DK726988D0 - PROCEDURES FOR DECAFFINING COFFEE WITH AN OVERCritical Fluid - Google Patents
PROCEDURES FOR DECAFFINING COFFEE WITH AN OVERCritical FluidInfo
- Publication number
- DK726988D0 DK726988D0 DK726988A DK726988A DK726988D0 DK 726988 D0 DK726988 D0 DK 726988D0 DK 726988 A DK726988 A DK 726988A DK 726988 A DK726988 A DK 726988A DK 726988 D0 DK726988 D0 DK 726988D0
- Authority
- DK
- Denmark
- Prior art keywords
- caffeine
- supercritical fluid
- beans
- coffee
- decaffining
- Prior art date
Links
- 239000012530 fluid Substances 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 2
- 235000010627 Phaseolus vulgaris Nutrition 0.000 abstract 2
- 244000046052 Phaseolus vulgaris Species 0.000 abstract 2
- 241000533293 Sesbania emerus Species 0.000 abstract 2
- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 abstract 2
- 238000000605 extraction Methods 0.000 abstract 2
- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000006096 absorbing agent Substances 0.000 abstract 1
- 238000010923 batch production Methods 0.000 abstract 1
- 229960001948 caffeine Drugs 0.000 abstract 1
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 abstract 1
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 1
- 239000001569 carbon dioxide Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/20—Reducing or removing alkaloid content; Preparations produced thereby; Extracts or infusions thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/20—Reducing or removing alkaloid content; Preparations produced thereby; Extracts or infusions thereof
- A23F5/206—Reducing or removing alkaloid content; Preparations produced thereby; Extracts or infusions thereof by extraction of the beans with selective solvents other than water or aqueous bean extracts, including supercritical gases
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Tea And Coffee (AREA)
- Apparatus For Making Beverages (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Telephonic Communication Services (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
A method of extracting caffeine from green coffee beans whereby an essentially caffeine-free supercritical fluid is continuously fed to one end of an extraction vessel containing green coffee beans and caffeine-laden supercritical fluid is continuously withdrawn from the opposite end. A portion of decaffeinated beans is periodically discharged while a fresh portion of undecaffeinated beans is essentially simultaneously charged to the extraction vessel. The caffeine-laden supercritical fluid is fed to a countercurrent water absorber. Supercritical carbon dioxide is the preferred supercritical fluid. The method of the present invention is more efficient than batch processes and produces an improved decaffeinated coffee.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/166,748 US4820537A (en) | 1987-03-13 | 1988-03-08 | Method for decaffeinating coffee with a supercritical fluid |
Publications (2)
Publication Number | Publication Date |
---|---|
DK726988D0 true DK726988D0 (en) | 1988-12-29 |
DK726988A DK726988A (en) | 1989-09-15 |
Family
ID=22604555
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DK726988A DK726988A (en) | 1988-03-08 | 1988-12-29 | PROCEDURES FOR DECAFFINING COFFEE WITH AN OVERCritical Fluid |
Country Status (15)
Country | Link |
---|---|
US (1) | US4820537A (en) |
