high yield in the production of compositions from different products delivered in perfectly dosed quantities assumes that all of these products and their dispensing devices are grouped together within the same unit. These arrangements for liquid and powder delivery devices are described in the applicant's prior patents. The advantage of these prior arrangements is that they provide only one motor to operate the different metering devices, which with the associated product tanks, are mounted on a mobile structure, for example a turntable, to be brought facing the actuating motor. This way of doing simplifies the realization of all, and facilitates the order. The advantage is to be able to use such a configuration for pasty product delivery devices, but the valve devices of the prior art do not lend themselves to such organization.

La présente invention a pour objet de résoudre les problèmes sus évoqués en proposant un dispositif universel qui puisse être utilisé pour la distribution dosée de tous types de produits qu'ils soient pâteux, liquides, semi-liquides ou pulvérulents avec lequel il est possible d'obtenir un degré de précision très élevé dans le dosage avec des moyens mécaniques simples, robustes et usinés avec les tolérances de la mécanique courante.The present invention aims to solve the aforementioned problems by providing a universal device that can be used for the metered dispensing of all types of products they are pasty, liquid, semi-liquid or powder with which it is possible to to obtain a very high degree of precision in the metering with simple mechanical means, robust and machined with the tolerances of the current mechanics.

Un autre objectif de la présente invention est la mise en oeuvre d'un dispositif pour la distribution et le dosage de produits pâteux qui permet d'allier la précision du dosage et la rapidité de distribution du produit.Another object of the present invention is the implementation of a device for dispensing and dosing of pasty products which allows to combine the precision of the dosage and the speed of distribution of the product.

Un autre objectif de la présente invention est la réalisation d'un dispositif pour la distribution et le dosage de produits pâteux dont l'organe d'obturation est constitué par une soupape et pour lequel ont été réduites les pertes de charges.Another object of the present invention is the production of a device for dispensing and dosing pasty products whose closure member is constituted by a valve and for which the pressure losses have been reduced.

Un autre objectif de la présente invention est la réalisation d'un dispositif pour la distribution et le dosage de produits pâteux, liquides ou semi-liquides à forte tension superficielle ou de produits pulvérulents à fort pouvoir d'agglomération.Another object of the present invention is the production of a device for dispensing and dosing pasty, liquid or semi-liquid products with a high surface tension or pulverulent products with high agglomeration power.

Un autre objectif de la présente invention est l'obtention d'un degré de précision très élevé dans le dosage des produits pâteux, liquides, semi-liquides et pulvérulents, ce degré de précision pouvant atteindre le dixième de milligramme.Another objective of the present invention is to obtain a very high degree of precision in the determination of pasty, liquid, semi-liquid and powdery products, this degree of precision being able to reach a tenth of a milligram.

Un autre objectif de la présente invention est la réalisation d'un dispositif pour la distribution et le dosage de produits pâteux, liquides ou semi-liquides à forte tension superficielle ou de produits pulvérulents à fort pouvoir d'agglomération qui assure d'une part la séparation de la queue de dose sans emploi d'organes mécaniques tels que racles et autres venant au contact du produit et d'autre part la chute de cette queue de dose dans le récipient dans lequel est distribuée la dose.Another object of the present invention is the production of a device for the dispensing and dosing of pasty, liquid or semi-liquid products with a high surface tension or of pulverulent products with a high agglomeration power which, on the one hand, ensures separation of the dose tail without use of mechanical organs such as doctor blades and others coming into contact with the product and secondly the fall of this dose tail in the container in which is dispensed the dose.

À cet effet, le dispositif pour la distribution dosée de produits pâteux ou liquides ou semi-liquides ou pulvérulents, comporte un corps de dispositif dans lequel est formé un conduit de passage du produit depuis un orifice d'introduction vers un ajutage de délivrance du produit en quantités dosées. Un siège de soupape est formé dans ledit conduit et une soupape est montée dans ce dernier de manière à pouvoir y coulisser et être appliquée contre le siège de soupape ou être écartée de ce dernier en sorte, soit d'interdire la délivrance du produit, soit permettre cette délivrance. La soupape est dotée d'une queue de soupape laquelle est montée en coulissement dans un alésage de guidage et coopère avec un mécanisme moteur d'actionnement de la soupape en écartement du siège ou vers le siège de soupape, le conduit de passage du produit comporte un segment rectiligne de passage du produit dans lequel segment est disposé le siège de soupape et s'étendent axialement et en totalité la soupape et la queue de soupape et dans lequel segment pénètre au moins en partie le mécanisme d'actionnement de la soupape, ce mécanisme étant au contact du produit de façon que la liaison mécanique entre la queue de soupape et le mécanisme d'actionnement soit également au contact du produit et soit lubrifié par le produit lui-même, le mécanisme d'actionnement de la soupape comprend, d'une part au moins un organe élastique agissant en poussée sur la soupape et sollicitant cette dernière vers le siège et donc vers une position de fermeture et d'autre part une tige d'actionnement, guidée axialement dans un alésage du corps de dispositif, lequel alésage est transversal au segment rectiligne de conduit de passage et débouche dans ledit segment, ladite tige venant au contact de la queue de soupape pour agir en poussée sur cette dernière, le contact entre la queue de soupape et le mécanisme d'actionnement étant établi par deux surfaces de glissement dont une est ménagée sur la queue de soupape et l'autre sur la tige d'actionnement, les deux dites surfaces étant situées dans le segment rectiligne de passage du produit, caractérisé en ce que l'une au moins des dites surfaces est plane et oblique par rapport à l'axe géométrique de déplacement de la soupape entre ses positions ouverte et fermée et oblique par rapport à l'axe géométrique de déplacement de la tige d'actionnement, afin que lorsque la tige d'actionnement est déplacée par un organe moteur dans le sens de l'enfoncement dans le corps de dispositif, la soupape soit écartée de son siège sous l'effet de la poussée exercée par la surface de glissement de la tige d'actionnement sur la surface de glissement de la queue de soupape.For this purpose, the device for the dosed dispensing of pasty or liquid or semi-liquid or powdery products, comprises a device body in which is formed a conduit for the passage of the product from an introduction orifice to a delivery nozzle of the product. in metered quantities. A valve seat is formed in said conduit and a valve is mounted therein so as to be slidable thereon and can be applied against the valve seat or be spaced from the valve seat to either prohibit the delivery of the product or allow this deliverance. The valve is provided with a valve stem which is slidably mounted in a guide bore and cooperates with a drive mechanism for actuating the valve away from the seat or towards the valve seat, the product passageway comprises a straight segment of passage of the product in which segment is disposed the valve seat and extend axially and in all the valve and the valve stem and in which segment at least partially penetrates the actuating mechanism of the valve, this the mechanism being in contact with the product so that the mechanical connection between the valve stem and the actuating mechanism is also in contact with the product and is lubricated by the product itself, the actuating mechanism of the valve comprises, at least one elastic member acting as a thrust on the valve and biasing the latter towards the seat and thus towards a closed position and on the other hand actuating geometry, guided axially in a bore of the device body, which bore is transverse to the rectilinear segment of conduit and opens into said segment, said rod coming into contact with the valve stem to act in thrust on the latter, the contact between the valve stem and the actuating mechanism being established by two sliding surfaces, one of which is formed on the valve stem and the other on the actuating rod, the said two surfaces being located in the rectilinear segment passage of the product, characterized in that at least one of said surfaces is flat and oblique with respect to the geometric axis of displacement of the valve between its open and closed positions and oblique with respect to the geometric axis of displacement of the actuating rod, so that when the actuating rod is moved by a drive member in the direction of depression into the device body, the valve is Cartee of its seat under the effect of the thrust exerted by the sliding surface of the actuating rod on the sliding surface of the valve stem.

