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CS207645B2 - Method of making the mononitrobenzene - Google Patents

Method of making the mononitrobenzene Download PDF

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Publication number
CS207645B2
CS207645B2 CS785136A CS513678A CS207645B2 CS 207645 B2 CS207645 B2 CS 207645B2 CS 785136 A CS785136 A CS 785136A CS 513678 A CS513678 A CS 513678A CS 207645 B2 CS207645 B2 CS 207645B2
Authority
CS
Czechoslovakia
Prior art keywords
reaction
nitric acid
mononitrobenzene
nitration
benzene
Prior art date
Application number
CS785136A
Other languages
Czech (cs)
English (en)
Inventor
Verner Alexanderson
James B Trecek
Cornelius M Vanderwaart
Original Assignee
American Cyanamid Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by American Cyanamid Co filed Critical American Cyanamid Co
Publication of CS207645B2 publication Critical patent/CS207645B2/cs

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • C07C201/08Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CS785136A 1977-08-19 1978-08-04 Method of making the mononitrobenzene CS207645B2 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/826,208 US4091042A (en) 1977-08-19 1977-08-19 Continuous adiabatic process for the mononitration of benzene

Publications (1)

Publication Number Publication Date
CS207645B2 true CS207645B2 (en) 1981-08-31

Family

ID=25245976

Family Applications (1)

Application Number Title Priority Date Filing Date
CS785136A CS207645B2 (en) 1977-08-19 1978-08-04 Method of making the mononitrobenzene

Country Status (21)

Country Link
US (1) US4091042A (nl)
JP (1) JPS5432424A (nl)
AT (1) AT357140B (nl)
AU (1) AU518647B2 (nl)
BE (1) BE867355A (nl)
BR (1) BR7803249A (nl)
CA (1) CA1083608A (nl)
CH (1) CH639936A5 (nl)
CS (1) CS207645B2 (nl)
DD (1) DD136960A5 (nl)
DE (1) DE2821571A1 (nl)
EG (1) EG13569A (nl)
FR (1) FR2400501A1 (nl)
GB (1) GB1597433A (nl)
IN (1) IN147796B (nl)
IT (1) IT1103488B (nl)
MX (1) MX148692A (nl)
NL (1) NL189757C (nl)
PL (1) PL113312B1 (nl)
PT (1) PT68105A (nl)
TR (1) TR19875A (nl)

