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EP0744460A3 - Foamed cleaning compositions and method of treating textile fabrics - Google Patents

Foamed cleaning compositions and method of treating textile fabrics Download PDF

Info

Publication number
EP0744460A3
EP0744460A3 EP96202406A EP96202406A EP0744460A3 EP 0744460 A3 EP0744460 A3 EP 0744460A3 EP 96202406 A EP96202406 A EP 96202406A EP 96202406 A EP96202406 A EP 96202406A EP 0744460 A3 EP0744460 A3 EP 0744460A3
Authority
EP
European Patent Office
Prior art keywords
cleaning compositions
textile fabrics
treating textile
foamed cleaning
surfactant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP96202406A
Other languages
German (de)
French (fr)
Other versions
EP0744460A2 (en
Inventor
Jean Wevers
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Procter and Gamble Co
Original Assignee
Procter and Gamble Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co
Priority to EP96202406A priority Critical patent/EP0744460A3/en
Publication of EP0744460A2 publication Critical patent/EP0744460A2/en
Publication of EP0744460A3 publication Critical patent/EP0744460A3/en
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/0005—Other compounding ingredients characterised by their effect
    • C11D3/0094—High foaming compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/65—Mixtures of anionic with cationic compounds
    • C11D1/652—Mixtures of anionic compounds with carboxylic amides or alkylol amides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/86—Mixtures of anionic, cationic, and non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0043—For use with aerosol devices
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/04—Detergent materials or soaps characterised by their shape or physical properties combined with or containing other objects
    • C11D17/048—Soap or detergent bars or cakes with an inner core consisting of insoluble material
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2041—Dihydric alcohols
    • C11D3/2044—Dihydric alcohols linear
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/36—Organic compounds containing phosphorus
    • C11D3/361—Phosphonates, phosphinates or phosphonites
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/04—Carboxylic acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/146—Sulfuric acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/29—Sulfates of polyoxyalkylene ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
    • C11D1/525—Carboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 contain two or more hydroxy groups per alkyl group, e.g. R3 being a reducing sugar rest
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
    • C11D2111/40—Specific cleaning or washing processes
    • C11D2111/42—Application of foam or a temporary coating on the surface to be cleaned

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Treatment Of Fiber Materials (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

The invention relates to a foam composition for cleaning textiles comprising detergent active components, including a surfactant system and from 10% to 82% by weight of detergent builder. The surfactant system consists of anionic surfactant and, optionally, nonionic surfactant, at a level of at least 18% by weight. Preferably both anionic and nonionic surfactants are present in the surfactant system of the foam.
The invention also relates to a method of cleaning textiles using foamed compositions, and also to a packaged product for delivering the foamed compositions.
EP96202406A 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics Withdrawn EP0744460A3 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP96202406A EP0744460A3 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
EP94200867 1994-03-30
EP94200867 1994-03-30
EP96202406A EP0744460A3 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics
EP94870189A EP0677577B1 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics

Related Parent Applications (2)

Application Number Title Priority Date Filing Date
EP94870189.1 Division 1994-12-05
EP94870189A Division EP0677577B1 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics

Publications (2)

Publication Number Publication Date
EP0744460A2 EP0744460A2 (en) 1996-11-27
EP0744460A3 true EP0744460A3 (en) 1999-10-27

Family

ID=26136134

Family Applications (5)

Application Number Title Priority Date Filing Date
EP94870189A Expired - Lifetime EP0677577B1 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics
EP96202406A Withdrawn EP0744460A3 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics
EP96203333A Withdrawn EP0768371A3 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics
EP96202407A Withdrawn EP0744461A3 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics
EP96203332A Withdrawn EP0768368A3 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics

Family Applications Before (1)

Application Number Title Priority Date Filing Date
EP94870189A Expired - Lifetime EP0677577B1 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics

Family Applications After (3)

Application Number Title Priority Date Filing Date
EP96203333A Withdrawn EP0768371A3 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics
EP96202407A Withdrawn EP0744461A3 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics
EP96203332A Withdrawn EP0768368A3 (en) 1994-03-30 1994-12-05 Foamed cleaning compositions and method of treating textile fabrics

Country Status (16)