On réalise ainsi un mécanisme d'actionnement particulièrement simple et peu coûteux.This provides a particularly simple and inexpensive actuation mechanism.

Selon une autre caractéristique de l'invention, la surface de glissement oblique forme avec l'axe géométrique de déplacement de la tige d'actionnement, un angle aigu de valeur inférieure à 45 degrés. Grâce à cette caractéristique, un déplacement donné de la tige d'actionnement s'accompagnera d'un moindre déplacement de la soupape. On obtient ainsi un effet de démultiplication du mouvement de la soupape conduisant à une meilleure précision positionnelle de cette dernière.According to another characteristic of the invention, the oblique sliding surface forms with the geometric axis of displacement of the actuating rod, an acute angle of value less than 45 degrees. Thanks to this characteristic, a given displacement of the actuating rod will be accompanied by a less displacement of the valve. This results in a reduction effect of the movement of the valve leading to a better positional accuracy of the latter.

Selon une autre caractéristique de l'invention, l'alésage de guidage de la tige d'actionnement est perpendiculaire à la section de passage du produit.According to another characteristic of the invention, the guide bore of the actuating rod is perpendicular to the passage section of the product.

Selon une autre caractéristique de l'invention, la section rectiligne de passage du produit est verticale.According to another characteristic of the invention, the straight section of passage of the product is vertical.

Selon encore une autre caractéristique de l'invention, le conduit de passage du produit est vertical et s'étend de manière rectiligne depuis un orifice d'entrée du produit vers un orifice de délivrance de ce dernier.According to yet another characteristic of the invention, the product passage is vertical and extends rectilinearly from an inlet of the product to a delivery port of the latter.

Selon encore une autre caractéristique de l'invention, l'organe moteur assurant le déplacement de la tige d'actionnement est externe au dispositif et indépendant de ce dernier.According to yet another characteristic of the invention, the motor member ensuring the displacement of the actuating rod is external to the device and independent of the latter.

Selon une autre caractéristique de l'invention, à l'ajutage de délivrance du produit est associé un dispositif de soufflage d'un fluide sous pression pour détacher, sous l'effet du souffle ou sous l'effet de la dépression ou de la pression en résultant, la queue de dose suspendue à l'ajutage de délivrance et favoriser la chute de cette queue de dose vers le récipient dans lequel a été distribuée la dose.According to another characteristic of the invention, the dispensing nozzle of the product is associated with a device for blowing a fluid under pressure to detach, under the effect of the blast or under the effect of the depression or the pressure resulting, the dose tail suspended from the delivery nozzle and promote the fall of this dose tail to the container in which was dispensed the dose.

Ainsi on sépare la queue de dose, de la buse de distribution, sans emploi de moyen mécanique, uniquement par des fluides qui peuvent être inertes vis-à-vis du produit à distribuer mais qui peuvent le cas échéant réagir avec eux si cet effet est recherché. On comprend aussi que la queue de dose est systématiquement incluse dans la dose ce qui garantit la précision du dosage. Par ailleurs est assuré ainsi, après chaque distribution, le nettoyage des faces externes de pourtour de l'ajutage de distribution, on évite par ce biais tout dépôt sécable à ce niveau qui pourrait éventuellement obstruer l'ajutage ou polluer les distributions ultérieures.Thus the dose tail is separated from the dispensing nozzle, without the use of mechanical means, solely by fluids which may be inert with respect to the product to be dispensed but which may, if appropriate, react with them if this effect is research. It is also understood that the dose tail is systematically included in the dose which guarantees the accuracy of the dosage. Moreover, it is ensured, after each distribution, the cleaning of the outer faces around the dispensing nozzle, this avoids any breakable deposit at this level which could possibly obstruct the nozzle or pollute subsequent distributions.

Selon une autre caractéristique de l'invention, le fluide sous pression est soufflé vers la queue de dose sous forme d'une impulsion ou d'un jet bref, d'une intensité appropriée, pour assurer une séparation rapide, compatible avec des cadences de distribution élevées. Par ailleurs la puissance du jet, combinée avec une orientation appropriée dans la direction d'écoulement du produit ou légèrement inclinée par rapport à cette dernière permet de créer une dépression autour de la queue de dose générant un phénomène d'aspiration de cette dernière conduisant d'abord à sa séparation de l'ajutage de distribution et à sa chute contrôlée vers le récipient.According to another characteristic of the invention, the fluid under pressure is blown towards the dose tail in the form of a pulse or a short jet, of an appropriate intensity, to ensure a rapid separation, compatible with rates of high distribution. Moreover, the power of the jet, combined with an appropriate orientation in the direction of flow of the product or slightly inclined relative to the latter, creates a depression around the tail of the dose generating a suction phenomenon of this last leading first to its separation from the dispensing nozzle and its controlled drop towards the container.

En variante, la direction du jet sera radiale à l'ajutage ou légèrement inclinée par rapport à un plan radial pour assurer une séparation par cisaillement.Alternatively, the direction of the jet will be radial to the nozzle or slightly inclined relative to a radial plane to provide shear separation.

En variante, le jet de séparation n'est plus soufflé par impulsion, mais de manière continue.In a variant, the separation jet is no longer pulsed, but continuously.

Selon une autre caractéristique de l'invention, le dispositif de soufflage est pourvu d'un ajutage de délivrance d'un fluide sous pression et ledit ajutage est formé autour de l'ajutage de délivrance du produit. Le fluide est ainsi réparti autour de la queue de dose, et cette répartition limite la déviation de la chute de la queue de dose vers le récipient.According to another characteristic of the invention, the blowing device is provided with a nozzle for delivering a fluid under pressure and said nozzle is formed around the product delivery nozzle. The fluid is thus distributed around the dose tail, and this distribution limits the deviation of the drop of the dose tail towards the container.

D'autres buts, avantages et caractéristiques de l'invention apparaîtront à la lecture de la description d'une forme préférée de réalisation donnée à titre d'exemple non limitatif en se référant aux dessins annexés en lesquels :

  • la figure 1 est une vue en coupe selon un plan longitudinal médian du dispositif selon une première forme de réalisation,
  • la figure 2 est une vue en coupe selon un plan longitudinal médian du dispositif selon une seconde forme de réalisation,
  • la figure 3 est une coupe du dispositif selon la ligne AA de la figure 2.
Other objects, advantages and features of the invention will appear on reading the description of a preferred embodiment given by way of non-limiting example with reference to the appended drawings in which:
  • FIG. 1 is a sectional view along a median longitudinal plane of the device according to a first embodiment,
  • FIG. 2 is a sectional view along a median longitudinal plane of the device according to a second embodiment,
  • FIG. 3 is a section of the device along the line AA of FIG. 2.