Families Citing this family (72)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4241229A (en) * 1979-08-08 1980-12-23 American Cyanamid Company Recovery of nitrated aromatic compounds from nitration wash liquors
JPS5785332A (en) * 1980-11-17 1982-05-28 Mitsui Toatsu Chem Inc Ortho-alkylation of phenolic compound
DE3409719A1 (de) * 1984-03-16 1985-09-19 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von dinitrotoluol
DE3409717C2 (de) * 1984-03-16 1994-03-31 Bayer Ag Verfahren zur Herstellung von Nitrobenzol
US4973770A (en) * 1988-12-15 1990-11-27 C-I-L, Inc. Manufacture of organic nitro compounds
US5313009A (en) * 1990-01-04 1994-05-17 Nrm International Technologies C.V. Nitration process
DE4309140C2 (de) * 1993-03-22 2001-09-20 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
TW236610B (en) * 1992-11-13 1994-12-21 Bayer Ag Preparation of dinitrotoluene
DE4410417A1 (de) * 1994-02-14 1995-08-17 Bayer Ag Verfahren zur adiabatischen Herstellung von Mononitrotoluolen
DE4411064A1 (de) * 1994-03-30 1995-10-05 Bayer Ag Verfahren zur adiabatischen Herstellung von Mononitrohalogenbenzolen
DE4428462A1 (de) * 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4428459A1 (de) * 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4437047A1 (de) * 1994-10-17 1996-04-18 Bayer Ag Verfahren zur Dinitrierung von aromatischen Verbindungen
US5763687A (en) 1995-12-15 1998-06-09 Mitsui Chemicals, Inc. Preparation process for aromatic mononitro compounds
PT1272268E (pt) * 2000-03-02 2012-07-24 Dow Global Technologies Llc Reator tubular, processo de realização de reações multifásicas líquido/ líquido num reator tubular, e um processo de nitração cíclica de compostos aromáticos num reator tubular
GB0307403D0 (en) 2003-03-31 2003-05-07 Medical Res Council Selection by compartmentalised screening
US20060078893A1 (en) 2004-10-12 2006-04-13 Medical Research Council Compartmentalised combinatorial chemistry by microfluidic control
GB0307428D0 (en) 2003-03-31 2003-05-07 Medical Res Council Compartmentalised combinatorial chemistry
US20050221339A1 (en) 2004-03-31 2005-10-06 Medical Research Council Harvard University Compartmentalised screening by microfluidic control
US7968287B2 (en) 2004-10-08 2011-06-28 Medical Research Council Harvard University In vitro evolution in microfluidic systems
DE102005057555B3 (de) * 2005-11-21 2007-05-16 Meissner Gmbh & Co Kg Josef Verfahren zur Herstellung von Salpetersäureestern einwertiger Alkohole
WO2007081387A1 (en) 2006-01-11 2007-07-19 Raindance Technologies, Inc. Microfluidic devices, methods of use, and kits for performing diagnostics
DE102006021857A1 (de) 2006-05-09 2007-11-15 Otto Bock Healthcare Ip Gmbh & Co. Kg Verfahren zum Gießen eines Prothesenschaftes
US9562837B2 (en) 2006-05-11 2017-02-07 Raindance Technologies, Inc. Systems for handling microfludic droplets
EP2530167A1 (en) 2006-05-11 2012-12-05 Raindance Technologies, Inc. Microfluidic Devices
US9074242B2 (en) 2010-02-12 2015-07-07 Raindance Technologies, Inc. Digital analyte analysis
EP3536396B1 (en) 2006-08-07 2022-03-30 The President and Fellows of Harvard College Fluorocarbon emulsion stabilizing surfactants
US8772046B2 (en) 2007-02-06 2014-07-08 Brandeis University Manipulation of fluids and reactions in microfluidic systems
US8592221B2 (en) 2007-04-19 2013-11-26 Brandeis University Manipulation of fluids, fluid components and reactions in microfluidic systems
DE102007059513A1 (de) 2007-12-11 2009-06-18 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol durch adiabate Nitrierung
WO2010009365A1 (en) 2008-07-18 2010-01-21 Raindance Technologies, Inc. Droplet libraries
US12038438B2 (en) 2008-07-18 2024-07-16 Bio-Rad Laboratories, Inc. Enzyme quantification
DE102008048713A1 (de) * 2008-09-24 2010-03-25 Bayer Materialscience Ag Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
CN102209703B (zh) 2008-11-10 2015-04-15 诺拉姆国际公司 制备单硝基苯的绝热工艺
JP5602143B2 (ja) * 2008-11-14 2014-10-08 ノラム インターナショナル リミテッド モノニトロベンゼンの生産における副産物ジニトロベンゼンの生成を低減する方法
CN101759568A (zh) * 2008-12-25 2010-06-30 南化集团研究院 硝基苯的绝热生产方法
DE102009005324B4 (de) 2009-01-16 2014-04-03 Plinke Gmbh Verfahren zur adiabatischen Nitrierung von Benzol
CN102333756B (zh) * 2009-02-26 2015-11-25 巴斯夫欧洲公司 制备硝化芳香族化合物及其混合物的方法
US8528589B2 (en) 2009-03-23 2013-09-10 Raindance Technologies, Inc. Manipulation of microfluidic droplets
WO2011042564A1 (en) 2009-10-09 2011-04-14 Universite De Strasbourg Labelled silica-based nanomaterial with enhanced properties and uses thereof
US10837883B2 (en) 2009-12-23 2020-11-17 Bio-Rad Laboratories, Inc. Microfluidic systems and methods for reducing the exchange of molecules between droplets
DE102010006984A1 (de) * 2010-02-05 2011-08-11 Bayer MaterialScience AG, 51373 Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
