DE69109153D1 - Herstellung von Isopropylidenbisphthalsäure und von Isopropylidenbisphthalsäureanhydrid. - Google Patents
Herstellung von Isopropylidenbisphthalsäure und von Isopropylidenbisphthalsäureanhydrid.Info
- Publication number
- DE69109153D1 DE69109153D1 DE69109153T DE69109153T DE69109153D1 DE 69109153 D1 DE69109153 D1 DE 69109153D1 DE 69109153 T DE69109153 T DE 69109153T DE 69109153 T DE69109153 T DE 69109153T DE 69109153 D1 DE69109153 D1 DE 69109153D1
- Authority
- DE
- Germany
- Prior art keywords
- isopropylidene
- acid
- bisphthalic
- isopropylidene bis
- dehydration
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- PAHZZOIHRHCHTH-UHFFFAOYSA-N 3-[2-(2,3-dicarboxyphenyl)propan-2-yl]phthalic acid Chemical compound C=1C=CC(C(O)=O)=C(C(O)=O)C=1C(C)(C)C1=CC=CC(C(O)=O)=C1C(O)=O PAHZZOIHRHCHTH-UHFFFAOYSA-N 0.000 title abstract 3
- 125000000654 isopropylidene group Chemical group C(C)(C)=* 0.000 title abstract 3
- 150000008064 anhydrides Chemical class 0.000 title 1
- 230000018044 dehydration Effects 0.000 abstract 3
- 238000006297 dehydration reaction Methods 0.000 abstract 3
- 230000003647 oxidation Effects 0.000 abstract 3
- 238000007254 oxidation reaction Methods 0.000 abstract 3
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 abstract 2
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 abstract 1
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 1
- 229910052794 bromium Inorganic materials 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 229910017052 cobalt Inorganic materials 0.000 abstract 1
- 239000010941 cobalt Substances 0.000 abstract 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 abstract 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 229910052726 zirconium Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
- C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Furan Compounds (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US48435490A | 1990-02-22 | 1990-02-22 | |
US07/484,346 US5028737A (en) | 1990-02-22 | 1990-02-22 | Preparation of isopropylidene bis(phthalic acid) |
Publications (1)
Publication Number | Publication Date |
---|---|
DE69109153D1 true DE69109153D1 (de) | 1995-06-01 |
Family
ID=27047966
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69109153T Expired - Lifetime DE69109153D1 (de) | 1990-02-22 | 1991-02-21 | Herstellung von Isopropylidenbisphthalsäure und von Isopropylidenbisphthalsäureanhydrid. |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP0443856B1 (de) |
JP (1) | JPH04219151A (de) |
AT (1) | ATE121720T1 (de) |
DE (1) | DE69109153D1 (de) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20100056750A1 (en) * | 2006-12-21 | 2010-03-04 | Ritter Joachim C | Process for the synthesis of halogenated aromatic diacids |
CN114276320A (zh) * | 2020-09-27 | 2022-04-05 | 中国石化扬子石油化工有限公司 | 一种偏苯三甲酸成酐的方法 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2712543A (en) * | 1954-06-11 | 1955-07-05 | Du Pont | Polyimide intermediates |
US3161693A (en) * | 1962-08-06 | 1964-12-15 | Standard Oil Co | Aromatic polycarboxylic acids |
-
1991
- 1991-02-21 AT AT91301397T patent/ATE121720T1/de not_active IP Right Cessation
- 1991-02-21 EP EP91301397A patent/EP0443856B1/de not_active Expired - Lifetime
- 1991-02-21 DE DE69109153T patent/DE69109153D1/de not_active Expired - Lifetime
- 1991-02-21 JP JP3078688A patent/JPH04219151A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
JPH04219151A (ja) | 1992-08-10 |
EP0443856A1 (de) | 1991-08-28 |
ATE121720T1 (de) | 1995-05-15 |
EP0443856B1 (de) | 1995-04-26 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8332 | No legal effect for de |