Tel que représenté, le dispositif selon l'invention, pour la distribution et le dosage précis, de l'ordre du dixième de milligramme, de produits pâteux pouvant présenter une forte tension superficielle ou de produits liquides, semi-liquides, ou encore de produits pulvérulents pouvant présenter un fort pouvoir d'agglomération, comprend un corps de dispositif 1 de forme parallélépipédique, dans lequel est formé un conduit 2 de passage du produit depuis un orifice d'introduction 3, vers un ajutage 4 de délivrance de produit en quantités dosées, sous lequel est disposé un récipient non représenté, prévu pour recueillir la dose délivrée par le dispositif. L'orifice 3 d'introduction sera connecté par une conduite appropriée à une réserve de produit à distribuer, cette réserve pourra être disposée selon un niveau supérieur par rapport au dispositif pour permettre un écoulement gravitaire du produit vers ledit dispositif. Cette réserve pourra aussi être pressurisée pour forcer le mouvement du produit vers le dispositif, on pourra prévoir aussi une pompe entre la réserve et le dispositif pour puiser le produit dans la réserve et le refouler dans le dispositif.As represented, the device according to the invention, for the precise dispensing and dosing, of the order of one-tenth of a milligram, of pasty products that may have a high surface tension or of liquid, semi-liquid products or products pulverulent materials that can exhibit a high agglomeration power, comprises a device body 1 of parallelepiped shape, in which is formed a conduit 2 for the passage of the product from an introduction orifice 3, to a nozzle 4 of product delivery in metered quantities , under which is disposed a not shown container, provided to collect the dose delivered by the device. The introduction orifice 3 will be connected by a suitable conduit to a supply of product to be dispensed, this reserve may be arranged at a higher level relative to the device to allow a gravity flow of the product to said device. This reserve may also be pressurized to force the movement of the product to the device, it may also provide a pump between the reserve and the device for drawing the product into the reserve and back in the device.

Le conduit 2, comme on peut le voir, présente, un segment rectiligne de passage du produit lequel segment en considérant le sens de passage du produit, une section aval verticale rectiligne de passage de produit, une section médiane verticale rectiligne de passage de produit. Une section amont verticale rectiligne de passage de produit se raccorde au dit segment rectiligne. Cette section amont peut être décalée latéralement par rapport à la section médiane et être connectée à cette dernière par une section formant coude. Les sections, médiane et aval, se prolongent mutuellement de manière axialement alignée. La section amont, comme on peut le voir en figure 1 peut aussi être située dans le prolongement axial de la section médiane. Dans ce cas de figure, les trois sections sont axialement alignées ce qui minimise les pertes de charges dans le conduit de passage du produit. On peut remarquer que ce conduit s'étend verticalement entre l'orifice d'entrée et l'orifice de délivrance ce qui facilite l'écoulement gravitaire du produit au travers du dispositif.The duct 2, as can be seen, has a rectilinear segment of the product passage which segment by considering the direction of passage of the product, a rectilinear vertical downstream product passage section, a rectilinear vertical cross section of product passage. A rectilinear upright vertical section of product passage connects to said rectilinear segment. This upstream section may be laterally offset from the median section and be connected thereto by a bend section. The sections, median and downstream, extend mutually axially aligned. The upstream section, as can be seen in Figure 1 may also be located in the axial extension of the middle section. In this case, the three sections are axially aligned, which minimizes the pressure losses in the product passage duct. It may be noted that this duct extends vertically between the inlet orifice and the delivery orifice which facilitates the gravity flow of the product through the device.

À faible écartement de l'ajutage de délivrance 4 est formé dans la section aval du conduit 2, un siège 5 de soupape. Ce siège, de forme tronconique, est traversé par la section aval du conduit. Comme on peut le voir, la section aval, en aval du siège 5 présente un diamètre réduit par rapport au diamètre de la section amont.At low spacing of the delivery nozzle 4 is formed in the downstream section of the conduit 2, a valve seat 5. This seat, of frustoconical shape, is crossed by the downstream section of the duct. As can be seen, the downstream section downstream of the seat 5 has a reduced diameter relative to the diameter of the upstream section.

Une soupape 6, de forme hémisphérique, ou conique est montée dans le conduit 2 de manière à pouvoir y coulisser pour être appliquée contre le siège 5 et interdire la délivrance du produit ou bien être écartée de ce siège et autoriser cette délivrance. Le conduit immédiatement en amont du siège 5 pourra présenter une forme tronconique. La soupape, entre sa position de fermeture et d'ouverture se déplace dans cette forme tronconique.A valve 6, hemispherical or conical is mounted in the duct 2 so as to slide to be applied against the seat 5 and prohibit the delivery of the product or be removed from this seat and allow this delivery. The duct immediately upstream of the seat 5 may have a frustoconical shape. The valve, between its closed position and opening moves in this frustoconical shape.

Comme on peut le voir, la soupape 6 est dotée d'une queue verticale 7 de soupape, rectiligne, s'étendant axialement dans la section médiane du conduit 2, cette queue 7 de soupape coopérant avec un mécanisme d'actionnement de la soupape 6 en écartement du siège 5 ou bien vers le siège 5, ce mécanisme d'actionnement pénétrant au moins en partie dans le segment rectiligne de passage de produit et venant au contact du produit de façon que la liaison mécanique entre la queue de soupape et le mécanisme d'actionnement soit également au contact du produit et soit lubrifiée par le produit lui-même.As can be seen, the valve 6 is provided with a straight vertical valve stem 7, extending axially in the middle section of the duct 2, this valve stem cooperating with a mechanism for actuating the valve 6 in spacing from the seat 5 or towards the seat 5, this actuating mechanism penetrating at least partly into the rectilinear segment of product passage and coming into contact with the product so that the mechanical connection between the valve stem and the mechanism the actuator is also in contact with the product and is lubricated by the product itself.

Pour permettre le passage du produit dans la section amont du conduit 2, la queue de soupape 7 présente un diamètre plus faible que le diamètre du conduit 2.To allow the passage of the product in the upstream section of the conduit 2, the valve stem 7 has a diameter smaller than the diameter of the conduit 2.

Pour assurer le guidage de la soupape 6, la queue de soupape 7 est montée de manière coulissante dans l'alésage traversant axial d'une douille de guidage 19, sous forme de disque, montée en blocage dans la section médiane du conduit de passage. Comme on peut le voir en figure 1, cette douille de guidage 19 s'étend transversalement dans la section de passage et comporte, autour de l'alésage de guidage, des perçages traversants de passage du produit.To guide the valve 6, the valve stem 7 is slidably mounted in the axial through bore of a guide sleeve 19 in the form of a disc, mounted in blocking in the middle section of the passage conduit. As can be seen in Figure 1, the guide sleeve 19 extends transversely in the passage section and comprises, around the guide bore, through-holes for the passage of the product.

Pour assurer le guidage de la soupape 6, pour le dispositif selon les figures 2 et 3, la queue de soupape 7 est montée de manière coulissante dans un alésage 7a pratiqué dans le corps de dispositif 1, dans le prolongement axial de la section médiane du conduit 2. L'alésage de guidage sera suffisamment long pour écarter tout risque d'arc-boutement à ce niveau. Un joint d'étanchéité pourra être disposé dans l'alésage 7a autour de la queue de soupape pour éviter tout reflux de produit dans l'alésage et assurer l'étanchéité mais préférentiellement l'alésage est borgne, la qualité du guidage de la queue de soupape dans l'alésage est du type H7-g6 par exemple et aucun joint d'étanchéité n'est utilisé. On laisse ainsi refluer volontairement le produit vers le fond de l'alésage 7a, ce reflux se présentant sous la forme d'un film dont l'intérêt est d'assurer la lubrification du guidage. La quantité de produit refluant vers le fond de l'alésage est très faible si bien que ce dernier ne se remplit que très lentement. Un remplissage total de cet alésage 7a n'est pas gênant en soit puisque sous l'effet du mouvement d'enfoncement du piston dans l'alésage, un mouvement de reflux du produit vers le conduit 2 se produira. On obtiendra ainsi un vidage de l'alésage.To guide the valve 6, for the device according to Figures 2 and 3, the valve stem 7 is slidably mounted in a bore 7a formed in the device body 1, in the axial extension of the middle section of the conduit 2. The guide bore will be long enough to avoid any risk of jamming at this level. A seal may be disposed in the bore 7a around the valve stem to prevent product backflow into the bore and ensure sealing but preferably the bore is blind, the quality of the guide of the tail of valve in the bore is of the type H7-g6 for example and no seal is used. It is thus allowed to flow back deliberately to the bottom of the bore 7a, this reflux occurring in the form of a film whose interest is to ensure the lubrication of the guide. The amount of product flowing towards the bottom of the bore is very small so that it fills only very slowly. A total filling of this bore 7a is not a problem in itself since under the effect of the driving movement of the piston in the bore, a backflow of the product to the conduit 2 will occur. This will result in emptying the bore.

