CN221797656U - Vapor deposition equipment and upper liner thereof - Google Patents
Vapor deposition equipment and upper liner thereof Download PDFInfo
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Abstract
Description
技术领域Technical Field
本实用新型涉及半导体设备领域,特别涉及一种气相沉积设备及其上衬垫。The utility model relates to the field of semiconductor equipment, in particular to a vapor deposition device and an upper liner thereof.
背景技术Background Art
化学气相沉积(Chemical Vapor Deposition,简称CVD)是指反应物质在气态条件下在晶圆表面发生化学反应生成所需材料薄膜的过程。化学气相沉积工艺可以沉积多种材料,包括大范围的绝缘材料、大多数半导体材料和金属材料。Chemical Vapor Deposition (CVD) refers to the process in which reactants react chemically on the wafer surface under gaseous conditions to form a thin film of the desired material. The chemical vapor deposition process can deposit a variety of materials, including a wide range of insulating materials, most semiconductor materials, and metal materials.
CVD设备通常包含一反应腔,反应腔包括腔体和腔体顶盖。反应腔内设有托盘,一个或多个晶圆放置在托盘上。托盘下方还设有加热器,由托盘将加热器辐射的热量均匀传递给晶圆。腔体顶盖的下方还设有耐腐蚀的上衬垫,上衬垫的下表面与托盘的上表面之间形成反应区域。CVD equipment usually includes a reaction chamber, which includes a chamber body and a chamber cover. A tray is provided in the reaction chamber, and one or more wafers are placed on the tray. A heater is also provided under the tray, and the tray evenly transfers the heat radiated by the heater to the wafer. A corrosion-resistant upper liner is also provided under the chamber cover, and a reaction area is formed between the lower surface of the upper liner and the upper surface of the tray.
进气装置(与托盘的中心区域相对)穿过上衬垫固定安装在腔体顶盖上,工艺气体从进气装置引入至反应区域内,对放置在托盘上的晶圆进行处理。工艺制程中,托盘带动晶圆高速旋转,使到达托盘上表面的不同种类工艺气体在高速旋转的托盘驱动下达到充分混合。工艺气体在特定温度下反应并沉积在晶圆W表面形成所需材料的薄膜,晶圆温度是影响晶圆W上材料沉积的速率的重要因素之一。The inlet device (opposite to the center area of the tray) is fixedly installed on the top cover of the chamber through the upper liner. The process gas is introduced from the inlet device into the reaction area to process the wafer placed on the tray. During the process, the tray drives the wafer to rotate at high speed, so that different types of process gases reaching the upper surface of the tray are fully mixed under the drive of the high-speed rotating tray. The process gas reacts at a specific temperature and deposits on the surface of the wafer W to form a thin film of the required material. The wafer temperature is one of the important factors affecting the rate of material deposition on the wafer W.
为了使进气装置流出的工艺气体以层流的方式均匀通过晶圆上表面,上衬垫通常平行于托盘。然而,随着工艺气体沿着托盘的径向方向向外流动,工艺气体的密度逐渐降低,影响薄膜的生长速度。为保证薄膜的生长速度,需要向反应腔内提供大量的工艺气体,导致工艺气体的利用率较低。尤其在生产较大直径的晶圆时,工艺气体的浪费现象尤为突出。In order to make the process gas flowing out of the inlet device pass through the upper surface of the wafer evenly in a laminar flow, the upper liner is usually parallel to the tray. However, as the process gas flows outward along the radial direction of the tray, the density of the process gas gradually decreases, affecting the growth rate of the film. In order to ensure the growth rate of the film, a large amount of process gas needs to be provided to the reaction chamber, resulting in a low utilization rate of the process gas. Especially when producing wafers with larger diameters, the waste of process gas is particularly prominent.
如何提高工艺气体的利用率和薄膜的生长速度,并保证晶圆表面薄膜的一致性,是目前亟需解决的问题。How to improve the utilization rate of process gases and the growth rate of thin films, and ensure the consistency of thin films on the wafer surface, is a problem that needs to be solved urgently.
