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DE10245262A1 - Detergent-portioned tablet portions II - Google Patents

Detergent-portioned tablet portions II Download PDF

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Publication number
DE10245262A1
DE10245262A1 DE2002145262 DE10245262A DE10245262A1 DE 10245262 A1 DE10245262 A1 DE 10245262A1 DE 2002145262 DE2002145262 DE 2002145262 DE 10245262 A DE10245262 A DE 10245262A DE 10245262 A1 DE10245262 A1 DE 10245262A1
Authority
DE
Germany
Prior art keywords
water
soluble
film
cleaning agent
temperatures
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
DE2002145262
Other languages
German (de)
Inventor
Alexander Lambotte
Matthias Reimann
Wolfgang Dr. Barthel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Priority to DE2002145262 priority Critical patent/DE10245262A1/en
Priority to DE2002123266 priority patent/DE10223266C1/en
Priority to PCT/EP2003/005082 priority patent/WO2003099985A2/en
Priority to AU2003240647A priority patent/AU2003240647A1/en
Publication of DE10245262A1 publication Critical patent/DE10245262A1/en
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/04—Detergent materials or soaps characterised by their shape or physical properties combined with or containing other objects
    • C11D17/041—Compositions releasably affixed on a substrate or incorporated into a dispensing means
    • C11D17/042—Water soluble or water disintegrable containers or substrates containing cleaning compositions or additives for cleaning compositions
    • C11D17/044—Solid compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B11/00—Wrapping, e.g. partially or wholly enclosing, articles or quantities of material, in strips, sheets or blanks, of flexible material
    • B65B11/50—Enclosing articles, or quantities of material, by disposing contents between two sheets, e.g. pocketed sheets, and securing their opposed free margins
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B9/00—Enclosing successive articles, or quantities of material, e.g. liquids or semiliquids, in flat, folded, or tubular webs of flexible sheet material; Subdividing filled flexible tubes to form packages
    • B65B9/02—Enclosing successive articles, or quantities of material between opposed webs
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C11D17/0082—Coated tablets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
    • B65B9/00—Enclosing successive articles, or quantities of material, e.g. liquids or semiliquids, in flat, folded, or tubular webs of flexible sheet material; Subdividing filled flexible tubes to form packages
    • B65B9/02—Enclosing successive articles, or quantities of material between opposed webs
    • B65B9/04—Enclosing successive articles, or quantities of material between opposed webs one or both webs being formed with pockets for the reception of the articles, or of the quantities of material
    • B65B9/045—Enclosing successive articles, or quantities of material between opposed webs one or both webs being formed with pockets for the reception of the articles, or of the quantities of material for single articles, e.g. tablets

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Molecular Biology (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)
  • Medicinal Preparation (AREA)
  • Medical Preparation Storing Or Oral Administration Devices (AREA)

Abstract

Ein Verfahren zur Herstellung mit wasserlöslichen Umhüllungen eng umhüllter Wasch- oder Reinigungsmitteltabletten, das im Auflegen einer wasserlöslichen Folie auf ein Form(en)werkzeug; Einlegen von Wasch- oder Reinigungsmitteltablette(n) in die Form(en); Auflegen einer weiteren wasserlöslichen Folie auf die Wasch- oder Reinigungsmitteltablette(n) in der/den Form(en); Versiegeln und optionales Schneiden der Folien besteht, läßt sich vorteilhaft durchführen, wenn die wasserlösliche Folie vor dem Auflegen auf ein Form(en)werkzeug auf Temperaturen oberhalb von 50 DEG C erwärmt wird und/oder das Einlegen der Tablette(n) durch Anwärmen der Folie auf Temperaturen von 100 DEG C bis 120 DEG C unterstützt wird und/oder die Versiegelung der Folie bei Temperaturen von 140 DEG C bis 180 DEG C durchgeführt wird.A process for the production with water-soluble wrappings of tightly wrapped detergent or cleaning agent tablets, which involves placing a water-soluble film on a mold (s); Inserting detergent or cleaning agent tablet (s) into the mold (s); Placing another water-soluble film on the washing or cleaning agent tablet (s) in the form (s); Sealing and optional cutting of the foils can be carried out advantageously if the water-soluble foil is heated to temperatures above 50 ° C. before being placed on a mold (s) and / or the tablet (s) are inserted by heating the foil at temperatures of 100 ° C. to 120 ° C. and / or the sealing of the film is carried out at temperatures from 140 ° C. to 180 ° C.