Une pollution du produit à distribuer par la quantité de produit contenue dans l'alésage 7a n'est pas non plus à craindre en raison, d'une part, du fait que le dispositif n'est utilisé que pour la distribution d'un seul produit et d'autre part, qu'il subit un nettoyage complet après chaque cycle de distribution.Pollution of the product to be distributed by the amount of product contained in the bore 7a is not to be feared because, firstly, because the device is used only for the distribution of a single product and on the other hand, that it undergoes a complete cleaning after each distribution cycle.

Selon une forme avantageuse de l'invention, le mécanisme d'actionnement de la soupape comprend, d'une part au moins un organe élastique 8 du type ressort à spires agissant en poussée sur la soupape 6 et sollicitant cette dernière vers le siège 5 donc vers une position de fermeture et d'autre part une tige 9 d'actionnement, guidée axialement dans un alésage 10 du corps de dispositif, lequel alésage est transversal au segment rectiligne de conduit de passage et débouche dans ledit segment. Préférentiellement, cet alésage de guidage 10 est perpendiculaire à la section médiane du conduit 2 et débouche dans cette dernière. La tige 9 d'actionnement vient au contact de la queue de soupape 7 et agit en poussée sur cette dernière, le contact entre la queue de soupape et le mécanisme d'actionnement étant établi par deux surfaces de glissement 11, 20 dont une 11 est ménagée sur la queue de soupape 7 et l'autre 20 sur la tige d'actionnement 9, les deux dites surfaces 11, 20 étant situées dans le segment rectiligne de passage du produit et étant en contact avec le dit produit.According to an advantageous form of the invention, the mechanism for actuating the valve comprises, on the one hand, at least one spring-like elastic member 8 acting in thrust on the valve 6 and urging the latter towards the seat 5, therefore to a closed position and on the other hand an actuating rod 9, guided axially in a bore 10 of the device body, which bore is transverse to the straight segment of conduit and opens into said segment. Preferably, this guide bore 10 is perpendicular to the median section of the conduit 2 and opens into the latter. The actuating rod 9 comes into contact with the valve stem 7 and acts in thrust on the latter, the contact between the valve stem and the actuating mechanism being established by two sliding surfaces 11, 20 of which one 11 is formed on the valve stem 7 and the other 20 on the actuating rod 9, both said surfaces 11, 20 being located in the rectilinear segment of the product and being in contact with said product.

L'une au moins de ces surfaces est plane et oblique par rapport à l'axe géométrique de déplacement de la soupape 6 entre ses positions ouverte et fermée afin que lorsque la tige d'actionnement 9 est déplacée dans le sens de l'enfoncement dans le corps de dispositif, la soupape 9 soit écartée de son siège sous l'effet de la poussée exercée par la surface de glissement 20 de la tige 9 sur la surface de glissement 11 de la queue de soupape et bien entendu sous l'effet du mouvement de glissement des deux surfaces 11, 20 l'une sur l'autre. Il y a lieu de noter que le mouvement d'écartement de la soupape 6 s'effectue à l'encontre de l'action de poussée exercée par l'organe élastique 8 sur la soupape 7. En revanche lors du mouvement inverse de la tige 11, la poussée du ressort 8 entraîne le mouvement de la soupape vers le siège 5 de soupape.At least one of these surfaces is flat and oblique with respect to the geometric axis of displacement of the valve 6 between its open and closed positions so that when the actuating rod 9 is moved in the direction of insertion into the device body, the valve 9 is spaced from its seat under the effect of the thrust exerted by the sliding surface 20 of the rod 9 on the sliding surface 11 of the valve stem and of course under the effect of the sliding movement of the two surfaces 11, 20 one over the other. It should be noted that the spacing movement of the valve 6 takes place against the thrust action exerted by the elastic member 8 on the valve 7. On the other hand, during the reverse movement of the rod 11, the thrust of the spring 8 causes the valve to move towards the valve seat 5.

Selon une première forme de réalisation, objet de la figure 1, l'organe élastique 8 est monté autour de la queue de soupape, en compression entre la soupape et la douille de centrage. Selon l'autre forme de réalisation du dispositif, objet des figures 2 et 3, l'organe élastique 8 est monté en compression entre le fond de l'alésage 7a et la queue 7 de soupape.According to a first embodiment, object of Figure 1, the elastic member 8 is mounted around the valve stem, in compression between the valve and the centering sleeve. According to the other embodiment of the device, object of Figures 2 and 3, the resilient member 8 is mounted in compression between the bottom of the bore 7a and the tail 7 valve.

La surface de glissement oblique pourra être ménagée sur la tige d'actionnement 9 ou sur la queue de soupape, l'autre surface pouvant présenter ou non la même oblicité afin d'obtenir un contact et un glissement plan sur plan moins sujet à usure qu'un contact et un glissement, ligne sur plan. Comme on peut le voir en figure 1, les deux surfaces 11, 20 sont toutes deux obliques.The oblique sliding surface may be provided on the actuating rod 9 or on the valve stem, the other surface may or may not have the same obliqueness in order to to obtain a contact and a sliding plan on plane less subject to wear than a contact and a slip, line on plan. As can be seen in Figure 1, both surfaces 11, 20 are both oblique.

La tige 9 est actionnée en coulissement axial par un organe moteur 9a externe au corps du dispositif. Cette tige 9 présente donc une portion externe au corps du dispositif avec laquelle coopère en poussée axiale l'organe moteur 9a. Cet organe moteur 9a peut être fixé au corps du dispositif ou bien être indépendant du dispositif et non fixé à ce dernier. Cet organe moteur 9a contrôle donc le mouvement de la tige 9 ainsi que son degré d'enfoncement dans l'alésage 9. Par ce biais cet organe moteur 9a contrôle le mouvement de la soupape ainsi que le degré d'ouverture de cette dernière. On comprend que la soupape grâce à ces moyens peut être placée dans une position de totale ouverture permettant l'écoulement du produit selon un débit maximal mais aussi selon une position intermédiaire, entre la position d'ouverture et de fermeture, choisie selon le débit désiré. L'organe moteur contrôle aussi le mouvement de retour de la tige 9 et donc la façon de la soupape est amenée en position de fermeture. Cet organe moteur sera contrôlé et commandé par une unité de contrôle et de commande.The rod 9 is actuated in axial sliding by a motor member 9a external to the body of the device. This rod 9 thus has a portion external to the body of the device with which cooperates in axial thrust the motor member 9a. This drive member 9a can be fixed to the body of the device or be independent of the device and not attached thereto. This drive member 9a thus controls the movement of the rod 9 and its degree of depression in the bore 9. By this means the drive member 9a controls the movement of the valve and the degree of opening of the latter. It is understood that the valve by these means can be placed in a position of total opening allowing the flow of the product at a maximum flow rate but also in an intermediate position, between the open position and closing, chosen according to the desired flow rate . The motor member also controls the return movement of the rod 9 and thus the way the valve is brought into the closed position. This motor unit will be controlled and controlled by a control unit.