实用新型内容Utility Model Content
本实用新型的目的是提供一种气相沉积设备,该气相沉积设备的上衬垫由第二母线或第三母线绕进气装置的中心轴旋转而成。第二母线、第三母线上各点与晶圆承载面之间的竖直距离、各点与进气装置中心轴之间的水平距离满足设定条件。通过改变上衬垫的形貌,大大提高了反应腔内工艺气体的利用率(也称提高了源效)以及晶圆表面薄膜的沉积速率,同时还兼顾了晶圆表面薄膜厚度的一致性。通过本实用新型的气相沉积设备能够在消耗更少工艺气体的前提下,在晶圆表面快速生长出高质量的薄膜。The purpose of the utility model is to provide a vapor deposition device, in which the upper liner is formed by rotating the second busbar or the third busbar around the central axis of the air intake device. The vertical distance between each point on the second busbar and the third busbar and the wafer bearing surface, and the horizontal distance between each point and the central axis of the air intake device meet the set conditions. By changing the morphology of the upper liner, the utilization rate of the process gas in the reaction chamber (also known as improving the source efficiency) and the deposition rate of the thin film on the wafer surface are greatly improved, while also taking into account the consistency of the thickness of the thin film on the wafer surface. The vapor deposition device of the utility model can quickly grow a high-quality thin film on the wafer surface while consuming less process gas.
为了达到上述目的,本实用新型提供一种气相沉积设备,包含一反应腔,所述反应腔内的下方设有托盘,所述托盘的上表面为晶圆承载面,所述气相沉积设备包含:In order to achieve the above object, the utility model provides a vapor deposition device, comprising a reaction chamber, a tray is provided at the bottom of the reaction chamber, and the upper surface of the tray is a wafer carrying surface. The vapor deposition device comprises:
上衬垫,其设置在所述反应腔内并与所述晶圆承载面相对,所述上衬垫与所述晶圆承载面之间形成反应区域;An upper liner, which is arranged in the reaction chamber and opposite to the wafer carrying surface, and a reaction area is formed between the upper liner and the wafer carrying surface;
进气装置,所述进气装置用于横向地向所述反应区域内注入工艺气体;an air inlet device, the air inlet device being used to inject process gas laterally into the reaction zone;
所述上衬垫由第二母线绕所述进气装置的中心轴旋转而成,所述第二母线由第一母线绕其起始点在竖直方向上旋转设定的角度而成,所述第一母线具有靠近所述中心轴的所述起始点和远离所述中心轴的终点;点x、y为所述第一母线上的任意两点,点x、y与所述晶圆承载面之间的竖直距离分别记为h1、h2,点x、y与所述中心轴之间的水平距离分别记为l1、l2,点x、y满足h1×l1=h2×l2,The upper pad is formed by rotating the second busbar around the central axis of the air inlet device, the second busbar is formed by rotating the first busbar around its starting point in the vertical direction by a set angle, the first busbar has the starting point close to the central axis and the end point far away from the central axis; points x and y are any two points on the first busbar, the vertical distances between points x and y and the wafer bearing surface are recorded as h 1 and h 2 respectively, the horizontal distances between points x and y and the central axis are recorded as l 1 and l 2 respectively, and points x and y satisfy h 1 ×l 1 =h 2 ×l 2 ,
或者,所述上衬垫由第三母线绕所述进气装置的中心轴旋转而成,所述第三母线为直线,所述第三母线与所述第一母线共用所述起始点和终点。Alternatively, the upper gasket is formed by rotating a third busbar around a central axis of the air intake device, the third busbar is a straight line, and the third busbar shares the starting point and the end point with the first busbar.
可选的,所述角度为[-2°,5°],定义所述第一母线绕所述起始点向靠近所述晶圆承载面的方向旋转时所述角度为负值,所述第一母线绕所述起始点向远离所述晶圆承载面的方向旋转时所述角度为正值。Optionally, the angle is [-2°, 5°], which defines that when the first busbar rotates around the starting point toward the direction close to the wafer carrying surface, the angle is a negative value, and when the first busbar rotates around the starting point toward the direction away from the wafer carrying surface, the angle is a positive value.
可选的,所述反应腔包含腔室顶盖,其位于所述上衬垫的上方;所述腔室顶盖内设有冷却流体通道。Optionally, the reaction chamber includes a chamber top cover, which is located above the upper liner; a cooling fluid channel is provided in the chamber top cover.
可选的,所述托盘的下方设有加热装置;沿所述托盘的径向方向,将所述托盘虚拟划分为多个环形温度带,相邻的所述环形温度带之间的温差超过设定的温差阈值;沿所述腔室顶盖的径向方向,将所述腔室顶盖虚拟划分为与所述多个环形温度带分别对应的多个环形调温区;所述环形调温区内的冷却流体通道与腔室顶盖下表面之间的距离取决于对应的所述环形温度带的温度。Optionally, a heating device is provided under the tray; along the radial direction of the tray, the tray is virtually divided into a plurality of annular temperature zones, and the temperature difference between adjacent annular temperature zones exceeds a set temperature difference threshold; along the radial direction of the chamber top cover, the chamber top cover is virtually divided into a plurality of annular temperature adjustment zones corresponding to the plurality of annular temperature zones respectively; the distance between the cooling fluid channel in the annular temperature adjustment zone and the lower surface of the chamber top cover depends on the temperature of the corresponding annular temperature zone.
可选的,所述腔室顶盖与所述上衬垫之间设有调温机构。Optionally, a temperature regulating mechanism is provided between the chamber top cover and the upper liner.
可选的,所述调温机构包括导热板;所述导热板的上表面贴合所述腔室顶盖的下表面。Optionally, the temperature adjustment mechanism includes a heat conducting plate; the upper surface of the heat conducting plate is in contact with the lower surface of the chamber top cover.
可选的,所述调温机构还包括形成在所述导热板与所述上衬垫之间的间隙。Optionally, the temperature adjustment mechanism further includes a gap formed between the heat conducting plate and the upper pad.
可选的,沿着远离所述进气装置的方向,所述间隙先变小后变大。Optionally, the gap first becomes smaller and then becomes larger in a direction away from the air intake device.
可选的,沿着远离所述进气装置的方向,所述导热板的厚度先变厚后变薄。Optionally, along the direction away from the air intake device, the thickness of the heat conducting plate first becomes thicker and then becomes thinner.
可选的,沿着远离所述进气装置的方向,所述导热板的表面发射率先变大后变小。Optionally, along the direction away from the air intake device, the surface emission of the heat conducting plate first increases and then decreases.
可选的,所述气相沉积设备还包括传热气体输入端和传热气体输出端,用于向所述间隙提供流动的传热气体。Optionally, the vapor deposition equipment further comprises a heat transfer gas input end and a heat transfer gas output end, for providing flowing heat transfer gas to the gap.
可选的,所述传热气体的组分可调。Optionally, the composition of the heat transfer gas is adjustable.
可选的,所述气相沉积设备还包括抽气环,所述抽气环围绕设置在所述托盘的侧下方。Optionally, the vapor deposition equipment further comprises an exhaust ring, which is arranged around the lower side of the tray.
可选的,所述抽气环包含内环、外环以及连接所述内环和外环的环顶面;沿抽气环的周向方向,在所述环顶面开有多个抽气孔。Optionally, the air pumping ring includes an inner ring, an outer ring and a ring top surface connecting the inner ring and the outer ring; and a plurality of air pumping holes are opened on the ring top surface along the circumferential direction of the air pumping ring.
可选的,所述气相沉积设备还包括侧壁衬垫,所述侧壁衬垫围绕所述托盘的外周设置,所述侧壁衬垫位于所述上衬垫和抽气环之间。Optionally, the vapor deposition equipment further comprises a side wall liner, wherein the side wall liner is arranged around the outer circumference of the tray, and the side wall liner is located between the upper liner and the vacuum ring.
可选的,所述侧壁衬垫的上端具有向所述进气装置方向延伸的气流引导部。Optionally, the upper end of the side wall liner has an airflow guide portion extending toward the air intake device.
可选的,所述上衬垫还包括从所述终点向远离所述中心轴的方向延伸的上衬垫承载部,所述上衬垫承载部的底面与所述气流引导部的顶面贴合。Optionally, the upper pad further includes an upper pad bearing portion extending from the end point in a direction away from the central axis, and a bottom surface of the upper pad bearing portion is in contact with a top surface of the airflow guiding portion.
可选的,所述进气装置包括位于不同高度的出气端,最接近所述上衬垫的所述出气端用于供应非活性气体。Optionally, the air inlet device includes air outlets located at different heights, and the air outlet closest to the upper pad is used to supply inactive gas.
本实用新型还提供一种上衬垫,所述上衬垫用于气相沉积设备,所述气相沉积设备包含一反应腔,所述反应腔内的下方设有托盘,所述托盘的上表面为晶圆承载面;The utility model also provides an upper liner, the upper liner is used for a vapor deposition device, the vapor deposition device comprises a reaction chamber, a tray is provided below the reaction chamber, and the upper surface of the tray is a wafer bearing surface;
所述上衬垫设置在所述反应腔内并与所述晶圆承载面相对,所述上衬垫与所述晶圆承载面之间形成反应区域;所述上衬垫的厚度大于2mm;The upper liner is arranged in the reaction chamber and is opposite to the wafer carrying surface, and a reaction area is formed between the upper liner and the wafer carrying surface; the thickness of the upper liner is greater than 2 mm;
所述气相沉积设备还包含一进气装置,所述进气装置用于横向地向所述反应区域内注入工艺气体;The vapor deposition apparatus further comprises a gas inlet device, the gas inlet device being used to inject process gas laterally into the reaction area;
所述上衬垫由第二母线绕所述进气装置的中心轴旋转而成,所述第二母线由第一母线绕其起始点在竖直方向上旋转设定的角度而成,所述第一母线具有靠近所述中心轴的所述起始点和远离所述中心轴的终点;点x、y为所述第一母线上的任意两点,点x、y与所述晶圆承载面之间的竖直距离分别记为h1、h2,点x、y与所述中心轴之间的水平距离分别记为l1、l2,点x、y满足h1×l1=h2×l2,The upper pad is formed by rotating the second busbar around the central axis of the air inlet device, the second busbar is formed by rotating the first busbar around its starting point in the vertical direction by a set angle, the first busbar has the starting point close to the central axis and the end point far away from the central axis; points x and y are any two points on the first busbar, the vertical distances between points x and y and the wafer bearing surface are recorded as h 1 and h 2 respectively, the horizontal distances between points x and y and the central axis are recorded as l 1 and l 2 respectively, and points x and y satisfy h 1 ×l 1 =h 2 ×l 2 ,
或者,所述上衬垫由第三母线绕所述进气装置的中心轴旋转而成,所述第三母线为直线,所述第三母线与所述第一母线共用所述起始点和终点。Alternatively, the upper gasket is formed by rotating a third busbar around a central axis of the air intake device, the third busbar is a straight line, and the third busbar shares the starting point and the end point with the first busbar.
可选的,所述角度为[-2°,5°],定义所述第一母线绕所述起始点向靠近所述晶圆承载面的方向旋转时所述角度为负值,所述第一母线绕所述起始点向远离所述晶圆承载面的方向旋转时所述角度为正值。Optionally, the angle is [-2°, 5°], which defines that when the first busbar rotates around the starting point toward the direction close to the wafer carrying surface, the angle is a negative value, and when the first busbar rotates around the starting point toward the direction away from the wafer carrying surface, the angle is a positive value.
与现有技术相比,本实用新型的有益效果在于:Compared with the prior art, the beneficial effects of the present invention are:
1)本实用新型气相沉积设备的上衬垫由第二母线/第三母线绕进气装置的中心轴旋转而成。第二母线/第三母线上各点与晶圆承载面之间的竖直距离、各点与进气装置中心轴之间的水平距离满足设定条件。通过改变上衬垫的形貌,大大提高了反应腔内工艺气体的利用率以及晶圆表面薄膜的沉积速率,同时还兼顾了晶圆表面薄膜厚度的一致性。通过本实用新型的气相沉积设备能够在消耗更少工艺气体的前提下,在晶圆表面快速生长出高质量的薄膜。1) The upper liner of the vapor deposition equipment of the utility model is formed by rotating the second busbar/third busbar around the central axis of the air intake device. The vertical distance between each point on the second busbar/third busbar and the wafer bearing surface, and the horizontal distance between each point and the central axis of the air intake device meet the set conditions. By changing the morphology of the upper liner, the utilization rate of the process gas in the reaction chamber and the deposition rate of the thin film on the wafer surface are greatly improved, while also taking into account the consistency of the thickness of the thin film on the wafer surface. The vapor deposition equipment of the utility model can quickly grow a high-quality thin film on the wafer surface while consuming less process gas.
