DE69203327D1 - Verfahren zur herstellung eines gereinigten derivates von einem acrylamidosulfonsäure-monomer. - Google Patents
Verfahren zur herstellung eines gereinigten derivates von einem acrylamidosulfonsäure-monomer.Info
- Publication number
- DE69203327D1 DE69203327D1 DE69203327T DE69203327T DE69203327D1 DE 69203327 D1 DE69203327 D1 DE 69203327D1 DE 69203327 T DE69203327 T DE 69203327T DE 69203327 T DE69203327 T DE 69203327T DE 69203327 D1 DE69203327 D1 DE 69203327D1
- Authority
- DE
- Germany
- Prior art keywords
- purified
- group
- nitrogens
- derivate
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000178 monomer Substances 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title 1
- MRXVCTWDXRBVLW-UHFFFAOYSA-N prop-2-enoylsulfamic acid Chemical compound OS(=O)(=O)NC(=O)C=C MRXVCTWDXRBVLW-UHFFFAOYSA-N 0.000 title 1
- 239000002184 metal Substances 0.000 abstract 3
- 229910052751 metal Inorganic materials 0.000 abstract 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 150000002739 metals Chemical class 0.000 abstract 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 abstract 2
- 150000003839 salts Chemical class 0.000 abstract 2
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000007086 side reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/42—Separation; Purification; Stabilisation; Use of additives
- C07C303/44—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Optical Couplings Of Light Guides (AREA)
- Peptides Or Proteins (AREA)
- Medicines Containing Antibodies Or Antigens For Use As Internal Diagnostic Agents (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US70974591A | 1991-06-03 | 1991-06-03 | |
| PCT/US1992/003754 WO1992021652A1 (en) | 1991-06-03 | 1992-05-06 | Process for the preparation of a purified acrylamido sulfonic acid monomer derivative |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69203327D1 true DE69203327D1 (de) | 1995-08-10 |
| DE69203327T2 DE69203327T2 (de) | 1995-11-02 |
Family
ID=24851163
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69203327T Expired - Fee Related DE69203327T2 (de) | 1991-06-03 | 1992-05-06 | Verfahren zur herstellung eines gereinigten derivates von einem acrylamidosulfonsäure-monomer. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US6331647B1 (de) |
| EP (1) | EP0541770B1 (de) |
| JP (1) | JPH05508869A (de) |
| AT (1) | ATE124682T1 (de) |
| AU (1) | AU1993692A (de) |
| CA (1) | CA2087715A1 (de) |
| DE (1) | DE69203327T2 (de) |
| ES (1) | ES2077421T3 (de) |
| FI (1) | FI930345L (de) |
| MX (1) | MX9202625A (de) |
| NO (1) | NO179323C (de) |
| WO (1) | WO1992021652A1 (de) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5912387A (en) * | 1997-01-28 | 1999-06-15 | The Dow Chemical Company | Amine heat stable salt neutralization having reduced solids |
| JP2004345994A (ja) * | 2003-05-21 | 2004-12-09 | Nippon Shokubai Co Ltd | Ｎ−ビニル−２−ピロリドンの精製方法 |
| WO2005080451A1 (en) * | 2004-02-19 | 2005-09-01 | The Lubrizol Corporation | Improviong the lipophilic properties of 2-acrylamido-2-methylpropanesulfonic acid |
| JP5304205B2 (ja) * | 2007-12-06 | 2013-10-02 | 東亞合成株式会社 | ２−アクリルアミド−２−メチルプロパンスルホン酸、及びその製造方法 |
| CN102452965B (zh) * | 2010-10-22 | 2013-08-14 | 中国石油化工股份有限公司 | 一种除去amps原料中阻聚剂的方法 |
| JP6231010B2 (ja) | 2011-11-29 | 2017-11-15 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | アクリルアミド−２−メチルプロパンスルホン酸（ａ）の塩を生成する方法、アクリルアミド−２−メチルプロパンスルホン酸（ａ）又はその塩、及びそれを用いた共重合体の製造方法 |
| US9073826B2 (en) | 2011-11-29 | 2015-07-07 | Basf Se | Process for preparing and purifying salts of acrylamido-2-methylpropanesulfonic acid |
| CN103086930A (zh) * | 2013-01-17 | 2013-05-08 | 潍坊泉鑫化工有限公司 | 从重结晶滤液中提取2-丙烯酰胺基-2-甲基丙磺酸的方法 |
| CN103086929B (zh) * | 2013-02-04 | 2014-11-05 | 梅龙毅 | 一种制备固体丙烯酰胺基烷基磺酸盐的方法 |
| CN103254102B (zh) * | 2013-06-06 | 2015-09-30 | 梅龙毅 | 一种纯化丙烯酰胺基烷基磺酸的方法 |