Comme on peut le voir, le mouvement d'enfoncement de la tige 9 dans l'alésage 10 vers la queue de soupape s'effectue à l'encontre de l'action d'un organe élastique de rappel 12 monté en compression dans l'alésage 10 entre un épaulement de ce dernier et un épaulement de la tige 9. Dans la forme préférée de réalisation, la tige 9 présente une forme de doigt de poussée 9b de diamètre réduit. Cette forme de doigt de poussée 9b est dotée en partie terminale de l'une 20 des deux surfaces de glissement, et l'organe élastique de rappel 12, sous forme de ressort à spires, est monté autour de cette forme de doigt de poussée. L'alésage 10 est formé en partie par l'alésage traversant d'une pièce amovible 9c de butée et d'étanchéité, engagée en vissage dans un taraudage du corps de dispositif 1. L'alésage de cette pièce, forme un épaulement de butée 9d contre lequel vient buter un épaulement de butée 9e de la tige 9. Ces deux épaulements limitent le mouvement de recul de la tige 9. Cette tige, en arrière de l'épaulement précité, présente un diamètre réduit.As can be seen, the driving movement of the rod 9 in the bore 10 towards the valve stem takes place against the action of an elastic return member 12 mounted in compression in the bore 10 between a shoulder of the latter and a shoulder of the rod 9. In the preferred embodiment, the rod 9 has a shape of push pin 9b of reduced diameter. This form of thrust finger 9b is provided at the end portion of one of the two sliding surfaces, and the resilient return member 12, in the form of a coil spring, is mounted around this thrust pin shape. The bore 10 is formed in part by the through bore of a removable piece 9c for abutment and sealing, engaged in screwing in a tapping of the device body 1. The bore of this piece, forms a stop shoulder 9d against which abuts an abutment shoulder 9e of the rod 9. These two shoulders limit the recoil movement of the rod 9. This rod, behind the aforementioned shoulder, has a reduced diameter.

La surface de glissement oblique forme avec l'axe géométrique de déplacement de l'actionneur, un angle aigu de valeur inférieure à 45 degrés. Grâce à cette caractéristique, un déplacement donné de la tige d'actionnement s'accompagnera d'un moindre déplacement de la soupape. On obtient ainsi un effet de démultiplication du mouvement de la soupape. Grâce à cet effet de réduction, on obtient également une meilleure précision positionnelle de la soupape et par voie de conséquence une meilleure maîtrise du débit du produit. Il va de soit que l'inclinaison des surfaces de glissement est compatible avec le coefficient de frottement de l'une sur l'autre. Il y a lieu de rappeler que ces deux surfaces sont au contact du produit de sorte que ce dernier en se déposant sur ces surfaces forme un film apte à diminuer ce coefficient de frottement et par voie de conséquence l'usure des deux surfaces de glissement.The oblique sliding surface forms with the geometric axis of displacement of the actuator, an acute angle of less than 45 degrees. Thanks to this characteristic, a given displacement of the actuating rod will be accompanied by a less displacement of the valve. This gives a reduction effect of the movement of the valve. Thanks to this reduction effect, a better positional accuracy of the valve is obtained as well as a better control of the flow of the product. It goes without saying that the inclination of the sliding surfaces is compatible with the coefficient of friction of one over the other. It should be recalled that these two surfaces are in contact with the product so that the latter by being deposited on these surfaces forms a film capable of reducing this coefficient of friction and consequently the wear of the two sliding surfaces.

Selon la forme préférée de réalisation, la queue de soupape 7 est dotée d'une lumière traversante dans un sens diamétral, la surface de glissement 11 propre à la queue de soupape étant constituée par la face supérieure (face amont en considérant le sens d'écoulement du produit) de cette lumière. Cette lumière est par ailleurs délimitée par deux faces planes parallèles entre elles et parallèles à l'axe longitudinal de la queue de soupape et par une face inférieure perpendiculaire ou oblique au dit axe. La forme de doigt de poussée 9b présente deux méplats parallèles, venant en regard des faces latérales de la lumière traversante. Pour assurer le calage angulaire de la queue de soupape dans le conduit 2 et pour que la surface de glissement 11 demeure toujours en regard de la tige 9, la forme de doigt de poussée 9b de cette dernière est astreinte par les épaulements de butée 9d, 9e, à demeurer toujours dans la lumière traversante. Les méplats de cette forme de doigt de poussée 9b et les faces latérales de la lumière constituent ensemble le calage angulaire. Comme on peut le voir sur les figures jointes, la surface de glissement 20 que présente le doigt est oblique et est en regard de la surface de glissement 11.According to the preferred embodiment, the valve stem 7 is provided with a through-hole in a diametrical direction, the sliding surface 11 specific to the valve stem being constituted by the upper face (upstream face, considering the direction of the valve). product flow) from this light. This light is further delimited by two plane faces parallel to each other and parallel to the longitudinal axis of the valve stem and by a lower face perpendicular or oblique to said axis. The thrust finger shape 9b has two parallel flats, coming opposite the lateral faces of the through-light. In order to ensure the angular setting of the valve stem in the duct 2 and for the sliding surface 11 to remain always opposite the rod 9, the push pin shape 9b of the latter is constrained by the stop shoulders 9d, 9th, to remain always in the crossing light. The flats of this form of thrust finger 9b and the lateral faces of the light together constitute the angular setting. As can be seen in the accompanying figures, the sliding surface 20 that the finger has is oblique and is opposite the sliding surface 11.

Préférentiellement, en vue de diminuer encore le coefficient de frottement des deux surfaces de glissement l'une sur l'autre, l'une d'entre elles au moins est recouverte de PTFE. On pourra prévoir le fait que l'une de ces surfaces soit taillée dans une pièce en PTFE. Ainsi comme on peut le voir en figure 1 la surface de glissement 11 est formée dans une pièce d'usure 22 en PTFE bloquée dans la queue de soupape 7. Comme on peut le voir cette queue de soupape est tubulaire et présente selon un plan diamétral deux lumières opposées décalées en hauteur. La pièce d'usure 22 est destinée à être introduite en force dans la queue de soupape et se présente sous la forme d'un cylindre. Cette pièce d'usure, selon l'un de ses diamètres sera équipée de la lumière traversante sus évoquée, la surface de glissement 11 sera toujours constituée par la face supérieure (face amont en considérant le sens d'écoulement du produit) de cette lumière. Lors du montage, la lumière de la pièce d'usure 22 sera amenée en regard des lumières de la queue de soupape.Preferably, in order to further reduce the coefficient of friction of the two sliding surfaces one on the other, at least one of them is covered with PTFE. It can be provided that one of these surfaces is cut in a PTFE part. Thus, as can be seen in FIG. 1, the sliding surface 11 is formed in a wear piece 22 made of PTFE locked in the valve stem 7. As can be seen, this valve stem is tubular and presents in a diametrical plane. two opposite lights offset in height. The wear part 22 is intended to be forced into the valve stem and is in the form of a cylinder. This wear part, according to one of its diameters will be equipped with the above-mentioned through-light, the sliding surface 11 will always be constituted by the upper face (upstream face considering the direction of flow of the product) of this light . During assembly, the light of the wear part 22 will be brought opposite the slots of the valve stem.

Pour séparer de l'ajutage 4 de délivrance, la queue de dose qui pourrait y adhérer sous l'effet de l'action des forces de tension superficielle, est prévu un dispositif 13 de soufflage d'un fluide sous pression.To separate from the delivery nozzle 4, the dose tail which could adhere under the effect of the action of the surface tension forces, is provided a device 13 for blowing a fluid under pressure.