EP (1) | EP0331852B1 (en) |
JP (1) | JP2763905B2 (en) |
KR (1) | KR960007092B1 (en) |
CN (1) | CN1024318C (en) |
AT (1) | ATE92269T1 (en) |
AU (1) | AU614325B2 (en) |
DE (1) | DE3882965T2 (en) |
DK (1) | DK726988A (en) |
ES (1) | ES2042775T3 (en) |
FI (1) | FI886029L (en) |
IE (1) | IE62173B1 (en) |
MY (1) | MY109308A (en) |
NO (1) | NO171703C (en) |
PH (1) | PH24380A (en) |
Families Citing this family (30)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3744329A1 (en) * | 1987-12-28 | 1989-07-06 | Schwarz Pharma Gmbh | METHOD FOR THE PRODUCTION OF AT LEAST ONE ACTIVE AGENT AND A TRAITER COMPRISING PREPARATION |
US4911941A (en) * | 1988-08-05 | 1990-03-27 | General Foods Corporation | Method for decaffeinating coffee with a supercritical fluid |
US4996317A (en) * | 1988-08-05 | 1991-02-26 | Kraft General Foods, Inc. | Caffeine recovery from supercritical carbon dioxide |
DE4003483A1 (en) * | 1989-02-09 | 1990-08-16 | Schoeller Bleckmann Stahlwerke | Caffeine removal from raw coffee - by extn. with supercritical carbon di:oxide super-satd. with water |
US4951561A (en) * | 1989-06-06 | 1990-08-28 | Kraft General Foods, Inc. | Apparatus for fluid-solid bed processing |
US4956176A (en) * | 1989-06-20 | 1990-09-11 | Kraft General Foods, Inc. | Solids-fluid contacting apparatus with screen at fluid outlet |
US4929462A (en) * | 1989-06-21 | 1990-05-29 | Kraft General Foods, Inc. | Method and apparatus for continuous contact of supercritical fluid with particulate solids |
ATE101971T1 (en) * | 1990-01-25 | 1994-03-15 | Gen Foods Inc | PROCESS FOR THE EXTRACTION OF ROAST AND GROUND COFFEE BEANS. |
US5288511A (en) * | 1990-08-23 | 1994-02-22 | Liquid Carbonic Corporation | Supercritical carbon dioxide decaffeination of acidified coffee |
US5279615A (en) * | 1991-06-14 | 1994-01-18 | The Clorox Company | Method and composition using densified carbon dioxide and cleaning adjunct to clean fabrics |
US5431843A (en) * | 1991-09-04 | 1995-07-11 | The Clorox Company | Cleaning through perhydrolysis conducted in dense fluid medium |
US5267455A (en) * | 1992-07-13 | 1993-12-07 | The Clorox Company | Liquid/supercritical carbon dioxide dry cleaning system |
DE4241487C2 (en) * | 1992-12-09 | 1996-07-25 | Indena Spa | New extracts of Cucurbita sp., Process for their preparation and their use in medicines and cosmetics |
DE4400096C2 (en) * | 1994-01-04 | 1997-06-12 | Barth Raiser Hopfenextraktion | Process for decaffeinating black tea |
US5490884A (en) * | 1994-09-09 | 1996-02-13 | Tastemaker | Method and system for extracting a solute from a fluid using dense gas and a porous membrane |
DE19524481C2 (en) * | 1995-07-05 | 2000-03-02 | Hopfenextraktion Hvg Barth, Raiser & Co | Procedure for decaffeinating black tea |
DE19810565A1 (en) | 1998-03-11 | 1999-09-16 | Basf Ag | Economical drying of microporous particles containing fluid e.g. inorganic, organic or polymer gel |
US6117431A (en) * | 1999-12-03 | 2000-09-12 | Pharmline Inc. | Method for obtaining an extract from ginkgo biloba leaves |
US20070225514A1 (en) * | 2006-03-27 | 2007-09-27 | Michael Wayne Davis | Method for drying organic material employing a supercritical carbon dioxide process |
US20070254076A1 (en) * | 2006-03-27 | 2007-11-01 | Bobier James E Jr | Method for extracting and recovery of water from organic materials employing supercritical carbon dioxide utilizing a heat exchanger system |
KR101790800B1 (en) * | 2009-07-21 | 2017-10-26 | 인터컨티넨탈 그레이트 브랜즈 엘엘씨 | Crude caffeine complex, improved food products using the crude caffeine complex, and methods of use thereof |
CN103313613B (en) | 2010-10-13 | 2016-04-06 | 洲际大品牌有限责任公司 | As the coffee-extract of the composition of food, medicine, cosmetics, dietary supplements and biological products |
KR102465498B1 (en) | 2014-12-02 | 2022-11-09 | 카오카부시키가이샤 | Roasted coffee beans |
IN2015MU00086A (en) | 2015-01-09 | 2015-04-10 | Deven Supercriticals Pvt Ltd | |
EP3165099A1 (en) * | 2015-11-03 | 2017-05-10 | Evonik Degussa GmbH | Removing oil and simultaneous removal of unwanted contaminants from beans with supercritical co2 |
EP3175897B1 (en) | 2015-12-04 | 2018-04-04 | Evonik Degussa GmbH | Improved method for the extraction of aromatic substances from fat-containing and/or aqueous liquid phases |
NZ750840A (en) * | 2016-08-22 | 2022-05-27 | Suntory Holdings Ltd | Coffee beans with high fatty acid methyl ester content |
US10758579B2 (en) | 2016-12-07 | 2020-09-01 | Metagreen Ventures | Systems and methods for extraction of natural products |
CN111758827A (en) * | 2020-07-17 | 2020-10-13 | 上海旭梅食品科技股份有限公司 | Coffee extract, preparation method thereof and beverage |
US12227505B2 (en) * | 2021-02-03 | 2025-02-18 | James Khreibani | Supercritical fluid extraction process with integrated pressure exchanger |
Family Cites Families (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2309139A (en) * | 1941-01-03 | 1943-01-26 | Gen Foods Corp | Process and apparatus for decaffeinating coffee |
US3092515A (en) * | 1959-09-14 | 1963-06-04 | Research Corp | Moving-bed liquid-solid contactor and operation thereof |
US3088394A (en) * | 1961-03-22 | 1963-05-07 | John H R Thornhill | Apparatus for extracting soluble constituents from vegetable matter |
DE1493190C3 (en) * | 1963-04-16 | 1980-10-16 | Studiengesellschaft Kohle Mbh, 4330 Muelheim | Process for the separation of mixtures of substances |
CH535543A (en) * | 1970-02-05 | 1973-04-15 | Studiengesellschaft Kohle Mbh | Process for decaffeinating green coffee |
AT313039B (en) * | 1971-05-07 | 1974-01-25 | Studiengesellschaft Kohle Mbh | Process for obtaining caffeine from green coffee |
US3862347A (en) * | 1972-06-30 | 1975-01-21 | Gen Foods Corp | Solid-liquid packed bed extraction |
CA1048940A (en) * | 1974-07-31 | 1979-02-20 | Gunther Gappa | Activated-carbon water purification controlled by analysis of carbon content in water |
US4247570A (en) * | 1976-08-04 | 1981-01-27 | Studiengesellschaft Kohle Mbh | Process for the decaffeination of coffee |
DE2637197C2 (en) * | 1976-08-18 | 1983-01-27 | Hag Ag, 2800 Bremen | Process for the removal of caffeine from natural substances containing caffeine with a supercritical extractant |
DE2639066A1 (en) * | 1976-08-30 | 1978-03-02 | Hag Ag | METHOD OF REMOVING IRRITANTS FROM COFFEE |
DE2727191B2 (en) * | 1977-06-16 | 1980-07-03 | Hag Ag, 2800 Bremen | Process for the selective extraction of caffeine from plant materials |
NL187665C (en) * | 1977-08-05 | 1991-12-16 | D E J Int Research | METHOD FOR REMOVING CAFFEINE FROM AN AQUEOUS COFFEE OR TEA EXTRACT AND METHOD FOR REMOVING CAFFEINE FROM GREEN COFFEE BEANS. |
DE2737793A1 (en) * | 1977-08-22 | 1979-03-08 | Peter Siegfried | Decaffeination of raw coffee - by selective extraction of caffeine with extractant and compressed gas at elevated temp. and pressure |