US10351905B2 (en) 2010-02-12 2019-07-16 Bio-Rad Laboratories, Inc. Digital analyte analysis
US9399797B2 (en) 2010-02-12 2016-07-26 Raindance Technologies, Inc. Digital analyte analysis
US9366632B2 (en) 2010-02-12 2016-06-14 Raindance Technologies, Inc. Digital analyte analysis
DE102010038519A1 (de) 2010-07-28 2012-02-02 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol durch adiabate Nitrierung
EP2622103B2 (en) 2010-09-30 2022-11-16 Bio-Rad Laboratories, Inc. Sandwich assays in droplets
WO2012109600A2 (en) 2011-02-11 2012-08-16 Raindance Technologies, Inc. Methods for forming mixed droplets
EP3736281A1 (en) 2011-02-18 2020-11-11 Bio-Rad Laboratories, Inc. Compositions and methods for molecular labeling
EP2772304B2 (de) 2011-05-19 2024-08-07 Josef Meissner GmbH & Co. KG Vorrichtungen zur Aufreinigung von Nitrierprodukten
EP2714970B1 (en) 2011-06-02 2017-04-19 Raindance Technologies, Inc. Enzyme quantification
US8841071B2 (en) 2011-06-02 2014-09-23 Raindance Technologies, Inc. Sample multiplexing
CN102311347B (zh) * 2011-06-28 2013-08-14 江苏科圣化工装备工程有限公司 由焦化苯连续生产混二硝基苯的装置及方法
US8658430B2 (en) 2011-07-20 2014-02-25 Raindance Technologies, Inc. Manipulating droplet size
US9150497B2 (en) 2011-10-14 2015-10-06 Council Of Scientific & Industrial Research Continuous two step flow synthesis of M-amino acetophenone
CN102516082B (zh) * 2011-11-28 2013-11-06 万华化学集团股份有限公司 由苯与混酸反应制备硝基苯以及洗涤粗硝基苯产物的方法
KR20140117474A (ko) * 2012-01-31 2014-10-07 바이엘 인텔렉쳐 프로퍼티 게엠베하 니트로벤젠을 제조하기 위한 방법 및 시스템
US8907144B2 (en) * 2012-03-22 2014-12-09 Noram International Limited Process for adiabatic production of mononitrotoluene
EP2877441B2 (de) 2012-07-27 2021-06-16 Covestro Intellectual Property GmbH & Co. KG Verfahren zur herstellung von nitrobenzol durch adiabate nitrierung
KR102066763B1 (ko) 2012-07-27 2020-01-15 코베스트로 도이칠란드 아게 단열 질화에 의한 니트로벤젠의 제조방법
PT2877443T (pt) 2012-07-27 2016-07-27 Covestro Deutschland Ag Processo para a produção de nitrobenzeno através de nitração adiabática
PT2991966T (pt) * 2013-04-29 2017-10-06 Covestro Deutschland Ag Processo para a produção de nitrobenzeno através de nitração adiabática
US11901041B2 (en) 2013-10-04 2024-02-13 Bio-Rad Laboratories, Inc. Digital analysis of nucleic acid modification
US9944977B2 (en) 2013-12-12 2018-04-17 Raindance Technologies, Inc. Distinguishing rare variations in a nucleic acid sequence from a sample
WO2015103367A1 (en) 2013-12-31 2015-07-09 Raindance Technologies, Inc. System and method for detection of rna species
US10647981B1 (en) 2015-09-08 2020-05-12 Bio-Rad Laboratories, Inc. Nucleic acid library generation methods and compositions
DE102017110084B4 (de) 2017-02-03 2019-07-04 Josef Meissner Gmbh & Co. Kg Verfahren und Anlage zur adiabatischen Nitrierung von Aromaten
EP3592727B1 (de) * 2017-03-07 2024-04-03 Covestro Deutschland AG Verfahren zur herstellung von nitrobenzol
WO2020011817A1 (de) 2018-07-12 2020-01-16 Covestro Deutschland Ag Verfahren zur herstellung von nitrobenzol durch adiabatisch betriebene nitrierung von benzol
DE102018217955B4 (de) * 2018-10-19 2020-06-04 Plinke Gmbh Verfahren zur Aufarbeitung von Mischsäure und Abwasser aus der Nitrierung von Aromaten sowie Vorrichtung zur Durchführung des Verfahrens
CN111393299A (zh) * 2020-05-06 2020-07-10 沈阳感光化工研究院有限公司 一种使用微通道连续流反应器对硝基苯进行硝化的方法
CN119451937A (zh) 2022-06-28 2025-02-14 巴斯夫欧洲公司 生产硝基苯的方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3087971A (en) * 1953-12-07 1963-04-30 Samuelsen Eirik Method for trinitrotoluene manufacture
GB1081091A (en) * 1964-01-08 1967-08-31 Ici Ltd Improvements in or relating to the preparation of dinitrotoluenes
US3928475A (en) * 1974-08-09 1975-12-23 Du Pont Azeotropic nitration of benzene
US4021498A (en) * 1975-12-09 1977-05-03 American Cyanamid Company Adiabatic process for nitration of nitratable aromatic compounds

Also Published As

Publication number Publication date
TR19875A (tr) 1980-04-03
AT357140B (de) 1980-06-25
AU518647B2 (en) 1981-10-15
DE2821571A1 (de) 1979-03-01
PL207037A1 (pl) 1979-05-07
IN147796B (nl) 1980-06-28
AU3529978A (en) 1979-10-25
BR7803249A (pt) 1979-03-27
ATA369978A (de) 1979-11-15
IT1103488B (it) 1985-10-14
PL113312B1 (en) 1980-12-31
BE867355A (fr) 1978-11-23
US4091042A (en) 1978-05-23
PT68105A (en) 1978-06-01
FR2400501A1 (fr) 1979-03-16
JPS5432424A (en) 1979-03-09
IT7849331A0 (it) 1978-05-12
DD136960A5 (de) 1979-08-08
GB1597433A (en) 1981-09-09
EG13569A (en) 1981-12-31
NL189757B (nl) 1993-02-16
CA1083608A (en) 1980-08-12
MX148692A (es) 1983-06-02
NL189757C (nl) 1993-07-16
NL7805409A (nl) 1979-02-21
CH639936A5 (de) 1983-12-15
FR2400501B1 (nl) 1984-01-27

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