Description

Die vorliegende Anmeldung ist eine Zusatzanmeldung zur deutschen Patentanmeldung DE 102 23 266 .0 (Anmeldetag: 24.05.2002). Die Stammanmeldung betrifft Wasch- oder Reinigungsmitteltablette aus verpreßtem teilchenförmigen Wasch- oder Reinigungsmittel, umfassend eine wasserlösliche Umhüllung, welche in engem Kontakt an der Wasch- oder Reinigungsmitteltablette anliegt; wobei die Tablette mindestens ein quellfähiges Desintegrationshilfsmittel enthält. Daneben betrifft die Stammanmeldung auch ein Verfahren zur Herstellung mit wasserlöslichen Umhüllungen eng umhüllter Wasch- oder Reinigungsmitteltabletten,das durch die SchritteThe present application is an additional application to the German patent application DE 102 23 266 .0 (filing date: May 24, 2002). The parent application relates to washing or cleaning agent tablets made of compressed particulate washing or cleaning agent, comprising a water-soluble coating which is in close contact with the washing or cleaning agent tablet; wherein the tablet contains at least one swellable disintegration aid. In addition, the parent application also relates to a process for the production with water-soluble wrappings of tightly wrapped detergent or cleaning agent tablets, which is carried out by the steps

  • a) Auflegen einer wasserlöslichen Folie auf ein Form(en)werkzeug;a) placing a water-soluble film on a mold (s);
  • b) Einlegen von Wasch- oder Reinigungsmitteltablette(n) in die Form(en);b) inserting detergent or cleaning agent tablet (s) into the To form);
  • c) Auflegen einer weiteren wasserlöslichen Folie auf die Wasch- oder Reinigungsmitteltablette(n) in der/den Form(en);c) placing another water-soluble film on the washing machine or detergent tablet (s) in the form (s);
  • d) Versiegeln und optionales Schneiden der Folien gekennzeichnet ist.d) sealing and optional cutting of the foils marked is.

Diese Zusatzanmeldung betrifft bevorzugte Ausgestaltungen des erfindungsgemäßen Verfahrens der Stammanmeldung. Das Verfahren zur Herstellung mit wasserlöslichen Umhüllungen eng umhüllter Wasch- oder Reinigungsmitteltabletten ist in der Stammanmeldung ausführlich beschrieben, so daß hier auf die Ausführungen in der Stammanmeldung verwiesen werden kann. Die Angaben zu Inhaltsstoffen, Folienmaterialien und weiteren Verfahrensparametern sind ebenfalls der Stammanmeldung zu entnehmen.This additional application relates to preferred configurations of the method according to the invention the parent registration. The process of making with water soluble wrappings tightly wrapped Detergent or cleaning agent tablets are in the parent registration in detail described, so here on the executions can be referenced in the parent application. The information on ingredients, Foil materials and other process parameters are also can be found in the parent registration.

Gegenstand der vorliegenden Zusatzanmeldung ist ein Verfahren zur Herstellung mit wasserlöslichen Umhüllungen eng umhüllter Wasch- oder Reinigungsmitteltabletten nach der Lehre der DE 102 23 266.0 , das dadurch gekennzeichnet ist, daß eine wasserlöslichen Folie vor dem Auflegen auf ein Form(en)werkzeug auf Temperaturen oberhalb von 50°C, vorzugsweise oberhalb von 70°C und insbesondere oberhalb von 90°C , erwärmt wird.The subject of the present additional application is a process for the production with water-soluble coatings of tightly coated detergent tablets according to the teaching of DE 102 23 266.0 , which is characterized in that a water-soluble film is heated to temperatures above 50 ° C, preferably above 70 ° C and in particular above 90 ° C, before being placed on a mold (s).