Le fluide sous pression peut être introduit dans le conduit 2 en aval du siège 5 de façon à chasser par poussée la queue de dose mais préférentiellement, le jet de fluide sous pression délivré par le dispositif 13 est externe au conduit 4. Selon cette forme préférée de réalisation, le dispositif de soufflage 13 est externe au conduit 2 et à l'ajutage 4.The pressurized fluid can be introduced into the conduit 2 downstream of the seat 5 so as to push the dose tail by pushing but preferably, the pressurized fluid jet delivered by the device 13 is external to the conduit 4. According to this preferred form embodiment, the blowing device 13 is external to the duct 2 and to the nozzle 4.

Préférentiellement, le fluide sous pression est soufflé vers la queue de dose sous forme d'une impulsion d'intensité relativement importante.Preferably, the fluid under pressure is blown towards the dose tail in the form of a pulse of relatively high intensity.

Selon la forme préférée de réalisation, le dispositif de soufflage 13 est équipé d'un ajutage 14 de délivrance du fluide sous pression. Cet ajutage est formé autour de l'ajutage de délivrance du produit de façon que le fluide en sortie de cet ajutage puisse se répartir autour de la queue de dose.According to the preferred embodiment, the blowing device 13 is equipped with a nozzle 14 for delivering the fluid under pressure. This nozzle is formed around the delivery nozzle of the product so that the fluid output of this nozzle can be distributed around the dose tail.

L'ajutage 4 de délivrance du produit est préférentiellement formé dans une buse 15, cette buse est dotée du siège 5. Préférentiellement la buse 15 est fixée de manière amovible au corps de dispositif 1. À cet effet, la buse 15 sera dotée d'une portion cylindrique filetée et sera engagée par cette portion cylindrique filetée dans un taraudage approprié, pratiqué dans le corps de dispositif autour de la section médiane du conduit 2. Cette disposition permet le démontage de la soupape 6 en vue de son nettoyage. En figure 1 on peut remarquer que la buse 15 vient appui contre la douille de guidage 19 et maintien cette dernière contre un épaulement formé dans la section médiane du conduit.The delivery nozzle 4 of the product is preferably formed in a nozzle 15, this nozzle is provided with the seat 5. Preferably the nozzle 15 is removably attached to the device body 1. For this purpose, the nozzle 15 will be equipped with a threaded cylindrical portion and will be engaged by this threaded cylindrical portion in a suitable thread, made in the device body around the middle section of the conduit 2. This arrangement allows the disassembly of the valve 6 for cleaning. In Figure 1 it can be seen that the nozzle 15 bears against the guide sleeve 19 and maintains the latter against a shoulder formed in the middle section of the conduit.

La buse 15 en amont de l'orifice de délivrance pourra recevoir une grille 21 apte à retenir les gouttes de liquides susceptibles de perturber le dosage. La buse 15, en amont de cette grille pourra présenter un évasement pour « tranquilliser » l'écoulement.The nozzle 15 upstream of the delivery port may receive a gate 21 adapted to retain drops of liquids that may disturb the assay. The nozzle 15, upstream of this grid may have a flare to "quiet" the flow.

Selon une autre forme de réalisation, telle qu'illustrée en figure 2 et 3, l'ajutage 14 de délivrance du fluide est formé par l'ouverture inférieure, circulaire d'une chambre 16 formée autour de la buse 15 et délimitée par une enveloppe 16a fixe par rapport à ladite buse. Comme on peut le voir, l'enveloppe 16a et la buse 15 sont coaxiales. L'enveloppe 16 est équipée d'au moins un perçage 17 d'introduction du fluide sous pression dans la chambre 16. Ce perçage est connecté, par une conduite appropriée du dispositif 13, à une source de fluide sous pression installée à distance ou à proximité du dispositif. Sur cette conduite pourra être installée une électrovanne commandée par un automate programmable ou tout autre moyen équivalent.According to another embodiment, as illustrated in FIGS. 2 and 3, the nozzle 14 for delivering the fluid is formed by the lower, circular opening of a chamber 16 formed around the nozzle 15 and delimited by an envelope 16a fixed with respect to said nozzle. As can be seen, the envelope 16a and the nozzle 15 are coaxial. The casing 16 is equipped with at least one piercing 17 for introducing the fluid under pressure into the chamber 16. This piercing is connected, by a suitable conduit of the device 13, to a source of pressure fluid installed remotely or proximity of the device. On this pipe may be installed a solenoid valve controlled by a programmable controller or any other equivalent means.

Telle que représentée, la surface externe de la buse 15 est de forme tronconique, la petite base du tronc de cône et l'ajutage 14 de délivrance du fluide sous pression étant disposés à proximité l'un de l'autre.As shown, the outer surface of the nozzle 15 is frustoconical in shape, the small base of the truncated cone and the nozzle 14 for delivering the fluid under pressure being arranged close to each other.

Selon une autre forme de réalisation, la surface externe de la buse 15 est cylindro-conique, l'ajutage de délivrance 14 du fluide sous pression étant situé dans ce cas à proximité immédiate de l'extrémité libre de la partie cylindrique. Cette surface cylindrique permet dans une certaine mesure l'orientation du jet de fluide sous pression sensiblement dans l'axe d'écoulement du produit et limite l'effet de cisaillement que peut produire le fluide sur la queue de dose. L'ajutage de délivrance du produit est pratiqué en extrémité de la partie cylindrique.According to another embodiment, the outer surface of the nozzle 15 is cylindro-conical, the delivery nozzle 14 of the pressurized fluid being located in this case in the immediate vicinity of the free end of the cylindrical portion. This cylindrical surface allows to a certain extent the orientation of the pressurized fluid jet substantially in the product flow axis and limits the shearing effect that the fluid can produce on the dose tail. The delivery nozzle of the product is formed at the end of the cylindrical portion.

Toujours selon la forme préférée de réalisation, la face interne de l'enveloppe 16a présente une partie tronconique dont la petite base est formée par l'ajutage 14 de délivrance du fluide sous pression. Comme on peut le voir, la partie tronconique de la face interne de l'enveloppe 16a présente un angle au sommet supérieur à l'angle au sommet de la partie tronconique de la surface externe de la buse 15. Cette disposition permet d'écarter la face interne de l'enveloppe 16a de la face externe de la buse 15 pour ménager une chambre 16 de volume suffisant. Le sommet du cône correspondant à la forme tronconique que présente la face interne de l'enveloppe 16 se situe sur l'axe de symétrie du conduit 2 à proximité de l'ajutage 4 de délivrance du produit. Selon la forme de réalisation objet des figures 1 et 2, ce sommet est situé en aval de cet ajutage afin de superposer à l'effet d'entraînement de la queue de dose un léger effet de cisaillement. Mais une telle forme de réalisation ne doit pas être considérée comme limitative, le sommet du cône pouvant être situé en amont de l'ajutage de délivrance 4 du produit.Still according to the preferred embodiment, the inner face of the casing 16a has a frustoconical portion whose small base is formed by the nozzle 14 for delivering the fluid under pressure. As can be seen, the frustoconical portion of the inner face of the envelope 16a has an apex angle greater than the angle at the apex of the frustoconical portion of the outer surface of the nozzle 15. This provision allows to remove the internal face of the casing 16a of the outer face of the nozzle 15 to provide a chamber 16 of sufficient volume. The top of the cone corresponding to the frustoconical shape that presents the inner face of the casing 16 is located on the axis of symmetry of the duct 2 near the nozzle 4 for delivering the product. According to the embodiment which is the subject of FIGS. 1 and 2, this vertex is located downstream of this nozzle in order to superimpose the driving effect of the dose tail a slight shearing effect. But such an embodiment should not be considered as limiting, the top of the cone may be located upstream of the delivery nozzle 4 of the product.

