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CS252373B1 - Use of static mixer for fflowing high-viscous mediums' viscosity continuous scanning - Google Patents

Use of static mixer for fflowing high-viscous mediums' viscosity continuous scanning Download PDF

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CS252373B1
CS252373B1 CS851110A CS111085A CS252373B1 CS 252373 B1 CS252373 B1 CS 252373B1 CS 851110 A CS851110 A CS 851110A CS 111085 A CS111085 A CS 111085A CS 252373 B1 CS252373 B1 CS 252373B1
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Czechoslovakia
Prior art keywords
viscosity
static mixer
fflowing
sensing
continuous scanning
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CS851110A
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Czech (cs)
Slovak (sk)
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CS111085A1 (en
Inventor
Mikulas Matisin
Pavol Havlik
Ondrej Andrascik
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Mikulas Matisin
Pavol Havlik
Ondrej Andrascik
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Application filed by Mikulas Matisin, Pavol Havlik, Ondrej Andrascik filed Critical Mikulas Matisin
Priority to CS851110A priority Critical patent/CS252373B1/en
Publication of CS111085A1 publication Critical patent/CS111085A1/en
Publication of CS252373B1 publication Critical patent/CS252373B1/en

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  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

Přesné kontinuálně snímanie viskozity spracovávaných tavenín syntetických polymérov, najma vo výrobě vlákien, sia zabezpečí použitím statického zmiešavača zabudovaného' db* 1 2potrubia. Statického zmiešavača sa tak využívá nielen akiO' prostriedku pre kontinuálnu homogenizáciu ale aj pre snímanie viskozity pretekajúceho vysokoviskózneho média vyhodnocováním tlakového spádu.Accurate continuous viscosity sensing processed polymers of synthetic polymers, especially in the production of fibers, it ensures using a static built-in mixer db * 1 2pipe. Static mixer thus utilizing not only the means for continuous homogenization as well as for sensing viscosity flowing high viscosity media by pressure compression drop.

Description

(54) Použitie sl&tického zmiešavača pre kontinuálně snímanie viskozity pretekajúcicli vysokoviskóznych médií(54) Use of a slurry mixer for continuously sensing viscosities flowing through high viscosity media

22

Přesné kontinuálně snímanie viskozity spracovávaných tavenín syntetických polymérov, najma vo výrobě vlákien, sia zabezpečí použitím statického zmiešavača zabudovaného' db* 1 2 potrubia. Statického zmiešavača sa tak využívá nielen akiO' prostriedku pre kontinuálnu homogenizáciu ale aj pre snímanie viskozity pretekajúceho vysokoviskózneho média vyhodnocováním tlakového spádu.Precision continuously sensing the viscosity of the melt processing synthetic polymers, especially in the production of fibers, sia ensure the use of built-in static mixer '* 1 2 db pipe. Thus, the static mixer is used not only as a means for continuous homogenization but also for sensing the viscosity of the flowing high viscosity medium by evaluating the pressure drop.

52 3 7 351 3 7 3

Predmetom vynálezu je použitie statického- zmiešavača pre snímanie viskozity vysokoviskóznych kvapalín ako sú taveniny polymérov.It is an object of the invention to use a static mixer for sensing the viscosity of highly viscous liquids such as polymer melts.

Doteraz neboli uspokojiv-o vyriešené spósoby a zariadenia na kontinuálně snímanie viskozity vysokoviskóznych kvapalín, ako sú například taveniny polymérov o teplotách 150 až 500 °C, najmá vo výrobných podmienkach.To date, methods and devices for continuously sensing the viscosity of highly viscous liquids, such as melt polymers at temperatures of 150 to 500 ° C, have not been satisfactorily solved, in particular under production conditions.

Pre tieto- účely sa dosial používali kapilárně viskozimetre u ktorých sa snímal tlakový rozdiel pred a za kapilárou umiestnené na obtoku produkčného potruhia, ako to uvádza ČS AO 188 489. Nevýhodou takéhoto merania je, že za krátku dobu sa zúžil príetokový profil kapiláry a tým změnil aj tlakový spád a tak sa v skutečnosti n-amerali chybné hodnoty.For this purpose, capillary viscometers have been used which have sensed the pressure difference before and after the capillary located on the bypass of the production line, as reported by CS AO 188 489. The disadvantage of such a measurement is that in a short time the flow profile of the capillary has narrowed and pressure drop and so in fact n-amerali wrong values.

Ďalšiu možnost poskytovali rotačně viskozimetre, v ktorých s-a meralo- zaťaženie pohonu rotujúceho meracieho- elementa, ktoré je úměrné viskozitě mer-aného média. Ich nevýhodou je, že sa nehodlá pre vysoké tlaky a teploty z dóvodu utesnenia a tiež pre usadzóvanie média ina rotačných elementech.Another possibility was provided by rotary viscometers in which the load of the rotating measuring element drive was proportional to the viscosity of the measured medium. Their disadvantage is that it is not suitable for high pressures and temperatures due to sealing and also for the settling of the medium on other rotating elements.