Country Link
EP (5) EP0677577B1 (en)
JP (1) JPH09511272A (en)
CN (1) CN1105169C (en)
AT (1) ATE242309T1 (en)
AU (1) AU2116295A (en)
BR (1) BR9507336A (en)
CZ (1) CZ286696A3 (en)
DE (1) DE69432785T2 (en)
ES (1) ES2199952T3 (en)
FI (1) FI963875L (en)
HU (1) HUT75204A (en)
MA (1) MA23488A1 (en)
NO (1) NO964069D0 (en)
PE (1) PE44695A1 (en)
TR (1) TR28672A (en)
WO (1) WO1995027026A1 (en)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0753559B1 (en) * 1995-07-13 2004-09-22 The Procter & Gamble Company Method of cleaning textile fabrics
EP0753558A1 (en) * 1995-07-13 1997-01-15 The Procter & Gamble Company Packaged foaming composition
EP0753560A1 (en) * 1995-07-13 1997-01-15 The Procter & Gamble Company Foam
DE69502097T2 (en) * 1995-07-13 1998-11-12 Procter & Gamble Packaged foaming composition
EP0753556B1 (en) * 1995-07-13 2003-10-15 The Procter & Gamble Company Packaged foaming composition
EP0753561B1 (en) * 1995-07-13 2003-05-07 The Procter & Gamble Company Packaged foaming composition
EP0839905A1 (en) 1996-11-05 1998-05-06 The Procter & Gamble Company Foam detergent composition with enzymes
GB9626551D0 (en) * 1996-12-20 1997-02-05 Procter & Gamble Packaged personal cleansing product
AU5609698A (en) * 1996-12-20 1998-07-17 Procter & Gamble Company, The Packaged personal cleansing product
GB9626463D0 (en) * 1996-12-20 1997-02-05 Procter & Gamble Packaged personal cleansing product
GB9626552D0 (en) * 1996-12-20 1997-02-05 Procter & Gamble Packaged personnal cleansing product
EP1037821A1 (en) 1997-08-27 2000-09-27 The Procter & Gamble Company Process for filling pressurised containers and valve therefor
US20070015675A1 (en) * 2005-07-15 2007-01-18 Painter Jeffrey D Self-pressurized spray stain remover
CN101046051B (en) * 2006-03-31 2012-06-27 海尔集团公司 Washing foam with special features used for foam lavation
US20100011511A1 (en) * 2007-02-20 2010-01-21 Novozymes A/S Enzyme Foam Treatment For Laundry
KR20130102536A (en) * 2010-08-30 2013-09-17 노보자임스 에이/에스 A concentrated soak wash
EP2611897A1 (en) * 2010-08-30 2013-07-10 Novozymes A/S A two-soak wash
CN102064740B (en) * 2010-12-08 2013-06-12 上海理工大学 Dish type high-multiple concentrating photovoltaic generating device
WO2018231750A1 (en) 2017-06-13 2018-12-20 The Procter & Gamble Company Process for treating at least one garment
CN111479911A (en) * 2017-12-12 2020-07-31 荷兰联合利华有限公司 Foamable cleaning composition

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3796599A (en) * 1971-07-21 1974-03-12 Center New Prod Dev Inc Method of treating clothers in a clothes dryer with a foam containing an adjuvant material
US3919101A (en) * 1970-03-17 1975-11-11 Colgate Palmolive Co Carpet cleaning composition and method
US4242377A (en) * 1974-02-11 1980-12-30 Colgate-Palmolive Company Fabric conditioning
EP0187004A2 (en) * 1984-12-14 1986-07-09 The Clorox Company Fabric cleaner
US4954286A (en) * 1988-04-14 1990-09-04 Lever Brothers Company Fabric pretreatment cleaning compositions
EP0586295A1 (en) * 1992-08-31 1994-03-09 Nln Quick-foaming, soap-free liquid compositions containing lower hydrocarbons and distributed from a pressurized gas container