| FR3041344B1 (fr) * | 2015-09-18 | 2019-12-13 | S.P.C.M. Sa | Procede d'obtention du monomere acide 2-acrylamido-2-methylpropanesulphonique et polymere comprenant ledit monomere |
| WO2017162545A1 (de) | 2016-03-24 | 2017-09-28 | Basf Se | Verfahren zur herstellung von atbs und copolymeren daraus |
| FR3064004B1 (fr) * | 2017-03-20 | 2019-03-29 | S.P.C.M. Sa | Forme cristalline hydratee de l'acide 2-acrylamido-2-methylpropane sulfonique |
| CN110857280B (zh) * | 2018-08-22 | 2022-06-03 | 潍坊金石环保科技有限公司 | 一种2-丙烯酰胺基-2-甲基丙磺酸盐的制备方法 |
| CN112047863A (zh) * | 2020-09-19 | 2020-12-08 | 寿光市荣晟新材料有限公司 | 一种2-丙烯酰胺基-2-甲基丙磺酸钠盐制备工艺 |
| FR3146673A1 (fr) | 2023-03-13 | 2024-09-20 | Snf Sa | Procédé de traitement d’une suspension de particules solides dans l’eau utilisant un polymère d’une forme cristalline du sel de sodium de l’acide 2-acrylamido-2-methylpropane sulfonique |
| FR3146680A1 (fr) * | 2023-03-13 | 2024-09-20 | Snf Sa | Forme cristalline du sel de sodium de l’acide 2-acrylamido-2-methylpropane sulfonique |
| FR3146690A1 (fr) | 2023-03-13 | 2024-09-20 | Snf Sa | Fluide de fracturation comprenant un polymère d’une forme cristalline du sel de sodium de l’acide 2-acrylamido-2-methylpropane sulfonique et procédé de fracturation hydraulique |
| FR3146689A1 (fr) | 2023-03-13 | 2024-09-20 | Snf Sa | Procédé de récupération assistée d’hydrocarbures utilisant un polymère d’une forme cristalline du sel de sodium de l’acide 2-acrylamido-2-methylpropane sulfonique |
| FR3146679A1 (fr) | 2023-03-13 | 2024-09-20 | Snf Sa | Forme cristalline du sel de potassium de l’acide 2-acrylamido-2-methylpropane sulfonique |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2549840A1 (de) * | 1975-11-06 | 1977-05-12 | Lubrizol Corp | Aminsalze und quartaere ammoniumsalze von acrylamidoalkansulfonsaeuren und deren polymerisate |
| JPS54106427A (en) * | 1978-02-09 | 1979-08-21 | Nitto Chem Ind Co Ltd | Purification of 2-acrylamide-2-methylpropane sulfonic acid |
| US4650614A (en) * | 1980-02-21 | 1987-03-17 | Medtronic, Inc. | Refining of reaction grade 2-acrylamido-2-methylpropane sulfonic acid |
| JPS58225056A (ja) * | 1982-06-24 | 1983-12-27 | Mitsui Toatsu Chem Inc | アミドアルカンスルホン酸誘導体の製造方法 |
| DE3627455A1 (de) * | 1985-08-15 | 1987-02-19 | Chevron Res | Acrylamido- und methacrylamido-n-substituierte sulfonsaeuren |
-
1992
- 1992-05-06 CA CA002087715A patent/CA2087715A1/en not_active Abandoned
- 1992-05-06 ES ES92912157T patent/ES2077421T3/es not_active Expired - Lifetime
- 1992-05-06 WO PCT/US1992/003754 patent/WO1992021652A1/en active IP Right Grant
- 1992-05-06 JP JP93500413A patent/JPH05508869A/ja active Pending
- 1992-05-06 AU AU19936/92A patent/AU1993692A/en not_active Abandoned
- 1992-05-06 DE DE69203327T patent/DE69203327T2/de not_active Expired - Fee Related
- 1992-05-06 AT AT92912157T patent/ATE124682T1/de active
- 1992-05-06 EP EP92912157A patent/EP0541770B1/de not_active Expired - Lifetime
- 1992-06-02 MX MX9202625A patent/MX9202625A/es not_active IP Right Cessation
-
1993
- 1993-01-27 FI FI930345A patent/FI930345L/fi unknown
- 1993-02-02 NO NO930357A patent/NO179323C/no unknown
-
1994
- 1994-12-14 US US08/355,712 patent/US6331647B1/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| WO1992021652A1 (en) | 1992-12-10 |
| FI930345A0 (fi) | 1993-01-27 |
| ES2077421T3 (es) | 1995-11-16 |
| MX9202625A (es) | 1993-04-01 |
| DE69203327T2 (de) | 1995-11-02 |
| NO930357L (no) | 1993-02-02 |
| ATE124682T1 (de) | 1995-07-15 |
| NO179323B (no) | 1996-06-10 |
| JPH05508869A (ja) | 1993-12-09 |
| FI930345L (fi) | 1993-01-27 |
| NO930357D0 (no) | 1993-02-02 |
| US6331647B1 (en) | 2001-12-18 |
| NO179323C (no) | 1996-09-18 |
| CA2087715A1 (en) | 1992-12-04 |
| AU1993692A (en) | 1993-01-08 |
| EP0541770A1 (de) | 1993-05-19 |
| EP0541770B1 (de) | 1995-07-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |