CN87215236U - Multifunction sulfide separator - Google Patents
Multifunction sulfide separator Download PDFInfo
- Publication number
- CN87215236U CN87215236U CN 87215236 CN87215236U CN87215236U CN 87215236 U CN87215236 U CN 87215236U CN 87215236 CN87215236 CN 87215236 CN 87215236 U CN87215236 U CN 87215236U CN 87215236 U CN87215236 U CN 87215236U
- Authority
- CN
- China
- Prior art keywords
- hole
- bath heater
- electric water
- gas
- flowmeter
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 title claims abstract description 13
- 238000012360 testing method Methods 0.000 claims abstract description 12
- 238000010521 absorption reaction Methods 0.000 claims abstract description 7
- 239000007789 gas Substances 0.000 claims description 12
- 239000012159 carrier gas Substances 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 241001411320 Eriogonum inflatum Species 0.000 claims description 6
- 229920001296 polysiloxane Polymers 0.000 claims description 5
- 206010061307 Neck deformity Diseases 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 230000002459 sustained effect Effects 0.000 claims description 4
- 239000012774 insulation material Substances 0.000 claims description 3
- 230000028016 temperature homeostasis Effects 0.000 claims description 2
- 238000004458 analytical method Methods 0.000 abstract description 8
- 150000003568 thioethers Chemical class 0.000 abstract 1
- 239000002250 absorbent Substances 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 2
- 230000002745 absorbent Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 2
- 238000004448 titration Methods 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004737 colorimetric analysis Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- -1 p-aminophenyl amine Chemical class 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
Images
Landscapes
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
The utility model discloses a multifunction sulfide separator, which comprises a hydroelectric bath heater, a sample reactor, a supporting gas distributor, and an absorption reactor, being a special device for sulfides analysis as well as an applicable seven holes hydroelectric bath heater; the separated domain of the S+[=] separated by the device is 0.002 mg / liter-1000 mg / liter, which completely meets various analysis test requirements. The utility model has the advantages of high speed, simple structure, and good quality.
Description
The utility model relates to analytical and testing instrument.
At present, p-aminophenyl amine colourimetry or iodimetric titration are adopted in the analysis of sulfide mostly both at home and abroad, generally all need sample is carried out pre-service.Pretreatment unit mostly is the easy device that once can only handle what a sample, analysis speed steamed bun, difficult quality guarantee.
The purpose of this utility model is, designs a kind of multi-functional sulfide separation vessel, as the specialized equipment of sulfide analysis, has that analysis speed is fast, quality good, characteristic of simple structure, can become a suitable hydroelectric bath heater with seven holes again.
The utility model is according to such principle design: the sample of getting certain content sulfide is in reaction bulb, be placed on the electric water-bath heater, under certain water temperature, add an amount of acid solution, sulfide in the sample just generates hydrogen sulfide gas with the acid effect, taken in the container that fills absorbent solution by carrier gas stream immediately, reach sulfide (S thus
=) purpose of separating with raw sample.Separated sulfide is measured its concentration for colorimetric or iodimetric titration.
Below in conjunction with drawings and Examples the utility model is explained.
Fig. 1 is a structural representation of the present utility model.As known in the figure, the utility model is made up of electric water-bath heater, sample product reactor, carrier gas divider, absorption reactor thermally.The electricity water-bath heater has cylindrical housing (1) and inner bag (2), is filled with conventional insulation material (3) between shell (1) and inner bag (2), for example asbestos.Control desk (26) is arranged on the shell (1), power switch (22), thermoregulation knob (24) and pilot lamp (23) (25) are housed on it.Be equipped with Y shape electrothermal tube (5) in the inner bag (2), in order to the water (4) in the heating inner bag (2).Ajutage (19) communicates with inner bag (2) bottom, so that release water (4) wherein.The end face of electricity water-bath heater has seven apertures in the human head cover (6), has six to be evenly distributed on the through hole (27) of same garden on week on it, and each through hole (27) is placed a sample product reactor.Another through hole (28) is positioned at the central authorities of cover (6).
Sample product reactor has the flat bottom flask (7) that places electric water-bath heater and stretch out from its end face through hole (27), its bottleneck has ground bottle stopper (9), this bottle stopper (9) have with bottle in the short neck funnel (12) and the wireway (10) that passes to bottleneck that communicate and pass to bottle at the bottom of wireway (8).The carrier gas divider is made up of dicyclo support (29) and gas distributor (15).Described dicyclo support (29) places cover (6) central authorities, and communicates with through hole (28) on it.There are 12 hole locating rings (13) at the top of this dicyclo support (29) and are positioned at the following suitably sustained ring (30) of distance of ring (13), and 12 holes of locating ring (13) are evenly distributed on the circumference.Cylindrical shape gas distributor (15) places dicyclo support (29) top middle position, its center of top is connected to carrier gas pipe (18), side wall upper part have six along garden week equally distributed gas chew (31), each gas is chewed and is connected to a silicone tube (20), the other end of this silicone tube (20) and flowmeter (14) join, and the other end of flowmeter (14) and pipe (8) join.The word folder replaced during flowmeter (14) can be used.
Absorption reactor thermally is made up of the test tube plug (17) that absorbs test tube (16) and have a side wireway, and test tube (16) places on the sustained ring (30) by the perforate on the 12 hole locating rings (13).Pipe (10) passes to the part of test tube (16).
The course of work of the present utility model as shown in Figure 1.The sample that adds the desire separation is built bottle stopper (9) in flat bottom flask (7), be placed in the electric water-bath heater.Nitrogen (N
2) enter in the carrier gas divider (15) by pipe (18), give six flat bottom flasks (7) through pipe (20), flowmeter (14), pipe (8) uniform distribution, flowmeter (14) is regulated flow.Appropriate amount of acid solution (H
2SO
4) inject bottle (7) through short neck funnel (12), energized switch (22), electrothermal tube (5) is with water (4) heating, and knob (24) is adjusted temperature.The hydrogen sulfide gas that generates is by carrier gas (N
2) wireway of flowing through (10) brings into from flask (7) and absorb test tube (16), absorbed by wherein absorbent solution (11).After said process finished, water (4) was discharged by ajutage (19).
In said apparatus, remove sample product reactor, carrier gas divider, absorption reactor thermally, promptly become a very useful hydroelectric bath heater with seven holes.
Characteristics of the present utility model have: (1) analytical effect is good, and when being 200 microgram such as the measured object addition, the amount of recording is 196.96 micrograms, and the rate of recovery is 98.5%, has satisfied to analyze fully and has surveyed The quality requirement of examination; (2) S=separates field width, and scope is 0.002 mg/litre---1000 mg/litre; (3) analysis speed is fast, directly analyzes; (4) simple in structure, dependable performance is the dedicated analysis equipment of sulfide; (5) can as a suitable hydroelectric bath heater with seven holes, realize the characteristic of an apparatus multifunction.
Description of drawings: Fig. 1 is structural drawing of the present utility model (only marked one group of sample product reactor and absorption reactor thermally among the figure, omitted other five groups), wherein:
1---garden cylindrical outer casing 2---inner bag
3---insulation material 4---water
5---Y type electrothermal tube 6---seven apertures in the human head cover
7---flat bottom flask 8---wireway
9---ground bottle stopper 10---wireway
The short neck funnel of 11---absorbent solutions 12---
13---12 hole locating ring 14---flowmeter
15---gas distributors 16---absorb test tube
17---test tube plug 18---carrier gas pipe
19---ajutage 20---silicone tube
22---power switch 33,25---pilot lamp
24---thermoregulation knob 26---control desk
27,28---through hole 29---dicyclo support
30---sustained rings 31---are chewed by gas
Claims (2)
1, a kind of multi-functional sulfide separation vessel, by electric water-bath heater, sample product reactor, the carrier gas divider, absorption reactor thermally is formed, described electric water-bath heater has cylindrical housing (1), inner bag (2) and be filled in insulation material (3) between (1) (2), control desk (26) is arranged on the shell (1), power switch (22) is arranged on it, thermoregulation knob (24) and pilot lamp (23) (25), feature of the present utility model is, be equipped with Y shape electrothermal tube (5) in the described inner bag (2), ajutage (19) communicates with the inner bag that fills water (4) (2) bottom, the end face of described electric water-bath heater has seven apertures in the human head cover (6), there are six to be evenly distributed on the through hole (27) of same garden on week on it, another through hole (28) is positioned at cover (6) central authorities, each through hole (27) is placed a sample product reactor, described sample product reactor has the flat bottom flask (7) that places electric water-bath heater and stretch out from through hole (27), the bottleneck of described flask (7) has ground bottle stopper (9), this bottle stopper (9) have with bottle in the short neck funnel (12) and the wireway (10) that passes to bottleneck that communicate and pass to bottle at the bottom of wireway (8), described carrier gas divider is made up of the dicyclo support (29) and the gas distributor (15) that place cover (6) central authorities and communicate with hole (28), there are 12 hole locating rings (13) at the top of described dicyclo support (29) and are positioned at the following suitably sustained ring (30) of distance of ring (13), have on the locating ring (13) and be evenly distributed on ten two holes of a garden on week, described gas distributor (15) places dicyclo support (29) top central authorities, its center of top is connected to carrier gas pipe (18), side wall upper part have six along garden week equally distributed gas chew (31), each gas is chewed and is connected to a silicone tube (20), the other end of described silicone tube (20) and flowmeter (14) join, the other end of this flowmeter (14) and pipe (8) join, described absorption reactor thermally is formed with the test tube plug (17) that has the side wireway by absorbing test tube (16), and test tube (16) places on the sustained ring (30) by the perforate on the 12 hole locating rings (13).
