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DE69832209D1 - Verfahren zur Herstellung von 3,3-Dimethylbutyraldehyd durch Oxidation von 3,3-Dimethylbutanol - Google Patents

Verfahren zur Herstellung von 3,3-Dimethylbutyraldehyd durch Oxidation von 3,3-Dimethylbutanol

Info

Publication number
DE69832209D1
DE69832209D1 DE69832209T DE69832209T DE69832209D1 DE 69832209 D1 DE69832209 D1 DE 69832209D1 DE 69832209 T DE69832209 T DE 69832209T DE 69832209 T DE69832209 T DE 69832209T DE 69832209 D1 DE69832209 D1 DE 69832209D1
Authority
DE
Germany
Prior art keywords
dimethylbutanol
dimethylbutyraldehyde
oxidation
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69832209T
Other languages
English (en)
Other versions
DE69832209T2 (de
Inventor
Indra Prakash
David J Ager
Alan R Katrizky
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nutrasweet Co
Original Assignee
Nutrasweet Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nutrasweet Co filed Critical Nutrasweet Co
Application granted granted Critical
Publication of DE69832209D1 publication Critical patent/DE69832209D1/de
Publication of DE69832209T2 publication Critical patent/DE69832209T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/29Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
    • C07C45/298Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups with manganese derivatives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/002Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by dehydrogenation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/29Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/29Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups
    • C07C45/294Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of hydroxy groups with hydrogen peroxide
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/30Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with halogen containing compounds, e.g. hypohalogenation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69832209T 1997-08-06 1998-08-04 Verfahren zur Herstellung von 3,3-Dimethylbutyraldehyd durch Oxidation von 3,3-Dimethylbutanol Expired - Lifetime DE69832209T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/907,048 US5856584A (en) 1997-08-06 1997-08-06 Preparation of 3,3-dimethylbutyraldehyde by oxidation of 3, 3-dimethylbutanol
US907048 1997-08-06

Publications (2)

Publication Number Publication Date
DE69832209D1 true DE69832209D1 (de) 2005-12-08
DE69832209T2 DE69832209T2 (de) 2006-07-27

Family

ID=25423434

Family Applications (2)

Application Number Title Priority Date Filing Date
DE69832209T Expired - Lifetime DE69832209T2 (de) 1997-08-06 1998-08-04 Verfahren zur Herstellung von 3,3-Dimethylbutyraldehyd durch Oxidation von 3,3-Dimethylbutanol
DE69819164T Expired - Lifetime DE69819164T2 (de) 1997-08-06 1998-08-04 Verfahren zur herstellung von 3,3-dimethylbutyraldehyd durch oxidation von 3,3-dimethylbutanol

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE69819164T Expired - Lifetime DE69819164T2 (de) 1997-08-06 1998-08-04 Verfahren zur herstellung von 3,3-dimethylbutyraldehyd durch oxidation von 3,3-dimethylbutanol

Country Status (17)

Country Link
US (1) US5856584A (de)
EP (2) EP1186591B1 (de)
JP (3) JP2001525384A (de)
KR (2) KR100622438B1 (de)
CN (2) CN1286790C (de)
AR (1) AR016582A1 (de)
AT (1) ATE252532T1 (de)
AU (1) AU749936B2 (de)
BR (1) BR9811854B1 (de)
CA (2) CA2299637C (de)
DE (2) DE69832209T2 (de)
ES (2) ES2246978T3 (de)
HU (1) HUP0003631A3 (de)
IL (1) IL134374A0 (de)
PE (1) PE96699A1 (de)
UY (1) UY25126A1 (de)
WO (1) WO1999029646A1 (de)

