DE226241C - - Google Patents
Info
- Publication number
- DE226241C DE226241C DENDAT226241D DE226241DA DE226241C DE 226241 C DE226241 C DE 226241C DE NDAT226241 D DENDAT226241 D DE NDAT226241D DE 226241D A DE226241D A DE 226241DA DE 226241 C DE226241 C DE 226241C
- Authority
- DE
- Germany
- Prior art keywords
- dye
- och
- parts
- dichlorodianisidine
- purple
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 150000001875 compounds Chemical class 0.000 claims description 2
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 claims description 2
- 239000000975 dye Substances 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M Sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- JWAZRIHNYRIHIV-UHFFFAOYSA-N 2-Naphthol Chemical compound C1=CC=CC2=CC(O)=CC=C21 JWAZRIHNYRIHIV-UHFFFAOYSA-N 0.000 description 1
- OZFUEQNYOBIXTB-VJOYVCHSSA-N 2-[(2E,5E)-5-[[4-[4-(2,2-diphenylethenyl)phenyl]-2,3,3a,8b-tetrahydro-1H-cyclopenta[b]indol-7-yl]methylidene]-2-(3-ethyl-4-oxo-2-sulfanylidene-1,3-thiazolidin-5-ylidene)-4-oxo-1,3-thiazolidin-3-yl]acetic acid Chemical compound O=C1N(CC)C(=S)S\C1=C(\S\1)N(CC(O)=O)C(=O)C/1=C\C1=CC=C(N(C2C3CCC2)C=2C=CC(C=C(C=4C=CC=CC=4)C=4C=CC=CC=4)=CC=2)C3=C1 OZFUEQNYOBIXTB-VJOYVCHSSA-N 0.000 description 1
- DFMDAJMTLJGKFW-UHFFFAOYSA-N 3-Chloro-2-nitrophenol Chemical compound OC1=CC=CC(Cl)=C1[N+]([O-])=O DFMDAJMTLJGKFW-UHFFFAOYSA-N 0.000 description 1
- 241000947840 Alteromonadales Species 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 210000002268 Wool Anatomy 0.000 description 1
- 229950011260 betanaphthol Drugs 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- -1 disodium salt Chemical class 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000001047 purple dye Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B35/00—Disazo and polyazo dyes of the type A<-D->B prepared by diazotising and coupling
- C09B35/02—Disazo dyes
- C09B35/039—Disazo dyes characterised by the tetrazo component
- C09B35/08—Disazo dyes characterised by the tetrazo component the tetrazo component being a derivative of biphenyl
- C09B35/10—Disazo dyes characterised by the tetrazo component the tetrazo component being a derivative of biphenyl from two coupling components of the same type
- C09B35/14—Disazo dyes characterised by the tetrazo component the tetrazo component being a derivative of biphenyl from two coupling components of the same type from hydroxy compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
PATENTSCHRIFTPATENT LETTERING
- M 226241 KLASSE 22 a. GRUPPE- M 226241 CLASS 22 a. GROUP
Verfahren zur Darstellung eines violetten Disazofarbstoffes.Process for the preparation of a purple disazo dye.
Es wurde gefunden, daß die Tetrazoverbindung des Dichlordianisidins der FormelIt has been found that the tetrazo compound of dichlorodianisidine of the formula
OCH*OCH *
N H2-NH 2 -
OCH3 OCH 3
-NH2,-NH 2 ,
Cl ClCl Cl
ίο das aus Chlornitrophenolätherίο the one from chloronitrophenol ether
(O C H3: N O2: Cl = 1:2:4) (OCH 3 : NO 2 : Cl = 1: 2: 4)
leicht dargestellt werden kann, bei Kombination mit 2 Molekülen 2-Naphtol-3: 6-disulfosäure einen rötlich violetten Farbstoff liefert, der sowohl zum Färben von Wolle als auch zur Darstellung von Pigmentfarben dienen kann. Diese letzteren sind vorzüglich kalk-, wasser- und ölecht und wegen ihrer guten Lichtechtheit und reinen rötlich violetten Nuance von besonderem Werte.can be easily represented when combined with 2 molecules of 2-naphthol-3: 6-disulfonic acid provides a reddish purple dye that is used both for dyeing wool and can serve to represent pigment colors. These latter are especially calcareous, water and oil and because of their good lightfastness and pure reddish purple Nuance of particular value.
Die Darstellung' des Farbstoffes kann wie folgt ausgeführt werden.The representation of the dye can be carried out as follows.
15,6 Teile Dichlordianisidin werden mit 6,9 Teilen Natriumnitrit und der nötigen Menge Salzsäure diazotiert und die, wenn nötig, filtrierte Lösung in eine bis zum Schluß der Kombination sodaalkalisch gehaltene und mit Eis gekühlte Lösung von 36 Teilen 2 - Naphtol -3:6- disulfosäure (Dinatriumsalz) einfließen gelassen. Nach Vollendung der Farbstoffbildung wird auf 700 angewärmt und der Farbstoff mit Salz gefallt, abfiltriert und getrocknet. Seine Überführung in Pigmentfarben kann nach den üblichen Methoden erfolgen. 15.6 parts of dichlorodianisidine are diazotized with 6.9 parts of sodium nitrite and the necessary amount of hydrochloric acid and, if necessary, the filtered solution is poured into a solution of 36 parts of 2-naphthol -3: 6 that is kept alkaline with soda until the end of the combination and is cooled with ice - Disulfonic acid (disodium salt) allowed to flow in. After completion of the dye formation is heated to 70 0 and the dye precipitated with salt, filtered and dried. It can be converted into pigment colors by the usual methods.
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE226241C true DE226241C (en) |
Family
ID=486805
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT226241D Active DE226241C (en) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE226241C (en) |
-
0
- DE DENDAT226241D patent/DE226241C/de active Active
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