2)本实用新型的腔室顶盖中设有冷却流体通道,能够有效带走由托盘、晶圆辐射至上衬垫的热量,减少反应气体在上衬垫表面沉积,从而有效减少反应腔内的颗粒污染物,显著提高了晶圆的成品率。同时还能够降低反应腔的清洗频率、大大提高了晶圆加工效率、明显降低了晶圆加工成本。2) The chamber top cover of the utility model is provided with a cooling fluid channel, which can effectively remove the heat radiated from the tray and the wafer to the upper liner, reduce the deposition of the reaction gas on the surface of the upper liner, and thus effectively reduce the particle pollutants in the reaction chamber, significantly improving the wafer yield. At the same time, it can also reduce the cleaning frequency of the reaction chamber, greatly improve the wafer processing efficiency, and significantly reduce the wafer processing cost.
3)本实用新型中,根据托盘表面的温差,将托盘虚拟划分为多个环形温度带,并将腔室顶盖虚拟划分为与所述多个环形温度带对应的环形调温区,若环形温度带的温度较高/较低,对应环形调温区内冷却流体通道与腔室顶盖下表面之间的距离较近/较远。这样可以按区域调节上衬垫的温度,有利于减小上衬垫的温度梯度,避免上衬垫发生变形。通过提高上衬垫温度的一致性,还可以提高反应腔内工艺气体温度的一致性(上衬垫与反应腔内的工艺气体之间存在热传递),有益于在晶圆表面生长厚度均匀的薄膜。3) In the present invention, the tray is virtually divided into a plurality of annular temperature zones according to the temperature difference on the tray surface, and the chamber top cover is virtually divided into annular temperature adjustment zones corresponding to the plurality of annular temperature zones. If the temperature of the annular temperature zone is higher/lower, the distance between the cooling fluid channel in the corresponding annular temperature adjustment zone and the lower surface of the chamber top cover is closer/farther. In this way, the temperature of the upper liner can be adjusted by region, which is beneficial to reduce the temperature gradient of the upper liner and avoid deformation of the upper liner. By improving the consistency of the temperature of the upper liner, the consistency of the temperature of the process gas in the reaction chamber can also be improved (there is heat transfer between the upper liner and the process gas in the reaction chamber), which is beneficial to growing a thin film with uniform thickness on the surface of the wafer.
4)本实用新型在腔室顶盖与上衬垫之间设有调温机构,所述调温机构包括设置在腔室顶盖与上衬垫之间的导热板,以及形成在导热板与上衬垫之间的间隙。通过导热板、间隙内的传热气体加强了上衬垫与腔室顶盖之间的热传递,有利于导走上衬垫的热量,防止薄膜在上衬垫表面沉积。4) The utility model is provided with a temperature regulating mechanism between the chamber top cover and the upper liner, and the temperature regulating mechanism includes a heat conducting plate arranged between the chamber top cover and the upper liner, and a gap formed between the heat conducting plate and the upper liner. The heat transfer between the upper liner and the chamber top cover is enhanced by the heat conducting plate and the heat transfer gas in the gap, which is conducive to conducting the heat of the upper liner and preventing the deposition of a film on the surface of the upper liner.
5)沿着远离进气装置的方向,本实用新型中导热板的厚度、表面发射率、间隙大小随托盘温度变化而变化,实现按区域调节上衬垫的温度,保证上衬垫温度的一致性。5) Along the direction away from the air inlet device, the thickness, surface emissivity and gap size of the heat conduction plate in the utility model change with the temperature of the tray, so as to adjust the temperature of the upper liner by area and ensure the consistency of the temperature of the upper liner.