2, multi-functional sulfide separation vessel according to claim 1 is characterized in that, the word folder replaced during described flowmeter (14) can be used.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 87215236 CN87215236U (en) | 1987-12-25 | 1987-12-25 | Multifunction sulfide separator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 87215236 CN87215236U (en) | 1987-12-25 | 1987-12-25 | Multifunction sulfide separator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN87215236U true CN87215236U (en) | 1988-08-31 |
Family
ID=4829409
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 87215236 Expired - Lifetime CN87215236U (en) | 1987-12-25 | 1987-12-25 | Multifunction sulfide separator |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN87215236U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100413594C (en) * | 2003-06-04 | 2008-08-27 | 吉耐尔基因方案解决有限公司 | Biological Material Processing Unit |
| CN104525075A (en) * | 2014-12-31 | 2015-04-22 | 周维保 | Device for reduction of copper oxide by hydrogen |
-
1987
- 1987-12-25 CN CN 87215236 patent/CN87215236U/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100413594C (en) * | 2003-06-04 | 2008-08-27 | 吉耐尔基因方案解决有限公司 | Biological Material Processing Unit |
| CN104525075A (en) * | 2014-12-31 | 2015-04-22 | 周维保 | Device for reduction of copper oxide by hydrogen |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4373024A (en) | Apparatus useful for foam breaking | |
| Le et al. | A new continuous hydride generator for the determination of arsenic, Antimony and tin by hybride generation atomic absorption spectrometry | |
| UA8348A1 (en) | converter for ammonia synthesis | |
| FR2519335B1 (en) | PRODUCTION OF HYDROCARBONS FROM METHANOL IN THE PRESENCE OF ZEOLITE TYPE CATALYSTS | |
| DE3160702D1 (en) | Device for the distribution to the cross-section of a receptacle of a gas flowing from a tube | |
| CN87215236U (en) | Multifunction sulfide separator | |
| US4456511A (en) | Photochemical method for generating chlorine dioxide gas | |
| ES2108007T3 (en) | DEVICE TO SEPARATE LIQUIDS AND / OR SOLIDS FROM A GASEOUS CURRENT. | |
| CN208414378U (en) | A kind of nucleic acid extraction purification devices | |
| CN102012369A (en) | Sensitive and stable atomic fluorescence generating system capable of atomizing continuously | |
| CA2289666C (en) | Method and apparatus for generating hydrogen gas by direct thermal decomposition of water | |
| Donnot et al. | Flash pyrolysis of tar from the pyrolysis of pine bark | |
| ES2190025T3 (en) | CONTINUOUS PREPARATION OF POLYETRAHYDROFURAN THROUGH A TRANSESTERIFICATION CASCADE WITH SELECTIVE FOAM DESTRUCTION. | |
| Parker et al. | The Catalyzed Reaction of Alkylmagnesium Halides wth Alkyl Halides. III. 1 Course of the Reaction | |
| CN219355731U (en) | Pretreatment device for synthetic ammonia raw material | |
| CN114713187B (en) | Liquid light hydrocarbon component adsorption dearsenization agent and preparation method thereof | |
| Earl | The colorful complexes of copper (II) | |
| CN212379151U (en) | Special purifying column for polycyclic aromatic hydrocarbon residues in traditional Chinese medicinal materials | |
| GB938406A (en) | Apparatus for the production of acetylene by incomplete combustion of hydrocarbons | |
| Konstantinova | Effect of Amount of Rhodium on the Adsorption and Electrocatalytic Properties of Rhodium Electrocatalysts | |
| CN206990543U (en) | A kind of energy-saving and emission-reduction monitor in real time and emergency management system | |
| CN208820020U (en) | A kind of lead-acid accumulator container formation device | |
| JPS57113353A (en) | Analyzer for isotope composition | |
| Walsh | Impact of copper smelter emissions on subalpine vegetation in the Anaconda-Pintler Range | |
| JPS57113352A (en) | Analyzer for isotope composition |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CX01 | Expiry of patent term |