CN222152078U - A liquid separation and purification device for multi-stage cleaning of solution - Google Patents
A liquid separation and purification device for multi-stage cleaning of solution Download PDFInfo
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- CN222152078U CN222152078U CN202420498423.XU CN202420498423U CN222152078U CN 222152078 U CN222152078 U CN 222152078U CN 202420498423 U CN202420498423 U CN 202420498423U CN 222152078 U CN222152078 U CN 222152078U
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- 239000007788 liquid Substances 0.000 title claims abstract description 129
- 238000000926 separation method Methods 0.000 title claims abstract description 30
- 238000004140 cleaning Methods 0.000 title claims abstract description 25
- 238000000746 purification Methods 0.000 title claims abstract description 9
- 230000007246 mechanism Effects 0.000 claims abstract description 41
- 238000007789 sealing Methods 0.000 claims description 13
- 238000009434 installation Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 230000008878 coupling Effects 0.000 claims description 2
- 238000010168 coupling process Methods 0.000 claims description 2
- 238000005859 coupling reaction Methods 0.000 claims description 2
- 239000000243 solution Substances 0.000 description 33
- 238000002474 experimental method Methods 0.000 description 8
- 238000007599 discharging Methods 0.000 description 7
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 229910000019 calcium carbonate Inorganic materials 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000593 microemulsion method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
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- Filtration Of Liquid (AREA)
Abstract
本实用新型涉及实验室器具技术领域，特别涉及一种用于溶液多级清洗的分液提纯装置，包括立式振动支架、多个分液漏斗，所述立式振动支架由上而下间隔设置有多块支撑板，多个所述分液漏斗依次插接在支撑板上的开孔内且并通过排液管串连连通形成多级分液机构，各级分液漏斗上位于所述排液管外侧设置有导流管口，所述导流管口内密封连接有导流管，所述导流管上端竖向伸入分液漏斗内且所述导流管伸入所述分液漏斗的高度可调，所述排液管及导流管上均设有控制阀，所述导流管下端通过导流软管与下一级分液机构的分液漏斗进液孔密封连通，本实用新型清洗、分液过程简单、连续、且清洗，分液时可直接针对目标溶液进行取液，有效减少分液排液时间。
The utility model relates to the technical field of laboratory equipment, and in particular to a liquid separation and purification device for multi-stage cleaning of a solution, comprising a vertical vibration support and a plurality of liquid separation funnels, wherein the vertical vibration support is provided with a plurality of support plates spaced from top to bottom, the plurality of liquid separation funnels are sequentially inserted into openings on the support plates and are connected in series through a liquid discharge pipe to form a multi-stage liquid separation mechanism, a guide pipe opening is provided on each level of the liquid separation funnel outside the liquid discharge pipe, a guide pipe is sealed and connected in the guide pipe opening, the upper end of the guide pipe vertically extends into the liquid separation funnel, and the height of the guide pipe extending into the liquid separation funnel is adjustable, the liquid discharge pipe and the guide pipe are both provided with a control valve, the lower end of the guide pipe is sealed and connected with a liquid inlet hole of the liquid separation funnel of the next level of liquid separation mechanism through a guide hose, the cleaning and liquid separation process of the utility model is simple, continuous, and clean, and liquid can be directly taken from a target solution during liquid separation, effectively reducing the liquid separation and drainage time.
Description
Technical Field
The utility model relates to the technical field of laboratory appliances, in particular to a liquid separating and purifying device for multi-stage cleaning of a solution.
Background
In the daily experiment process of a laboratory, a separating and purifying and impurity removing means with higher frequency is usually adopted for operation, but in the experiment, if the ideal purifying and impurity removing effect is to be achieved, multiple times of cleaning, liquid separation and purification are often needed, for example, in the process of preparing nano calcium carbonate by a microemulsion method, the mixed solution generating calcium carbonate sediment is needed to be transferred into the separating funnel for layering, the upper layer solution is cleaned with deionized water for 3 times, ethanol is added for precipitation, then centrifugation is carried out, the sediment is dispersed into n-hexane to form a transparent solution, so that the nano calcium carbonate product is obtained, the multiple cleaning process is complicated and intermittent, labor is wasted, a plurality of used vessels are needed, pollution is easy to be caused, in addition, in the daily experiment, when the solution is layered into two layers in the separating funnel, the target solution needed to be taken is the upper layer solution, the lower layer solution is needed to be discharged firstly, then the upper layer solution is needed to be discharged again, the required time is long, the experiment efficiency is greatly influenced, and in the liquid discharging process of the lower layer solution is easy to discharge part of the upper layer solution, so that the experiment result is influenced.