NL7712503A (en) * | 1977-11-14 | 1979-05-16 | D E J Int Research | PROCEDURE FOR DECAFFINING GREEN COFFEE BEANS. |
US4348422A (en) * | 1978-02-13 | 1982-09-07 | Studiengesellschaft Kohle M.B.H. | Process for the direct decaffeination of aqueous coffee extract solutions |
US4322445A (en) * | 1978-08-14 | 1982-03-30 | Siegfried Peter | Process for decaffeinating coffee |
EP0010636A1 (en) * | 1978-11-06 | 1980-05-14 | Societe Des Produits Nestle S.A. | Caffeine extraction |
US4251559A (en) * | 1978-11-06 | 1981-02-17 | Societe D'assistance Technique Pour Produits Nestle S.A. | Decaffeination process |
US4341804A (en) * | 1979-03-26 | 1982-07-27 | General Foods Corporation | Decaffeination of aqueous roasted coffee extract |
US4246291A (en) * | 1979-03-26 | 1981-01-20 | General Foods Corporation | Decaffeination of aqueous extracts |
US4481223A (en) * | 1983-10-13 | 1984-11-06 | General Foods Corporation | Decaffeination with treated activated carbon |
DE3445502A1 (en) * | 1983-12-13 | 1985-06-20 | Cafe Toro Ltda., Bogota | Process and device for decaffeinating green coffee |
DE3532957A1 (en) * | 1985-09-14 | 1987-03-19 | Metallgesellschaft Ag | METHOD AND DEVICE FOR EXTRACTING VALUABLES FROM GRAINY USE |
-
1988
- 1988-03-08 US US07/166,748 patent/US4820537A/en not_active Expired - Lifetime
- 1988-12-21 CN CN89100853A patent/CN1024318C/en not_active Expired - Fee Related
- 1988-12-22 AT AT88312257T patent/ATE92269T1/en not_active IP Right Cessation
- 1988-12-22 DE DE88312257T patent/DE3882965T2/en not_active Expired - Fee Related
- 1988-12-22 ES ES88312257T patent/ES2042775T3/en not_active Expired - Lifetime
- 1988-12-22 EP EP88312257A patent/EP0331852B1/en not_active Expired - Lifetime
- 1988-12-28 NO NO885793A patent/NO171703C/en unknown
- 1988-12-29 DK DK726988A patent/DK726988A/en not_active Application Discontinuation
- 1988-12-29 FI FI886029A patent/FI886029L/en not_active Application Discontinuation
-
1989
- 1989-01-24 IE IE20289A patent/IE62173B1/en not_active IP Right Cessation
- 1989-01-25 AU AU28826/89A patent/AU614325B2/en not_active Ceased
- 1989-01-25 MY MYPI89000086A patent/MY109308A/en unknown
- 1989-01-27 KR KR1019890000878A patent/KR960007092B1/en not_active IP Right Cessation
- 1989-02-06 PH PH38161A patent/PH24380A/en unknown
- 1989-03-07 JP JP1054861A patent/JP2763905B2/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
NO171703B (en) | 1993-01-18 |
CN1024318C (en) | 1994-04-27 |
EP0331852A2 (en) | 1989-09-13 |
EP0331852B1 (en) | 1993-08-04 |
NO885793L (en) | 1989-09-11 |
IE62173B1 (en) | 1994-12-28 |
DK726988A (en) | 1989-09-15 |
ES2042775T3 (en) | 1993-12-16 |
CN1036125A (en) | 1989-10-11 |
JP2763905B2 (en) | 1998-06-11 |
MY109308A (en) | 1997-01-31 |
NO885793D0 (en) | 1988-12-28 |
KR960007092B1 (en) | 1996-05-27 |
NO171703C (en) | 1993-04-28 |
AU2882689A (en) | 1989-09-14 |
ATE92269T1 (en) | 1993-08-15 |
US4820537A (en) | 1989-04-11 |
IE890202L (en) | 1989-09-08 |
DE3882965D1 (en) | 1993-09-09 |
EP0331852A3 (en) | 1990-12-19 |
DE3882965T2 (en) | 1994-02-24 |
AU614325B2 (en) | 1991-08-29 |
FI886029L (en) | 1989-09-09 |
PH24380A (en) | 1990-06-13 |
JPH01309640A (en) | 1989-12-14 |
KR890013997A (en) | 1989-10-21 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ATS | Application withdrawn |