Durch das Erwärmen der Folie vor dem Verformungsvorgang wird das Verfahren der Stammanmeldung erleichtert und das Verfahrensergebnis verbessert. Alternativ zur Erwärmung vor dem Auflegen auf das Form(en)werkzeug oder in Ergänzung dazu kann die Folie während des Umformvorgangs erwärmt werden. Ein weiterer Gegenstand der vorliegenden Zusatzanmeldung ist daher ein Verfahren zur Herstellung mit wasserlöslichen Umhüllungen eng umhüllter Wasch- oder Reinigungsmitteltabletten nach der Lehre der DE 102 23 266.0 , das dadurch gekennzeichnet ist, daß die Verformung der wasserlöslichen Folie durch das Einlegen der Tablette(n) in Schritt b) durch Anwärmen der Folie auf Temperaturen von 100 bis 120°C unterstützt wird.By heating the film before the shaping process, the process of registering the parent is made easier and the process result is improved. As an alternative to heating, or in addition to being placed on the mold (s), the film can be heated during the forming process. Another subject of the present additional application is therefore a process for the production with water-soluble coatings of tightly coated washing or cleaning agent tablets according to the teaching of DE 102 23 266.0 , which is characterized in that the deformation of the water-soluble film is supported by inserting the tablet (s) in step b) by heating the film to temperatures of 100 to 120 ° C.

Eine Kombination der beiden Verfahrensvarianten ist möglich und bevorzugt.A combination of the two process variants is possible and preferred.

Die Versiegelung, die in Schritt d) des Verfahrens der Stammanmeldung erfolgt, wird vorzugsweise bei höheren Temperaturen durchgeführt. Hier sind erfindungsgemäßen Verfahren bevorzugt, die bei Temperaturen oberhalb von 100°C aber unterhalb von 200°C arbeiten. Ein weiterer Gegenstand der vorliegenden Zusatzanmeldung ist daher ein Verfahren zur Herstellung mit wasserlöslichen Umhüllungen eng umhüllter Wasch- oder Reinigungsmitteltabletten nach der Lehre der DE 102 23 266.0 , bei dem die Versiegelung der Folie in Schritt d) bei Temperaturen von 140°C bis 180°C, vorzugsweise von 150°C bis 170°C und insbesondere bei Temperaturen von 155°C bis 165°C, durchgeführt wird.The sealing, which takes place in step d) of the parent registration process, is preferably carried out at higher temperatures. Processes according to the invention which operate at temperatures above 100 ° C. but below 200 ° C. are preferred here. Another subject of the present additional application is therefore a process for the production with water-soluble coatings of tightly coated washing or cleaning agent tablets according to the teaching of DE 102 23 266.0 , in which the sealing of the film in step d) is carried out at temperatures from 140 ° C. to 180 ° C., preferably from 150 ° C. to 170 ° C. and in particular at temperatures from 155 ° C. to 165 ° C.

In Ergänzung zur Lehre der Stammanmeldung hat sich als vorteilhaft herausgestellt, wenn die im Form(en)werkzeug zu verformende Folie und die Folie, mit der versiegelt wird, unterschiedliche Materialstärken aufweisen. In Ergänzung zu Anspruch 13 der Stammanmeldung liegt ein weiterer Aspekt der vorliegenden Zusatzanmeldung in einem Verfahren, bei dem die wasserlösliche Folie, die im Form(en)werkzeug geformt wird, eine Dicke von 30 bis 80 μm, vorzugsweise von 35 bis 70 μm und insbesondere von 40 bis 60 μm, aufweist.In addition to the teaching of the parent application has proven to be advantageous if the tool (s) in the mold The film to be deformed and the film used to seal it are different thicknesses exhibit. In addition to claim 13 of the parent application is another aspect of the present Additional registration in a procedure in which the water-soluble film, which is molded in the mold (s), a thickness of 30 to 80 microns, preferably from 35 to 70 μm and in particular from 40 to 60 μm, having.

Die Stärke der Siegelfolie ist vorzugsweise geringer. Hier sind Verfahren bevorzugt, bei denen die wasserlösliche Folie, die in Schritt c) aufgelegt wird, eine Dicke von 20 bis 60 μm, vorzugsweise von 25 bis 50 μm und insbesondere von 30 bis 45 μm, aufweist.The thickness of the sealing film is preferably less. Processes in which the water-soluble film, which is placed in step c), a thickness of 20 to 60 microns, preferably from 25 to 50 μm and in particular from 30 to 45 μm.

Anstelle einer einlagigen Folie können erfindungsgemäß auch mehrlagige Folienlaminate eingesetzt werden. Solche Laminate besitzen den Vorteil, daß die einzelnen Lagen den jeweiligen Umgebungsbedingungen angepaßt werden können. So kann zum Beispiel eine Innenfolie genutzt werden, welche gegenüber der einzufüllenden Zusammensetzung inert ist und keine unerwünschten Reaktionen mit der Füllung eingeht. Eine Außenfolie, welche den Umgebungseinflüssen besser widersteht, kann in einem solchen Zweifolienlaminat die Zusammensetzung vor äußeren Einflüssen schützen. Erfindungsgemäß einsetzbar sind selbstverständlich auch Dreifolienlaminate, Vierfolienlaminate usw. wobei den einzelnen Folien unterschiedliche Funktionen (mechanische Stabilisierung, Dampfsperre, Optik, Funktionalität durch Inkorporation von Inhaltsstoffen usw.) zugeordnet werden können.Instead of a single-layer film, multilayer films can also be used according to the invention Foil laminates are used. Such laminates have the advantage that the individual Layers can be adapted to the respective environmental conditions. For example an inner film can be used, which is compared to the one to be filled The composition is inert and there are no undesirable reactions with the filling. An outer film, which the environmental influences The composition can withstand better in such a two-layer laminate protect against external influences. Can be used according to the invention are a matter of course also three-film laminates, four-film laminates, etc. where the individual films different functions (mechanical stabilization, vapor barrier, Optics, functionality through Incorporation of ingredients, etc.) can be assigned.

Weitere Angaben zu Folienmaterialien, Tabletteninhaltsstoffen und Verfahrensparametern sind der Stammanmeldung zu entnehmen.Further information on foil materials, Tablet ingredients and process parameters are the parent application refer to.

Claims (5)

Verfahren zur Herstellung mit wasserlöslichen Umhüllungen eng umhüllter Wasch- oder Reinigungsmitteltabletten nach der Lehre der DE 102 23 266.0 , dadurch gekennzeichnet, daß eine wasserlöslichen Folie vor dem Auflegen auf ein Form(en)werkzeug auf Temperaturen oberhalb von 50°C, vorzugsweise oberhalb von 70°C und insbesondere oberhalb von 90°C , erwärmt wird.Process for the production with water-soluble coatings of tightly coated detergent or cleaning agent tablets according to the teaching of DE 102 23 266.0 , characterized in that a water-soluble film is heated to temperatures above 50 ° C, preferably above 70 ° C and in particular above 90 ° C, before being placed on a mold (s). Verfahren zur Herstellung mit wasserlöslichen Umhüllungen eng umhüllter Wasch- oder Reinigungsmitteltabletten nach der Lehre der DE 102 23 266.0 , dadurch gekennzeichnet, daß die Verformung der wasserlöslichen Folie durch das Einlegen der Tablette(n) in Schritt b) durch Anwärmen der Folie auf Temperaturen von 100 bis 120°C unterstützt wird.Process for the production with water-soluble coatings of tightly coated detergent or cleaning agent tablets according to the teaching of DE 102 23 266.0 , characterized in that the deformation of the water-soluble film is supported by inserting the tablet (s) in step b) by heating the film to temperatures of 100 to 120 ° C. Verfahren zur Herstellung mit wasserlöslichen Umhüllungen eng umhüllter Wasch- oder Reinigungsmitteltabletten nach der Lehre der DE 102 23 266.0 , dadurch gekennzeichnet, daß die Versiegelung der Folie in Schritt d) bei Temperaturen von 140°C bis 180°C, vorzugsweise von 150°C bis 170°C und insbesondere bei Temperaturen von 155°C bis 165°C, durchgeführt wird.Process for the production with water-soluble coatings of tightly coated detergent or cleaning agent tablets according to the teaching of DE 102 23 266.0 , characterized in that the sealing of the film in step d) is carried out at temperatures from 140 ° C to 180 ° C, preferably from 150 ° C to 170 ° C and in particular at temperatures from 155 ° C to 165 ° C. Verfahren nach einem der Ansprüche 1 bis 3, dadurch gekennzeichnet, daß die wasserlösliche Folie, die im Form(en)werkzeug geformt wird, eine Dicke von 30 bis 80 μm, vorzugsweise von 35 bis 70 μm und insbesondere von 40 bis 60 μm, aufweist.Method according to one of claims 1 to 3, characterized in that that the water-soluble Foil that is formed in the mold (s) tool, a thickness of 30 to 80 μm, preferably from 35 to 70 μm and in particular from 40 to 60 μm, having. Verfahren nach einem der Ansprüche 1 bis 4, dadurch gekennzeichnet, daß die wasserlösliche Folie, die in Schritt c) aufgelegt wird, eine Dicke von 20 bis 60 μm, vorzugsweise von 25 bis 50 μm und insbesondere von 30 bis 45 μm, aufweist.Method according to one of claims 1 to 4, characterized in that that the water-soluble Film, which is placed in step c), a thickness of 20 to 60 microns, preferably from 25 to 50 μm and in particular from 30 to 45 μm, having.
DE2002145262 2002-05-24 2002-05-24 Detergent-portioned tablet portions II Ceased DE10245262A1 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
DE2002145262 DE10245262A1 (en) 2002-05-24 2002-05-24 Detergent-portioned tablet portions II
DE2002123266 DE10223266C1 (en) 2002-05-24 2002-05-24 Tablets with close-fitting water-soluble sheath, used in domestic washing machine and automatic dishwasher, especially in rinse-in compartment, contain swellable disintegration agent
PCT/EP2003/005082 WO2003099985A2 (en) 2002-05-24 2003-05-15 Tablet portions which can be dosed in a rinsing chamber
AU2003240647A AU2003240647A1 (en) 2002-05-24 2003-05-15 Tablet portions which can be dosed in a rinsing chamber

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE2002145262 DE10245262A1 (en) 2002-05-24 2002-05-24 Detergent-portioned tablet portions II
DE2002123266 DE10223266C1 (en) 2002-05-24 2002-05-24 Tablets with close-fitting water-soluble sheath, used in domestic washing machine and automatic dishwasher, especially in rinse-in compartment, contain swellable disintegration agent

Publications (1)

Publication Number Publication Date
DE10245262A1 true DE10245262A1 (en) 2004-04-08

Family

ID=29585305

Family Applications (2)

Application Number Title Priority Date Filing Date
DE2002145262 Ceased DE10245262A1 (en) 2002-05-24 2002-05-24 Detergent-portioned tablet portions II
DE2002123266 Expired - Fee Related DE10223266C1 (en) 2002-05-24 2002-05-24 Tablets with close-fitting water-soluble sheath, used in domestic washing machine and automatic dishwasher, especially in rinse-in compartment, contain swellable disintegration agent

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE2002123266 Expired - Fee Related DE10223266C1 (en) 2002-05-24 2002-05-24 Tablets with close-fitting water-soluble sheath, used in domestic washing machine and automatic dishwasher, especially in rinse-in compartment, contain swellable disintegration agent

Country Status (3)

Country Link
AU (1) AU2003240647A1 (en)
DE (2) DE10245262A1 (en)
WO (1) WO2003099985A2 (en)

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