Disclosure of Invention
Aiming at the problems, the utility model aims to provide the liquid separating and purifying device for the multi-stage cleaning of the solution, which has the advantages that the cleaning and liquid separating processes are simple and continuous, the cleaning and liquid separating processes are all carried out in a closed container, the pollution risk is reduced, the liquid can be directly taken from the target solution during liquid separation, the liquid separating and discharging time is effectively shortened, and the cleaning and liquid separating and purifying efficiency is improved.
The liquid separating and purifying device for the solution multilevel cleaning comprises a vertical vibration support and a plurality of separating funnels, wherein a plurality of supporting plates are arranged on the vertical vibration support from top to bottom at intervals, openings for installing the separating funnels are formed in the supporting plates, an elastic buffer cushion is arranged in the openings, the separating funnels are sequentially inserted into the openings from top to bottom, the separating funnels are sequentially communicated with each other from top to bottom through liquid discharge pipes in series to form a multilevel liquid separating mechanism, a flow guide pipe orifice is arranged on the separating funnel of each liquid separating mechanism and is positioned outside the liquid discharge pipe, a flow guide pipe is connected in a sealing mode in the flow guide pipe orifice, the upper end of the flow guide pipe vertically extends into the separating funnels, the height of the flow guide pipe extending into the separating funnels is adjustable, control valves are arranged on the liquid discharge pipes and the flow guide pipes, the lower ends of the flow guide pipes are hermetically communicated with the liquid inlet holes of the separating funnels of the next level liquid separating mechanism through flow guide hoses, and the liquid feeding pipes are respectively provided with a liquid feeding pipe orifice and a sealing cover.
Further, the outer wall of the flow guiding pipe is provided with external threads, and the flow guiding pipe is in threaded connection with the flow guiding pipe orifice.
Further, the lower end of the liquid discharge pipe is connected with a section of a second guide hose through a pipe joint, and the lower end of the second guide hose is communicated with a separating funnel of a next-stage liquid separating mechanism in a sealing way through a liquid inlet hole II.
Further, vertical vibration support includes base and vertical bracing piece, the backup pad sets up on the vertical bracing piece, the base center is equipped with the bar groove, the left and right sides in bar groove from top to bottom all is provided with 2 at least stand pipes in the clearance, vertical bracing piece left and right sides rigid coupling has slidable grafting to be in the guide bar in the stand pipe, just be provided with buffer spring between stand pipe and the guide bar, be provided with vibration clearance between guide bar tip and the tip of stand pipe, the base top is provided with the vibration actuating mechanism that vibrates vertical bracing piece.
Further, the vibration driving mechanism comprises a cam driving mechanism, and the vertical supporting rod is provided with a bearing plate for bearing the thrust of the cam driving mechanism.
Further, the lower end of the vertical supporting rod is fixedly connected with a sliding block, a sliding groove capable of allowing the sliding block to slide left and right is formed in the bottom of the strip-shaped groove, and elastic buffer layers are arranged on two sides of the sliding block or/and the inner side of the sliding groove.
Further, the installation height of the supporting plate on the vertical supporting rod is adjustable.
Further, be provided with the screw thread on the vertical bracing piece, be provided with the round hole that can hold the bracing piece and pass in the backup pad, be located on the vertical bracing piece below equal threaded connection in backup pad has the nut that the location was used.