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL7014739A (en) * 1970-10-08 1972-04-11
NL7115726A (en) * 1971-11-15 1973-05-17
US3781212A (en) * 1972-10-27 1973-12-25 Townsend & Townsend Aerosol enzyme detergents stabilized with carbon dioxide
GB1500719A (en) * 1974-06-14 1978-02-08 Procter & Gamble Ltd Foaming and conditioning detergent composition
AT344123B (en) 1975-07-02 1978-07-10 Henkel Kgaa METHOD AND DEVICE FOR WASHING TEXTILES
DE2713841A1 (en) * 1976-03-31 1977-10-13 Gillette Co AEROSOL PRODUCT
US4252656A (en) 1978-03-21 1981-02-24 Colgate-Palmolive Company Foam conditioner for fabrics
US4295845A (en) * 1979-06-18 1981-10-20 Lever Brothers Company Pretreatment composition for stain removal
US4457857A (en) * 1980-10-20 1984-07-03 Lever Brothers Company Pretreatment composition for stain removal
JPS58149372A (en) 1982-02-23 1983-09-05 皆川　基 Foam washing method
JPS61197695A (en) * 1985-02-27 1986-09-01 大三工業株式会社 Foaming detergent composition for aerosol
DE3823977A1 (en) * 1988-02-08 1990-01-18 Henkel Kgaa IMPROVED MACHINE WASHING PROCESS FOR DIRTY TEXTILE
US4991751A (en) 1989-12-19 1991-02-12 Precision Valve Corporation Foam actuator for metering an aerosol product
EP0550695B1 (en) * 1990-09-28 1997-07-16 The Procter & Gamble Company Polyhydroxy fatty acid amide surfactants to enhance enzyme performance
AU4786893A (en) * 1992-07-28 1994-02-14 Dowbrands Inc. An instantaneously self-foaming liquid cleansing composition and dispenser therefor
GB9305975D0 (en) 1993-03-23 1993-05-12 Minnesota Mining & Mfg Metered-dose aerosol valves
US5397493A (en) * 1993-07-06 1995-03-14 Lever Brothers Company, Division Of Conopco, Inc. Process for making concentrated heavy duty detergents
US5393468A (en) * 1993-07-14 1995-02-28 Colgate Palmolive Company Hard surface cleaner
US6928094B2 (en) 2002-12-16 2005-08-09 Intel Corporation Laser driver circuit and system

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3919101A (en) * 1970-03-17 1975-11-11 Colgate Palmolive Co Carpet cleaning composition and method
US3796599A (en) * 1971-07-21 1974-03-12 Center New Prod Dev Inc Method of treating clothers in a clothes dryer with a foam containing an adjuvant material
US4242377A (en) * 1974-02-11 1980-12-30 Colgate-Palmolive Company Fabric conditioning
EP0187004A2 (en) * 1984-12-14 1986-07-09 The Clorox Company Fabric cleaner
US4954286A (en) * 1988-04-14 1990-09-04 Lever Brothers Company Fabric pretreatment cleaning compositions
EP0586295A1 (en) * 1992-08-31 1994-03-09 Nln Quick-foaming, soap-free liquid compositions containing lower hydrocarbons and distributed from a pressurized gas container

Also Published As

Publication number Publication date
EP0677577A1 (en) 1995-10-18
EP0744461A3 (en) 1999-10-20
BR9507336A (en) 1997-09-16
DE69432785D1 (en) 2003-07-10
HUT75204A (en) 1997-04-28
MX9604517A (en) 1997-09-30
NO964069L (en) 1996-09-27
AU2116295A (en) 1995-10-23
CN1105169C (en) 2003-04-09
EP0768371A2 (en) 1997-04-16
JPH09511272A (en) 1997-11-11
EP0768368A2 (en) 1997-04-16
PE44695A1 (en) 1996-01-18
EP0744460A2 (en) 1996-11-27
EP0677577B1 (en) 2003-06-04
MA23488A1 (en) 1995-10-01
WO1995027026A1 (en) 1995-10-12
DE69432785T2 (en) 2004-04-29
NO964069D0 (en) 1996-09-27
HU9602659D0 (en) 1996-11-28
EP0768371A3 (en) 1999-10-27
EP0744461A2 (en) 1996-11-27
FI963875A0 (en) 1996-09-27
EP0768368A3 (en) 1999-10-27
TR28672A (en) 1997-01-31
CZ286696A3 (en) 1997-02-12
FI963875A7 (en) 1996-09-27
FI963875L (en) 1996-09-27
CN1148867A (en) 1997-04-30
ATE242309T1 (en) 2003-06-15
ES2199952T3 (en) 2004-03-01

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