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US5856584A (en) * 1997-08-06 1999-01-05 The Nutrasweet Company Preparation of 3,3-dimethylbutyraldehyde by oxidation of 3, 3-dimethylbutanol
US6573409B1 (en) 1999-07-02 2003-06-03 The Nutrasweet Company Process for the preparation of 3,3-dimethylbutanal
DE50002160D1 (de) 1999-11-19 2003-06-18 Ciba Sc Holding Ag Verfahren zur selektiven Oxidation von Alkoholen unter Verwendung leicht abtrennbarer Nitroxylradikale
US7838708B2 (en) 2001-06-20 2010-11-23 Grt, Inc. Hydrocarbon conversion process improvements
DE602004032212D1 (de) * 2003-01-30 2011-05-26 Nutrasweet Property Holdings Inc Bromfreies katalysatorsystem auftempo-basis zur oxidation primärer und sekundärer alkohole mit naoci alsoxidationsmittel
WO2005021468A1 (en) 2003-07-15 2005-03-10 Grt, Inc. Hydrocarbon synthesis
US20050171393A1 (en) 2003-07-15 2005-08-04 Lorkovic Ivan M. Hydrocarbon synthesis
US6825384B1 (en) * 2004-01-29 2004-11-30 The Nutrasweet Company Bromine free TEMPO based catalyst system for oxidation of primary and secondary alcohols using NaOCl as an oxidant
KR20060129510A (ko) * 2004-02-26 2006-12-15 더 뉴트라스위트 컴퍼니 일차 및 이차 알콜의 호기성 산화를 위한 촉매계
US7244867B2 (en) 2004-04-16 2007-07-17 Marathon Oil Company Process for converting gaseous alkanes to liquid hydrocarbons
US8642822B2 (en) 2004-04-16 2014-02-04 Marathon Gtf Technology, Ltd. Processes for converting gaseous alkanes to liquid hydrocarbons using microchannel reactor
US20080275284A1 (en) 2004-04-16 2008-11-06 Marathon Oil Company Process for converting gaseous alkanes to liquid hydrocarbons
US7674941B2 (en) 2004-04-16 2010-03-09 Marathon Gtf Technology, Ltd. Processes for converting gaseous alkanes to liquid hydrocarbons
US8173851B2 (en) 2004-04-16 2012-05-08 Marathon Gtf Technology, Ltd. Processes for converting gaseous alkanes to liquid hydrocarbons
US20060100469A1 (en) 2004-04-16 2006-05-11 Waycuilis John J Process for converting gaseous alkanes to olefins and liquid hydrocarbons
JP2006182764A (ja) * 2004-12-03 2006-07-13 Daiso Co Ltd 第1級または第2級アルコールの新規酸化方法
DE102005030728A1 (de) * 2005-07-01 2007-01-04 Lanxess Deutschland Gmbh Verfahren zur Ruthenium-katalysierten Oxidation von Alkoholen mit Hypochlorit
UA95943C2 (ru) 2006-02-03 2011-09-26 ДжиАрТи, ИНК. Отделение легких газов от галогенов
MX2008009911A (es) 2006-02-03 2009-02-27 Grt Inc Proceso continuo para convertir gas natural a hidrocarburos liquidos.
KR20100027141A (ko) 2007-05-24 2010-03-10 지알티, 인코포레이티드 가역적으로 할로겐화수소를 흡수 및 방출할 수 있는 존 반응기
US8282810B2 (en) 2008-06-13 2012-10-09 Marathon Gtf Technology, Ltd. Bromine-based method and system for converting gaseous alkanes to liquid hydrocarbons using electrolysis for bromine recovery
NZ591207A (en) 2008-07-18 2013-03-28 Grt Inc Continuous process for converting natural gas to liquid hydrocarbons
CN101508632B (zh) * 2009-03-25 2012-06-13 东南大学 多相催化氧化制备3,3-二甲基丁醛的方法
CN102030667A (zh) * 2009-09-30 2011-04-27 昆明全新生物制药有限公司 一种4-(n,n-二烷胺基)丁醛缩二醇的制备方法
US8367884B2 (en) 2010-03-02 2013-02-05 Marathon Gtf Technology, Ltd. Processes and systems for the staged synthesis of alkyl bromides
US8198495B2 (en) 2010-03-02 2012-06-12 Marathon Gtf Technology, Ltd. Processes and systems for the staged synthesis of alkyl bromides
CN102241573B (zh) * 2010-05-10 2014-06-11 陕西天汉生物科技有限公司 一种3,3-二甲基丁醛的制备方法
CN101962327A (zh) * 2010-08-30 2011-02-02 海门慧聚药业有限公司 4-(n,n-二甲氨基)-丁醛缩二甲醇的合成新工艺
CN102030668B (zh) * 2010-10-24 2013-10-30 绍兴文理学院 二甲胺丁缩醛的制备方法
US8815050B2 (en) 2011-03-22 2014-08-26 Marathon Gtf Technology, Ltd. Processes and systems for drying liquid bromine
US8436220B2 (en) 2011-06-10 2013-05-07 Marathon Gtf Technology, Ltd. Processes and systems for demethanization of brominated hydrocarbons
US8829256B2 (en) 2011-06-30 2014-09-09 Gtc Technology Us, Llc Processes and systems for fractionation of brominated hydrocarbons in the conversion of natural gas to liquid hydrocarbons
US8802908B2 (en) 2011-10-21 2014-08-12 Marathon Gtf Technology, Ltd. Processes and systems for separate, parallel methane and higher alkanes' bromination
US9193641B2 (en) 2011-12-16 2015-11-24 Gtc Technology Us, Llc Processes and systems for conversion of alkyl bromides to higher molecular weight hydrocarbons in circulating catalyst reactor-regenerator systems
CN104119212B (zh) * 2013-04-27 2016-03-02 中国科学院大连化学物理研究所 一种催化氧化3,3-二甲基-1-丁醇制备3,3-二甲基-1-丁醛的方法
JP6155832B2 (ja) * 2013-05-16 2017-07-05 セイコーエプソン株式会社 センサー素子、電子機器、および移動体
CN104649874A (zh) * 2013-11-15 2015-05-27 中国科学院大连化学物理研究所 3,3-二甲基-1-丁醇脱氢制3,3-二甲基-1-丁醛的方法
BR112017009030B1 (pt) * 2014-10-30 2021-01-12 Organofuel Sweden Ab Métodos para conversão de uma ligação co ou c=o em uma ligação c-h