Before an experiment, the separating funnel of each liquid separating mechanism is sequentially inserted into an opening from top to bottom, the separating funnels of the liquid separating mechanisms are sequentially connected in series through liquid discharging pipes from top to bottom, when the target solution to be cleaned is the solution of the upper layer, the liquid discharging pipes of the liquid separating funnels and the control valves on the liquid guiding pipes are closed, the height of the liquid guiding pipes extending into the liquid separating funnels is adjusted, the flow guiding inlets at the tops of the liquid guiding pipes are positioned above the liquid level of the solution to be layered or cleaned, firstly, the uppermost liquid separating mechanism is opened to correspond to the sealing cover on the liquid outlet of the liquid separating funnels, the solution to be layered is placed into the liquid separating funnels from the liquid outlet of the upper layer to be kept stand for separation into two layers, after layering, when the target solution to be cleaned is the solution of the lower layer, the liquid separating funnels are directly opened, the liquid guiding pipes are vertically arranged into the upper layer solution, the liquid guiding inlets at the tops of the liquid guiding funnels are positioned at the bottom of the liquid guiding pipes, the liquid guiding pipes are opened, the liquid guiding pipes are vertically arranged into the liquid guiding funnels after the liquid guiding pipes are vertically arranged into the liquid separating funnels, the liquid separating pipes are driven to be cleaned by vibration, and then the liquid separating mechanisms are driven to be fully cleaned, and finally, the liquid is mixed and finally, the liquid is separated and washed by the liquid separating mechanism is driven and finally, after the liquid is fully washed.
The utility model has the beneficial effects that the cleaning and liquid separation processes are simple and continuous, and are all carried out in the closed container, so that the pollution risk is reduced, the liquid can be directly taken from the target solution during liquid separation, the liquid separation and discharging time is effectively shortened, and the cleaning and liquid separation and purification efficiency is improved.
Drawings
The utility model is described in more detail below, by way of example, with reference to the accompanying drawings, in which:
FIG. 1 is a schematic structural view of embodiment 1 of the present utility model.
Fig. 2 is a schematic view showing the installation structure of the vertical vibration cradle of embodiment 1 of the present utility model.
Fig. 3 is a schematic view showing the installation structure of the neutral vibration mount according to embodiment 2 of the present utility model.
FIG. 4 is a schematic diagram of the installation structure of the cam driving structure and the bearing plate in embodiment 2 of the present utility model.
In the figure: A hydraulic pump is composed of a base, a vertical support rod, a vibration driving mechanism, a bar-shaped groove, a 012, a guide pipe, a 013, a guide rod, a 014, a buffer spring, a 015, a vibration gap, a 016, a sliding block, a 017, a sliding groove, a 018, an elastic buffer layer, a 031, a cam driving mechanism, a 032, a bearing plate, a 1, a vertical vibration support, a 2, a separating funnel, a 3, a liquid separating mechanism, a 11, a support plate, a 12, an opening, a 13, an elastic buffer cushion layer, a 21, a liquid discharge pipe, a 22, a guide pipe orifice, a 23, a guide pipe, a 24, a control valve, a 25, a guide hose, a 26, a liquid inlet hole, a 27, a liquid feeding pipe orifice, a 28, a sealing cover, a 29, a second liquid inlet hole, a 231, a guide inlet and a 251.
Detailed Description
In the present utility model, for convenience of description, the description of the relative positional relationship of the respective components is described in terms of the layout patterns of the drawings of the specification, for example, the positional relationship of upper, lower, left, right, etc. is determined in terms of the layout directions in the drawings of the specification.
Embodiment 1, refer to fig. 1, fig. 2, a liquid separation purification device for solution multistage cleaning, including vertical vibration support 1, a plurality of separating funnel 2, vertical vibration support 1 is provided with polylith backup pad 11 from top to bottom interval, and the polylith all be equipped with the trompil 12 of installation separating funnel on the backup pad 11, be provided with elastic buffer layer 13 in the trompil 12, a plurality of separating funnel 2 from top to bottom peg graft in proper order in the trompil 12 and a plurality of separating funnel 2 from top to bottom loops through fluid-discharge tube 21 series connection and forms multistage liquid separation mechanism 3, is located on separating funnel 2 of each liquid separation mechanism 3 the fluid-conducting tube 21 outside is provided with water conservancy diversion mouth 22, sealing connection has honeycomb duct 23 in the water conservancy diversion mouth 22, the vertical stretch into in separating funnel 2 of honeycomb duct 23 upper end just the height-adjustable of separating funnel 2, all be equipped with control valve 24 on fluid-conducting tube 21 and the honeycomb duct 23, the 23 lower extreme passes through fluid-conducting hose 25 and the separating funnel 2 of next stage liquid separation mechanism 2 is equipped with sealing cover 27 on the fluid-conducting tube 27, the upper end is equipped with the fluid-conducting tube 27 on the fluid-conducting tube 2 and is equipped with sealing cover 27.