Préférentiellement l'enveloppe 16a présente une partie cylindrique dans le prolongement de la partie tronconique. Cette partie cylindrique peut être pourvue d'au moins un perçage traversant 17, d'introduction du fluide sous pression dans la chambre 16. Ce perçage peut être pratiqué aussi dans la partie tronconique de l'enveloppe. Sur les figures jointes n'est représenté qu'un seul perçage traversant, mais en variante pourront être prévus plusieurs perçages équirépartis, pour mieux équilibrer le jet de fluide en sortie de l'ajutage 14 et éviter toute déviation de ce dernier.Preferably the envelope 16a has a cylindrical portion in the extension of the frustoconical portion. This cylindrical portion may be provided with at least one through hole 17 for introducing the pressurized fluid into the chamber 16. This drilling may also be performed in the frustoconical portion of the envelope. In the accompanying figures is shown only one through hole, but alternatively may be provided several equidistributed holes, to better balance the jet of fluid output of the nozzle 14 and avoid any deviation of the latter.

Préférentiellement, le ou chaque perçage traversant 17 est disposé en regard de la partie conique de la surface externe de la buse 15. Toujours selon la forme préférée de réalisation, le ou chaque perçage traversant occupe une position radiale, mais cette position pourra être inclinée par exemple vers l'ajutage de délivrance 14.Preferably, the or each through bore 17 is disposed facing the conical portion of the outer surface of the nozzle 15. Still according to the preferred embodiment, the or each through hole occupies a radial position, but this position may be inclined by example to the delivery nozzle 14.

Préférentiellement, les positions respectives des ajutages de délivrance du produit et de délivrance du fluide sous pression sont réglables l'une par rapport à l'autre.Preferably, the respective positions of the product delivery nozzle and the delivery of the fluid under pressure are adjustable relative to each other.

À cet effet l'enveloppe 16a du dispositif 13 de soufflage est fixée par vissage sur la buse 15. Cette disposition permet d'ajuster la position des ajutages de manière très précise, dans l'exemple de réalisation représenté sur les figures, l'ajutage 14 est légèrement au-dessus de l'alésage 4. Cette possibilité de réglage permet une étroite adaptation du dispositif de soufflage aux particularités du produit à distribuer. Ainsi ces positions respectives pourront évoluer en fonction de propriétés physiques des produits à distribuer, l'effet recherché étant la séparation de la queue de dose.For this purpose the casing 16a of the blowing device 13 is fixed by screwing on the nozzle 15. This arrangement makes it possible to adjust the position of the nozzles very precisely, in the embodiment shown in the figures, the nozzle 14 is slightly above the bore 4. This adjustment possibility allows a close adaptation of the blowing device to the particularities of the product to be dispensed. Thus, these respective positions may evolve according to the physical properties of the products to be dispensed, the desired effect being the separation of the dose tail.

Préférentiellement le fluide utilisé pour détacher la queue de dose de la buse 15, se présente à l'état gazeux, ce fluide pouvant être de l'air. En variante, ce fluide pourra se présenter à l'état liquide dans ce cas, il pourra être de l'azote liquide.Preferably the fluid used to detach the dose tail of the nozzle 15 is in the gaseous state, this fluid may be air. Alternatively, this fluid may be in the liquid state in this case, it may be liquid nitrogen.

Ce fluide pourra se présenter à l'état gazeux à température ambiante mais en variante, il pourra se présenter à l'état liquide à température ambiante.This fluid may be in the gaseous state at room temperature but alternatively, it may be in the liquid state at room temperature.

On pourra aussi utiliser un fluide constitué par un produit pulvérulent.It will also be possible to use a fluid consisting of a powdery product.

Le fluide utilisé pourra être inerte vis-à-vis du produit à distribuer et éventuellement des produits déjà déversés dans le récipient ou au contraire, il pourra réagir avec ce ou ces derniers selon l'effet physique ou chimique recherché.The fluid used may be inert with respect to the product to be dispensed and possibly products already poured into the container or, conversely, it may react with this or these depending on the desired physical or chemical effect.

On a décrit un dispositif qui n'est équipé que d'une seule buse, mais en variante, ce dispositif pourra être doté de plusieurs buses, montées coaxialement les unes dans les autres à écartement les unes des autres pour former des chambres annulaires dotées d'ouverture circulaires formant ajutages. Cette disposition permet la distribution simultanée de plusieurs produits devant être associés dans une même composition. Selon cette forme de réalisation, l'enveloppe 16a du dispositif de soufflage 13 est montée autour de la buse la plus extérieure.There is described a device that is equipped with only one nozzle, but alternatively, this device may be provided with several nozzles, mounted coaxially in one another spaced apart from each other to form annular chambers with circular opening forming nozzles. This arrangement allows the simultaneous distribution of several products to be associated in the same composition. According to this embodiment, the casing 16a of the blowing device 13 is mounted around the outermost nozzle.

Le dispositif tel que décrit est doté de perçages 18 de fixation à un support approprié, ce support pouvant se présenter sous la forme d'un plateau. Ce plateau pourra recevoir plusieurs dispositifs du genre précité. Le dispositif pourra être équipé de perçages d'indexation, non représentés, destinés à coopérer en emboîtement de forme avec des doigts d'indexation. Une telle configuration ne requiert qu'un seul moteur 9a.The device as described is provided with holes 18 for attachment to a suitable support, this support may be in the form of a tray. This tray may receive several devices of the aforementioned kind. The device may be equipped with indexing holes, not shown, for cooperating in shape interlocking with indexing fingers. Such a configuration requires only a single motor 9a.

Il y a lieu de noter que les caractéristiques dimensionnelles externes du dispositif tel que décrit sont identiques à celles du dispositif objet du brevet EP 929 498 du demandeur. Cette disposition particulièrement avantageuse permet d'utiliser le dispositif selon l'invention avec ceux objets de ce brevet.It should be noted that the external dimensional characteristics of the device as described are identical to those of the device which is the subject of the applicant's patent EP 929 498. This particularly advantageous arrangement makes it possible to use the device according to the invention with those objects of this patent.

Il va de soi que les divers composants du dispositif selon l'invention seront réalisés dans des matières aptes à résister à la corrosion. Ainsi on pourra utiliser de l'acier inoxydable, du PTFE (POLYTETRAFLUOROETHYLENE°) notamment pour la réalisation de la soupape, ainsi que d'autres matières adaptées.It goes without saying that the various components of the device according to the invention will be made of materials capable of resisting corrosion. Thus one can use stainless steel, PTFE (POLYTETRAFLUOROETHYLENE °) especially for the realization of the valve, as well as other suitable materials.

La présente invention apporte une solution particulièrement simple au problème du dosage des produits pâteux à forte tension superficielle, les essais effectués ont démontré que des précisions de l'ordre du dixième de milligramme sont parfaitement envisageables.The present invention provides a particularly simple solution to the problem of dosing pasty products with high surface tension, the tests carried out have demonstrated that accuracies of the order of a tenth of a milligram are perfectly conceivable.

Il va de soi que la présente invention peut recevoir tous aménagements et variantes du domaine des équivalents techniques sans pour autant sortir du cadre défini par les revendications ci-après.It goes without saying that the present invention can receive any arrangements and variants of the field of technical equivalents without departing from the scope defined by the claims below.