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ES8506627A1 (es) * 1983-08-11 1985-08-01 Monsanto Co Un procedimiento para preparar derivados de piridina sustituidos en las posiciones 2 y 6
NZ231962A (en) * 1988-12-23 1992-10-28 Squibb & Sons Inc 7-oxabicycloheptane derivatives as prostaglandin analogs; medicaments
JPH0832647B2 (ja) * 1989-01-27 1996-03-29 大阪有機化学工業株式会社 1級アルコールからアルデヒドの製造法
NZ232897A (en) * 1989-04-03 1992-12-23 Squibb & Sons Inc Interphenylene 7-oxabicycloheptyl substituted heterocyclic amide prostaglandin analogues, preparation and pharmaceutical compositions thereof
JP3039025B2 (ja) * 1991-07-19 2000-05-08 吉富製薬株式会社 置換アセトアルデヒドの製造方法
JPH05310632A (ja) * 1992-04-28 1993-11-22 Sumitomo Chem Co Ltd m−フェノキシベンズアルデヒドの製造方法
JP3626520B2 (ja) * 1994-12-26 2005-03-09 株式会社クラレ 3−置換−3−メチルブタナールの製造方法
US5631366A (en) * 1995-01-12 1997-05-20 Hoffmann-La Roche Inc. Process for making 3-formylcephem derivatives
JPH08198795A (ja) * 1995-01-20 1996-08-06 Kuraray Co Ltd セネシオンアルデヒドの製造方法
JPH08198893A (ja) * 1995-01-27 1996-08-06 Nippon Kayaku Co Ltd 14α−ヒドロキシ−4−アンドロステン−3,6,17−トリオンの製造法
US5821374A (en) * 1995-11-21 1998-10-13 Hoffmann-La Roche Inc. Process for the oxidation of alcohols
US5856584A (en) * 1997-08-06 1999-01-05 The Nutrasweet Company Preparation of 3,3-dimethylbutyraldehyde by oxidation of 3, 3-dimethylbutanol

Also Published As

Publication number Publication date
CN1238320C (zh) 2006-01-25
DE69819164D1 (de) 2003-11-27
EP1186591B1 (de) 2005-11-02
CA2486890C (en) 2009-03-31
JP2010031021A (ja) 2010-02-12
KR20060010871A (ko) 2006-02-02
AR016582A1 (es) 2001-07-25
KR100622438B1 (ko) 2006-09-19
CN1266419A (zh) 2000-09-13
CA2299637C (en) 2005-10-11
ATE252532T1 (de) 2003-11-15
CA2299637A1 (en) 1999-06-17
US5856584A (en) 1999-01-05
HUP0003631A3 (en) 2001-08-28
BR9811854B1 (pt) 2009-08-11
EP1003703B1 (de) 2003-10-22
HUP0003631A2 (hu) 2001-05-28
PE96699A1 (es) 1999-09-29
EP1186591A3 (de) 2002-03-20
ES2205563T3 (es) 2004-05-01
KR100585332B1 (ko) 2006-05-30
UY25126A1 (es) 1998-08-31
CN1286790C (zh) 2006-11-29
AU749936B2 (en) 2002-07-04
AU9773898A (en) 1999-06-28
DE69832209T2 (de) 2006-07-27
BR9811854A (pt) 2000-08-15
JP2012102113A (ja) 2012-05-31
EP1186591A2 (de) 2002-03-13
WO1999029646A1 (en) 1999-06-17
ES2246978T3 (es) 2006-03-01
CA2486890A1 (en) 1999-06-17
EP1003703A1 (de) 2000-05-31
JP2001525384A (ja) 2001-12-11
DE69819164T2 (de) 2004-07-22
CN1515533A (zh) 2004-07-28
KR20010022562A (ko) 2001-03-26
IL134374A0 (en) 2001-04-30

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