The outer wall of the flow guide pipe 23 is provided with external threads, the flow guide pipe 23 is in threaded connection with the flow guide pipe orifice 22, the lower end of the liquid discharge pipe 21 is connected with a section of a second flow guide hose 251 through a pipe joint, and the lower end of the second flow guide hose 251 is in sealing communication with the separating funnel 2 of the next-stage liquid separating mechanism 3 through an adapter and a second liquid inlet 29.
The vertical vibration support 1 comprises a base 01 and a vertical support rod 02, wherein the support plate 11 is arranged on the vertical support rod 02, a strip-shaped groove 011 is formed in the center of the base 01, at least 2 guide pipes 012 are arranged on the left side and the right side of the strip-shaped groove 011 from top to bottom in a clearance mode, guide rods 013 in the guide pipes 012 are fixedly connected on the left side and the right side of the vertical support rod 02 in a sliding mode, buffer springs 014 are arranged between the guide pipes 012 and the guide rods 013, vibration clearance 015 is formed between the end portions of the guide rods 013 and the end portions of the guide pipes 012, and a vibration driving mechanism 03 for vibrating the vertical support rod 02 is arranged at the top of the base 01.
The installation height of the supporting plate 11 on the vertical supporting rod 02 is adjustable, threads are arranged on the vertical supporting rod 02, round holes capable of allowing the supporting rod to penetrate through are formed in the supporting plate 11, and nuts for positioning are connected with the upper surface and the lower surface of the vertical supporting rod 02 in a threaded mode.
Before an experiment, the separating funnel 2 of each liquid separating mechanism 3 is sequentially inserted into an opening 12 from top to bottom, the separating funnels 2 of each liquid separating mechanism 3 are sequentially connected in series through a liquid discharge pipe 21 from top to bottom, a liquid discharge pipe 21 on the separating funnels 2 of each liquid separating mechanism 3 and a control valve 24 on a liquid guide pipe 23 are closed, the height of the liquid guide pipe 23 extending into the separating funnels 2 is regulated, a flow guide inlet 231 at the top of the liquid guide pipe 23 is positioned above the liquid level of a solution to be layered or cleaned, during the experiment, firstly, a sealing cover 28 on a liquid outlet 27 on the liquid separating funnels 2 corresponding to the uppermost liquid separating mechanism 3 is opened, the solution to be layered is placed into the separating funnels 2 from the liquid outlet 27 to be kept stand for two layers, after layering, when the target solution to be cleaned is the lower layer solution, the control valve 24 on the liquid discharge pipe 21 of the separating funnels 2 is directly opened, when the target solution to be cleaned is an upper solution, adjusting the height of the upper end of the guide pipe 23 vertically extending into the separating funnel 2 to enable the guide inlet 231 at the top of the guide pipe 23 to be positioned at the bottom of the upper solution, opening the control valve 24 on the guide pipe 23 to discharge liquid, placing cleaning liquid into the separating funnel 2 of the next-stage liquid separating mechanism 3 from the upper liquid pipe orifice 27 to clean the target solution, starting the vibration driving mechanism of the vertical vibration bracket 1 to enable the cleaning liquid and the target solution to be fully mixed and cleaned during cleaning, stopping the vibration driving mechanism to enable the cleaned mixed solution to be subjected to standing layering again, repeating the operation, discharging the target solution into the next-stage liquid separating mechanism 3 through the liquid discharging pipe 21 (or the guide pipe 23) to perform cleaning and liquid separating, until the cleaning of each level is completed.
In embodiment 2, referring to fig. 3 and fig. 4, as a further optimization design of embodiment 1, the vibration driving mechanism 03 includes a cam driving mechanism 031, a bearing plate 032 for bearing the thrust of the cam driving mechanism 031 is disposed on the vertical supporting rod 02, a slider 016 is fixedly connected to the lower end of the vertical supporting rod 02, a sliding groove 017 capable of allowing the slider 016 to slide left and right is disposed at the bottom of the bar-shaped groove 011, elastic buffer layers 018 are disposed on two sides of the slider 016 or/and the inner side of the sliding groove 017, and an elastic rubber ring having a buffer function is disposed at the top of the bar-shaped groove 011.
