DE69904757D1 - METHOD FOR PRODUCING SINTERABLE METAL POWDER FROM TUNGSTEN AND COPPER - Google Patents
METHOD FOR PRODUCING SINTERABLE METAL POWDER FROM TUNGSTEN AND COPPERInfo
- Publication number
- DE69904757D1 DE69904757D1 DE69904757T DE69904757T DE69904757D1 DE 69904757 D1 DE69904757 D1 DE 69904757D1 DE 69904757 T DE69904757 T DE 69904757T DE 69904757 T DE69904757 T DE 69904757T DE 69904757 D1 DE69904757 D1 DE 69904757D1
- Authority
- DE
- Germany
- Prior art keywords
- tungsten
- copper
- metal powder
- reduction
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 title abstract 4
- 229910052721 tungsten Inorganic materials 0.000 title abstract 4
- 239000010937 tungsten Substances 0.000 title abstract 4
- 239000000843 powder Substances 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 229910052751 metal Inorganic materials 0.000 title abstract 2
- 239000002184 metal Substances 0.000 title abstract 2
- 239000012691 Cu precursor Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 1
- 239000002131 composite material Substances 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 239000010949 copper Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
- 229920005862 polyol Polymers 0.000 abstract 1
- 150000003077 polyols Chemical class 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/16—Making metallic powder or suspensions thereof using chemical processes
- B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
- B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/17—Metallic particles coated with metal
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/04—Making non-ferrous alloys by powder metallurgy
- C22C1/045—Alloys based on refractory metals
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01H—ELECTRIC SWITCHES; RELAYS; SELECTORS; EMERGENCY PROTECTIVE DEVICES
- H01H1/00—Contacts
- H01H1/02—Contacts characterised by the material thereof
- H01H1/021—Composite material
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Powder Metallurgy (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
Method for the production of a composite powder consisting of finely interspersed tungsten and copper, which powder can be directly pressed and sintered to provide products having density values exceeding 96 % with respect to the theoretical one and high values for electrical and thermal conductivity, the method essentially comprising the reduction of a copper precursor in the presence of tungsten metal suspended in an organic liquid phase produced by one or a mixture of polyols. The reaction is carried out by heating the suspension to a temperature of at least 60 DEG C and keeping it at a such temperature for a sufficient time to bring about the reduction of the copper precursor by means of the organic phase and tungsten therein.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT1998RM000776A IT1302926B1 (en) | 1998-12-16 | 1998-12-16 | PROCEDURE FOR THE PRODUCTION OF TUNGSTEN-RAMESINTERIZABLE COMPOSITE POWDERS. |
PCT/IT1999/000321 WO2000035616A1 (en) | 1998-12-16 | 1999-10-12 | Process for the production of tungsten-copper composite sinterable powders |
Publications (1)
Publication Number | Publication Date |
---|---|
DE69904757D1 true DE69904757D1 (en) | 2003-02-06 |
Family
ID=11406255
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69904757T Expired - Lifetime DE69904757D1 (en) | 1998-12-16 | 1999-10-12 | METHOD FOR PRODUCING SINTERABLE METAL POWDER FROM TUNGSTEN AND COPPER |
Country Status (7)
Country | Link |
---|---|
EP (1) | EP1140397B1 (en) |
AT (1) | ATE230321T1 (en) |
AU (1) | AU1073800A (en) |
CZ (1) | CZ20012180A3 (en) |
DE (1) | DE69904757D1 (en) |
IT (1) | IT1302926B1 (en) |
WO (1) | WO2000035616A1 (en) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10041194A1 (en) | 2000-08-23 | 2002-03-07 | Starck H C Gmbh | Process for the production of composite components by powder injection molding and suitable composite powder |
CN100402204C (en) * | 2003-01-21 | 2008-07-16 | 奥斯兰姆施尔凡尼亚公司 | Electrochemical displacement-deposition method for preparing composite metal powder |
CN102554218A (en) * | 2011-11-23 | 2012-07-11 | 西安理工大学 | Method for preparing tungsten-copper composite powder by means of electroless copper plating |
CN104722753B (en) * | 2015-03-24 | 2017-01-18 | 中国石油集团川庆钻探工程有限公司 | Preparation method of tungsten-copper powder for shaped charge cover of perforating charge |
US10737248B2 (en) * | 2018-06-26 | 2020-08-11 | Uop Llc | Crystalline transition metal tungstate |
CN113020588B (en) * | 2021-02-26 | 2023-02-24 | 西安稀有金属材料研究院有限公司 | Preparation method of graphene oxide doped tungsten-copper core-shell structure material |
CN113523295B (en) * | 2021-07-20 | 2023-01-17 | 天津大学 | A preparation method of copper-coated tungsten spherical composite powder for additive manufacturing |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2537898A1 (en) * | 1982-12-21 | 1984-06-22 | Univ Paris | METHOD FOR REDUCING METAL COMPOUNDS BY THE POLYOLS, AND METAL POWDERS OBTAINED BY THIS PROCESS |
GB2236117A (en) * | 1989-09-20 | 1991-03-27 | Shell Int Research | Process for preparing silver powder |
US5439638A (en) * | 1993-07-16 | 1995-08-08 | Osram Sylvania Inc. | Method of making flowable tungsten/copper composite powder |
FR2723015B1 (en) * | 1994-07-29 | 1996-09-13 | Commissariat Energie Atomique | PROCESS FOR OBTAINING IRON OR IRON POWDERS BY ORGANIC LIQUID PHASE PRECIPITATION |
US5759230A (en) * | 1995-11-30 | 1998-06-02 | The United States Of America As Represented By The Secretary Of The Navy | Nanostructured metallic powders and films via an alcoholic solvent process |
-
1998
- 1998-12-16 IT IT1998RM000776A patent/IT1302926B1/en active IP Right Grant
-
1999
- 1999-10-12 AT AT99954333T patent/ATE230321T1/en not_active IP Right Cessation
- 1999-10-12 CZ CZ20012180A patent/CZ20012180A3/en unknown
- 1999-10-12 WO PCT/IT1999/000321 patent/WO2000035616A1/en not_active Application Discontinuation
- 1999-10-12 AU AU10738/00A patent/AU1073800A/en not_active Abandoned
- 1999-10-12 DE DE69904757T patent/DE69904757D1/en not_active Expired - Lifetime
- 1999-10-12 EP EP99954333A patent/EP1140397B1/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
AU1073800A (en) | 2000-07-03 |
EP1140397A1 (en) | 2001-10-10 |
WO2000035616A1 (en) | 2000-06-22 |
ATE230321T1 (en) | 2003-01-15 |
EP1140397B1 (en) | 2003-01-02 |
ITRM980776A1 (en) | 2000-06-16 |
IT1302926B1 (en) | 2000-10-10 |
CZ20012180A3 (en) | 2002-03-13 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8332 | No legal effect for de |