Claims (25)

  1. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products, comprising a device body (1) in which there is formed a conduit (2) for the product to pass from an orifice (3) for introducing the product to a nozzle (4) for delivering the product in dosed quantities, a valve seat (5) being formed in said conduit (2) and a valve (6) being mounted in said conduit so as to be able to slide therein and to be applied against the valve seat (5) in order to prevent the delivery of the product or to be separated from said seat (5) to allow the delivery of the product, the valve (6) being provided with a valve stem (7) slidably mounted in a guide bore (7a) and cooperating with a drive mechanism actuating the valve (6) so as to move away from the seat (5) or towards the valve seat, the product passage conduit (2) comprises a rectilinear segment for the passage of the product, in which segment the valve seat is disposed and the valve (6) and valve stem (7) entirely extend axially and in which segment the valve actuation mechanism at least partly enters, this mechanism being in contact with the product so that the mechanical connection between the valve stem (7) and the actuation mechanism is also in contact with the product and is lubricated by the product itself, the mechanism actuating the valve (6) comprises on the one hand at least one elastic member (8) acting so as to thrust on the valve (6) and biasing the latter towards the seat (5) and therefore towards a closure position and on the other hand an actuation rod (9) guided axially in a bore (10) of the device body, said bore being transverse to the rectilinear passage conduit segment and opening out in said segment, said rod (9) coming into contact with the valve stem (7) in order to act so as to push on the latter, the contact between the valve stem (7) and the actuation mechanism being established by two sliding surfaces (11, 20), one of which (11) is provided on the valve stem (7) and the other (20) on the actuation rod (9), said two surfaces (11, 20) being situated in the rectilinear product passage segment, characterised in that at least one of said surfaces is planar and oblique with respect to the geometric axis of movement of the valve (6) between its open and closed position and oblique with respect to the movement axis of the actuation rod (9), so that, when the actuation rod (9) is moved by a drive member (9a) in the direction of movement into the device body, the valve (6) is separated from its seat (5) under the effect of the push exerted by the sliding surface of the actuation rod (9), on the sliding surface of the valve stem (7).
  2. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 1, characterised in that the oblique sliding surface (11, 20) forms, with the geometric movement axis of the actuation rod (9), an acute angle with a value of less than 45°.
  3. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 1, characterised in that the guide bore (10) of the actuation rod (9) is perpendicular to the product passage section.
  4. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according any one of the preceding claims, characterised in that the rectilinear product passage section is vertical.
  5. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of the preceding claims, characterised in that the product passage conduit (2) is vertical and extends in a rectilinear fashion from an orifice (3) for the entry of the product to an orifice (4) for delivering the latter.
  6. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of the preceding claims, characterised in that the drive member (9a) providing the movement of the actuation rod (9) is external to the device and independent of the latter.
  7. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of the preceding claims, characterised in that the product delivery nozzle (4) is associated with a device (13) for blowing a fluid under pressure in order, under the effect of the blowing or under the effect of the negative pressure or under the effect of the pressure resulting therefrom, to detach the dosing stem attached to the delivery nozzle (4).
  8. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 7, characterised in that the pressurised fluid is blown towards the dosing stem in the form of a pulse.
  9. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 7 or claim 8, characterised in that the pressurised fluid is introduced into the conduit (2) downstream of the seat (5).
  10. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 7 or claim 8, characterised in that the jet of pressurised fluid delivered by the device (13) is external to the conduit (4).
  11. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 10, characterised in that the blowing device (13) is provided with a nozzle (14) for delivering a pressurised fluid and in that the said nozzle (14) is formed around the product delivery nozzle (4).
  12. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 11, characterised in that the product delivery nozzle (4) is formed in a duct (15) and in that the fluid delivery nozzle (14) is formed by a circular opening in an envelope (16a) delimiting a chamber (16) around the duct (15).
  13. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 12, characterised in that the external surface of the duct (15) is frustoconical in shape, the small base of the truncated cone and the pressurised fluid delivery nozzle (14) being disposed in proximity to each other.
  14. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 12, characterised in that the external surface of the nozzle (15) is cylindro-conical in shape, the pressurised fluid delivery nozzle (14) being situated in the immediate proximity of the free end of the cylindrical part.
  15. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 12, characterised in that the internal face of the envelope (16a) has a frustoconical part, the small base of which is formed by the pressurised fluid delivery nozzle (14).
  16. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 15, characterised in that the vertex of the cone corresponding to the frustoconical shape presented by the internal face of the envelope (16) is situated on the axis of symmetry of the conduit (2) close to the product delivery nozzle (4).
  17. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of claims 12, 15, 16, characterised in that the wall of the envelope (16a) is provided with at least one bore (17) for introducing pressurised fluid into the chamber (16).
  18. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of claims 12, 15, 16, 17, characterised in that the nozzle (15) is fixed by screwing into the device body.
  19. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of claims 7 to 18, characterised in that the respective positions of the product delivery nozzle (4) and pressurised fluid delivery nozzle (14) are adjustable with respect to each other.
  20. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of claims 11, 15, 16, 17, 19, characterised in that the chamber (16) of the pressurised fluid blowing device is fixed by screwing to the nozzle (15).
  21. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of claims 7 to 20, characterised in that the fluid used for detaching the dosing stem of the duct is in the gaseous state.
  22. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of claims 7 to 20, characterised in that the fluid used for detaching the dosing stem of the duct is in the liquid state.
  23. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of claims 7 to 20, characterised in that the fluid used for detaching the dosing stem of the duct is in the gaseous state at ambient temperature.
  24. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to any one of claims 7 to 20, characterised in that the fluid used for detaching the dosing stem of the duct is in the liquid state at ambient temperature.
  25. A device for dispensing and dosing viscous, liquid, semiliquid or powdery products according to claim 12, characterised in that it is provided with several ducts, mounted coaxially with each one another, separated from one another, in order to form annular chambers provided with circular openings forming a nozzle, and in that the envelope (16a) of the blowing device (13) is mounted around the outermost nozzle.
EP02718238A 2001-03-02 2002-03-04 Filling head Expired - Lifetime EP1381557B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0103349 2001-03-02
FR0103349A FR2821615B1 (en) 2001-03-02 2001-03-02 DEVICE FOR THE DOSED DELIVERY OF PRECISION OF PASTY OR LIQUID OR POWDER PRODUCTS
PCT/FR2002/000771 WO2002070395A1 (en) 2001-03-02 2002-03-04 Filling head

Publications (2)

Publication Number Publication Date
EP1381557A1 EP1381557A1 (en) 2004-01-21
EP1381557B1 true EP1381557B1 (en) 2006-01-04

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EP02718238A Expired - Lifetime EP1381557B1 (en) 2001-03-02 2002-03-04 Filling head

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US (1) US6860414B2 (en)
EP (1) EP1381557B1 (en)
JP (1) JP4060714B2 (en)
AT (1) ATE315001T1 (en)
DE (1) DE60208535T2 (en)
ES (1) ES2258621T3 (en)
FR (1) FR2821615B1 (en)
WO (1) WO2002070395A1 (en)

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ATE315001T1 (en) 2006-02-15
DE60208535T2 (en) 2006-11-16
JP4060714B2 (en) 2008-03-12
US6860414B2 (en) 2005-03-01
ES2258621T3 (en) 2006-09-01
EP1381557A1 (en) 2004-01-21
WO2002070395A1 (en) 2002-09-12
JP2004530599A (en) 2004-10-07
DE60208535D1 (en) 2006-03-30
US20040149784A1 (en) 2004-08-05
FR2821615B1 (en) 2004-12-03
FR2821615A1 (en) 2002-09-06

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