The foregoing has shown and described the basic principles, principal features and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the above-described embodiments, and that the above-described embodiments and descriptions are only preferred embodiments of the present invention, and are not intended to limit the invention, and that various changes and modifications may be made therein without departing from the spirit and scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (7)
1. The utility model provides a be used for solution multistage abluent branch liquid purification device, its characterized in that, includes vertical vibration support, a plurality of separating funnel, vertical vibration support from top to bottom interval is provided with the polylith backup pad, polylith all be equipped with the trompil of installation separating funnel in the backup pad, be provided with the elastic buffer layer in the trompil, a plurality of separating funnel from top to bottom peg graft in proper order in the trompil and a plurality of separating funnel from top to bottom loops through fluid-discharge tube series connection in proper order and forms multistage liquid separation mechanism, and the separating funnel of each liquid separation mechanism is gone up and is located the fluid-discharge tube outside is provided with the water conservancy diversion mouth of pipe, the intraductal sealing connection of water conservancy diversion mouth has the honeycomb duct, the vertical entering of upper end of liquid separation funnel just the honeycomb duct stretches into in the height-adjustable of separating funnel, all be equipped with the control valve on liquid discharge tube and the honeycomb duct, the honeycomb duct lower extreme is through water conservancy diversion hose and the liquid inlet sealing connection of the separating funnel of next level liquid separation mechanism, all be equipped with the liquid filling mouth of pipe and go up liquid sealing cap on the liquid discharge tube, the liquid pipe lower extreme is connected with two sections through the fluid-discharge tube coupling through two fluid-discharge tube fluid-feed inlets down, the second section fluid-discharge tube passes through the water diversion hose and second-level adapter.
2. The device for multi-stage cleaning of a liquid separating and purifying a solution according to claim 1, wherein the outer wall of the guide pipe is provided with external threads, and the guide pipe is in threaded connection with the opening of the guide pipe.
3. The liquid separating and purifying device for multi-stage cleaning of solution according to claim 1, wherein the vertical vibration support comprises a base and a vertical support rod, the support plate is arranged on the vertical support rod, a strip-shaped groove is arranged in the center of the base, at least 2 guide pipes are arranged on the left side and the right side of the strip-shaped groove from top to bottom in a gap mode, guide rods which can be slidably inserted into the guide pipes are fixedly connected on the left side and the right side of the vertical support rod, buffer springs are arranged between the guide pipes and the guide rods, a vibration gap is arranged between the end portions of the guide rods and the end portions of the guide pipes, and a vibration driving mechanism for vibrating the vertical support rod is arranged at the top of the base.
4. A liquid separation and purification device for multi-stage cleaning of a solution according to claim 3, wherein the vibration driving mechanism comprises a cam driving mechanism, and the vertical supporting rod is provided with a bearing plate for bearing the thrust of the cam driving mechanism.
5. The device for multi-stage cleaning of a liquid separating and purifying a solution according to claim 4, wherein a slide block is fixedly connected to the lower end of the vertical supporting rod, a slide groove capable of allowing the slide block to slide left and right is arranged at the bottom of the strip-shaped groove, and elastic buffer layers are arranged on two sides of the slide block or/and the inner side of the slide groove.
6. A liquid separation and purification device for multi-stage cleaning of a solution according to any one of claims 3 to 5, wherein the installation height of the supporting plate on the vertical supporting rod is adjustable.
7. The device for multi-stage cleaning of a liquid separating and purifying a solution according to claim 6, wherein the vertical supporting rod is provided with threads, the supporting plate is provided with round holes for allowing the supporting rod to pass through, and nuts for positioning are connected with the vertical supporting rod in a threaded manner on the upper surface and the lower surface of the supporting plate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202420498423.XU CN222152078U (en) | 2024-03-14 | 2024-03-14 | A liquid separation and purification device for multi-stage cleaning of solution |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202420498423.XU CN222152078U (en) | 2024-03-14 | 2024-03-14 | A liquid separation and purification device for multi-stage cleaning of solution |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN222152078U true CN222152078U (en) | 2024-12-13 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202420498423.XU Active CN222152078U (en) | 2024-03-14 | 2024-03-14 | A liquid separation and purification device for multi-stage cleaning of solution |
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| Country | Link |
|---|---|
| CN (1) | CN222152078U (en) |
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- 2024-03-14 CN CN202420498423.XU patent/CN222152078U/en active Active
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