Uvedené nedostatky rieši použitie statického zmiešavača ako prostriedku pre kontinuálně snímanie viskozity pretekajúcehO vysokoviskózneho média, pri ktorom meraní najmá vo výrobných podmienkach nedochádza k změnám t-okOvých podmienok taveniny polyméru statickým zmiešavačom a v dósledku toho- ku změnám tlakového spádu média pred a za statickým zmiešavačom.The aforementioned drawbacks are solved by the use of a static mixer as a means for continuously sensing the viscosity of a flowing high viscosity medium, in which the measurement at least under production conditions does not change the t-eye conditions of the polymer melt by the static mixer.

Pri využití statických zmiešavačov, najmá překážkových sme zistili, že počas dlhodobého používania týchto, nedochádza k tvorbě usadenín na jeho, povrchu tak, aby došlo k změnám tokových vlastností v takom rozsahu, aby meranie v prevádzko-vých podmienkach nebolo, reprodukovatelné. Naviac príetokový profil statického zmiešavača je mnohonásobné váčší, než ako to bývá u kapilárnych viskozimetrov, ktoré je nutné riešit do- obtoku produkčného, potrubia, ako je tomu v ČS AO 188 489, kde preteká len časť média vzhladom na malý prierez kapiláry. Z tohto dóvodu dochádza k znehodnoteniu merania. Cez statický zmiešavač výhodné prechádza celé spracované množstvo média, u ktorého ježiadúc-a najváčšia homogenita a tým aj jeho statické zmiešavanie — htomogenizácia.Using static mixers, especially obstacle mixers, we have found that during long-term use of these, deposits do not form on its surface so that the flow properties change to such an extent that measurement under operational conditions is not reproducible. In addition, the flow profile of the static mixer is many times greater than that of capillary viscometers, which need to be solved in the bypass of the production line, as in CS AO 188 489, where only a portion of the medium flows due to the small cross-section of the capillary. For this reason, the measurement is impaired. Advantageously, the entire treated quantity of the medium passes through the static mixer, with the desired homogeneity and hence its static mixing - htomogenization.

Velkým problémom najmá u vysokých tlakov okolto 20 MPa a teplót do 350 °C meraného- média je utesnenie a uloženie hriadele rotačného snímača tak, aby toto ne-ovplyvňovato odpor meraného média voči jeho, rotačnému prvku. U rotačných, ako aj u kapilárnych snímačov viskozity pre funkciu je potřebná přídavná energie. U navrhovaného použitia přídavná energia nie je potřebná.A major problem, especially at high pressures of about 20 MPa and temperatures up to 350 ° C of the measured medium, is the sealing and bearing of the rotary encoder shaft so that this does not affect the resistance of the measured medium to its rotating element. For rotary as well as capillary viscosity sensors for the function, additional energy is required. For the proposed use, additional energy is not needed.

Príkladom je použitie statického zmiešavača, pozostávajúceho z rúry, v ktorej sú zabudované přepážky róznych tvaro-v, ktoré zabezpečujú premiešanie pretekajúceho média. Snímáním tlakového, spádu na statickom zmiešavači sa dá kontinuálně vyhodnocovat viskozita pretekajúceho média.An example is the use of a static mixer consisting of an oven in which various baffles of various shapes are incorporated to ensure that the flowing medium is mixed. By sensing the pressure drop on the static mixer, the viscosity of the flowing medium can be continuously evaluated.

PO-užitím statického zmiešavača ako prostriedku pre kontinuláne snímanie viskozity pretekajúceho vysokoviskózneho média podl-a tohto- vynálezu jednoduchým a spolehlivým spósobom rieši problém snímania zmien viskozity v procese spracovania termoplastických polymérov, pri ktorom viskozita taveniny je dóležitým technologickým parametrom. Pri autom-atizácii procesov spracovania termoplastických polymérov plastikářským, ale najmá vláknaremským potstupo-m je dóležité získat' spofahlivé údaje o viskozitě taveniny pre počítačové vstupy a -na základe nich upravovat celý technologický postup.By using a static mixer as a means for continuously measuring the viscosity of the flowing high viscosity medium according to the invention, it solves in a simple and reliable manner the problem of sensing viscosity changes in the process of processing thermoplastic polymers where melt viscosity is an important technological parameter. In automating the processing of thermoplastic polymers by plastic, but especially fiber, processes, it is important to obtain reliable melt viscosity data for computer inputs and adjust the entire process accordingly.

Claims (1)

PREDMETSUBJECT Použitie statického zmiešavača zabudovaného do potruhia ako prostriedku pre kontinuálně snímanie viskozity vysotooviskózVYNÁLEZU něho média pri vyhodnocovaní tlakového spádu.The use of a static mixer incorporated into the trunk as a means for continuously sensing the viscosity of the high viscosity medium of the invention in the evaluation of the pressure drop.
CS851110A 1985-02-18 1985-02-18 Use of static mixer for fflowing high-viscous mediums' viscosity continuous scanning CS252373B1 (en)

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CS252373B1 true CS252373B1 (en) 1987-08-13

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