DE915505C - Verfahren zur Herstellung harzartiger Kondensationsprodukte - Google Patents
Verfahren zur Herstellung harzartiger KondensationsprodukteInfo
- Publication number
- DE915505C DE915505C DEB7485D DEB0007485D DE915505C DE 915505 C DE915505 C DE 915505C DE B7485 D DEB7485 D DE B7485D DE B0007485 D DEB0007485 D DE B0007485D DE 915505 C DE915505 C DE 915505C
- Authority
- DE
- Germany
- Prior art keywords
- preparation
- condensation products
- resinous condensation
- resinous
- compounds
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 4
- 239000007859 condensation product Substances 0.000 title description 3
- 238000002360 preparation method Methods 0.000 title 1
- 150000001875 compounds Chemical class 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 239000010687 lubricating oil Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 claims description 2
- 150000008282 halocarbons Chemical class 0.000 claims 1
- 229910015900 BF3 Inorganic materials 0.000 description 5
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 description 5
- PAAZPARNPHGIKF-UHFFFAOYSA-N 1,2-dibromoethane Chemical compound BrCCBr PAAZPARNPHGIKF-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 150000001722 carbon compounds Chemical class 0.000 description 2
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- 239000010721 machine oil Substances 0.000 description 2
- 239000012261 resinous substance Substances 0.000 description 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- 239000003502 gasoline Substances 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M1/00—Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants
- C10M1/08—Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants with additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F240/00—Copolymers of hydrocarbons and mineral oils, e.g. petroleum resins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F257/00—Macromolecular compounds obtained by polymerising monomers on to polymers of aromatic monomers as defined in group C08F12/00
- C08F257/02—Macromolecular compounds obtained by polymerising monomers on to polymers of aromatic monomers as defined in group C08F12/00 on to polymers of styrene or alkyl-substituted styrenes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
- C08G61/02—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G50/00—Production of liquid hydrocarbon mixtures from lower carbon number hydrocarbons, e.g. by oligomerisation
- C10G50/02—Production of liquid hydrocarbon mixtures from lower carbon number hydrocarbons, e.g. by oligomerisation of hydrocarbon oils for lubricating purposes
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/04—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing aromatic monomers, e.g. styrene
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/22—Alkylation reaction products with aromatic type compounds, e.g. Friedel-crafts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/02—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/101—Condensation polymers of aldehydes or ketones and phenols, e.g. Also polyoxyalkylene ether derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Lubricants (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
- Verfahren zur Herstellung harzartiger Kondensationsprodukte Gegenstand des Patents 727 116 ist ein Verfahren zur Herstellung von harzartigen, insbesondere als Schmierölverbesserungsmittel geeigneten Verbindungen, nach dem ungesättigte Kohlenstoffverbindungen mit einen Kohlenstoffring enthaltenden harzartigen Stoffen in Gegenwart von Lösungsmitteln, die im wesentlichen aus Chlorkohlenwasserstoffen oder chlorierten Äthern bestehen, unter Vermittlung von Borfluorid oder einer mit Fluorverbindungen behandelten Bleicherde in Reaktion gebracht werden.
- Es wurde nun gefunden, daß man an Stelle der im Hauptpatent erwähnten Chlorverbindungen auch die entsprechenden Verbindungen der übrigen Halogene, insbesondere von Brom und Jod, verwenden kann. Diese Verbindungen besitzen ebenso wie die Chlorverbindungen ein gutes Lösungsvermögen für Borfluorid und erleichtern dadurch die Umsetzung von ungesättigten Kohlenwasserstoffen mit harzartigen Stoffen unter dem Einfluß von Borfluorid. Beispiel In eine Mischung von 67 kg eines durch Spalten von Paraffin gewonnenen, an ungesättigten Kohlenstoffverbindungen reichen Produktes mit 33 kg Polystyrol und 75 1 Äthy lenbromid wird unter Rühren bei 30 bis 4o° während 8 Stunden Borfluorid eingeleitet. Das Kondensationsprodukt wird in 18o kg Maschinenöl (Viskosität 8,5° E/50°) unter Erwärmen auf r5o° gelöst und zur Entfernung von Äthylenbromid und Borfluorid mit überhitztem Wasserdampf behandelt. Setzt man zu einem deutschen Maschinenöl 311/o des so erhaltenen Produktes zu, so steigt die Viskosität des Schmieröls von i,6'° E auf r,96° E/99° und der Viskositätsindex von 5o auf go. Verwendet man als Lösungsmittel statt Äthylenbromid Benzol, Benzin, Äther, Ketone oder Alkohole oder arbeitet man überhaupt in Abwesenheit von Lösungsmitteln, so entstehen keine hochviskosen Produkte.
Claims (1)
- PATENTANSPRUCH: Verfahren zur Herstellung von harzartigen, insbesondere als Schmierölverbesserungsmittel geeigneten Verbindungen nach Patent 727 116, dadurch gekennzeichnet, daß als Lösungsmittel andere Halogenkohlenwasserstoffe als Chlorkohlenwasserstoffe verwendet werden.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEI58939D DE727116C (de) | 1937-08-28 | 1937-08-28 | Verfahren zur Herstellung harzartiger Kondensationsprodukte |
| DEB7485D DE915505C (de) | 1937-08-28 | 1937-09-11 | Verfahren zur Herstellung harzartiger Kondensationsprodukte |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEI58939D DE727116C (de) | 1937-08-28 | 1937-08-28 | Verfahren zur Herstellung harzartiger Kondensationsprodukte |
| DEB7485D DE915505C (de) | 1937-08-28 | 1937-09-11 | Verfahren zur Herstellung harzartiger Kondensationsprodukte |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE915505C true DE915505C (de) | 1954-07-22 |
Family
ID=34634941
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEI58939D Expired DE727116C (de) | 1937-08-28 | 1937-08-28 | Verfahren zur Herstellung harzartiger Kondensationsprodukte |
| DEB7485D Expired DE915505C (de) | 1937-08-28 | 1937-09-11 | Verfahren zur Herstellung harzartiger Kondensationsprodukte |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEI58939D Expired DE727116C (de) | 1937-08-28 | 1937-08-28 | Verfahren zur Herstellung harzartiger Kondensationsprodukte |
Country Status (1)
| Country | Link |
|---|---|
| DE (2) | DE727116C (de) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE900736C (de) * | 1948-07-16 | 1954-01-04 | Monsanto Chemicals | Schmiermittel und Verfahren zu ihrer Herstellung |
| DE1079327B (de) * | 1953-09-17 | 1960-04-07 | Exxon Research Engineering Co | Verfahren zur Isolierung thermoplastischer Mischpolymerer vom Styrol-Isobutylen-Typ |
-
1937
- 1937-08-28 DE DEI58939D patent/DE727116C/de not_active Expired
- 1937-09-11 DE DEB7485D patent/DE915505C/de not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE727116C (de) | 1942-10-27 |
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