6)本实用新型中,可以根据反应腔内的工艺、反应腔内的温度实时调节传热气体的组分,以此实时调节上衬垫的温度。在不同材料的沉积工艺中,均能够减少上衬垫的沉积物。6) In the present invention, the composition of the heat transfer gas can be adjusted in real time according to the process and temperature in the reaction chamber, thereby adjusting the temperature of the upper liner in real time. In the deposition process of different materials, the deposits on the upper liner can be reduced.
附图说明BRIEF DESCRIPTION OF THE DRAWINGS
为了更清楚地说明本实用新型技术方案,下面将对描述中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图是本实用新型的一个实施例,对于本领域普通技术人员来讲,在不付出创造性劳动的前提下,还可以根据这些附图获得其他的附图:In order to more clearly illustrate the technical solution of the utility model, the following is a brief introduction to the drawings required for the description. Obviously, the drawings described below are an embodiment of the utility model. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work:
图1为一种气相沉积设备的示意图;FIG1 is a schematic diagram of a vapor deposition apparatus;
图2为图1的A-A视图;Fig. 2 is the A-A view of Fig. 1;
图3为本实用新型实施例一中,气相沉积设备的示意图;FIG3 is a schematic diagram of a vapor deposition device in Embodiment 1 of the present invention;
图4为本实用新型实施例一中,进气装置的示意图;FIG4 is a schematic diagram of an air intake device in Embodiment 1 of the present utility model;
图5为本实用新型实施例一中,托盘、侧壁衬垫、抽气环的俯视图;FIG5 is a top view of the tray, the side wall gasket, and the air pumping ring in the first embodiment of the present utility model;
图6为本实用新型实施例一、实施例二中,第一母线、第二母线、第三母线的示意图;FIG6 is a schematic diagram of the first busbar, the second busbar, and the third busbar in Embodiment 1 and Embodiment 2 of the present utility model;
图7为生成图1中气相沉积设备的上衬垫的水平直线示意图;FIG7 is a schematic diagram of a horizontal straight line for generating an upper liner of the vapor deposition apparatus of FIG1 ;
图8为多个实施例中,晶圆表面薄膜平均生长速度、薄膜一致性差异的对比图;FIG8 is a comparison diagram of average growth rate of thin films on wafer surfaces and differences in film consistency in multiple embodiments;
图9为多个实施例中,沿晶圆径向方向,晶圆表面薄膜的沉积速度示意图;FIG9 is a schematic diagram of the deposition rate of a thin film on a wafer surface along the radial direction of the wafer in multiple embodiments;
图10为本实用新型实施例三中,将托盘划分为多个环形温度带、将腔室顶盖划分为多个环形调温区的示意图;FIG10 is a schematic diagram of dividing the tray into a plurality of annular temperature zones and the chamber top cover into a plurality of annular temperature adjustment zones in Embodiment 3 of the present invention;
图11为本实用新型实施例四中,具有渐变厚度的导热板的示意图。FIG. 11 is a schematic diagram of a heat conducting plate with a gradually varying thickness in Embodiment 4 of the present invention.
具体实施方式DETAILED DESCRIPTION
下面将结合本实用新型实施例中的附图,对本实用新型实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本实用新型一部分实施例,而不是全部的实施例。基于本实用新型中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本实用新型保护的范围。The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.
应当理解,当在本说明书和所附权利要求书中使用时,术语“包括”指示所描述特征、整体、步骤、操作、元素和/或组件的存在,但并不排除一个或多个其它特征、整体、步骤、操作、元素、组件和/或其集合的存在或添加。It should be understood that when used in this specification and the appended claims, the term "comprising" indicates the presence of described features, integers, steps, operations, elements and/or components, but does not exclude the presence or addition of one or more other features, integers, steps, operations, elements, components and/or groups thereof.
还应当理解,在此本申请说明书中所使用的术语仅仅是出于描述特定实施例的目的而并不意在限制本申请。如在本申请说明书和所附权利要求书中所使用的那样,除非上下文清楚地指明其它情况,否则单数形式的“一”、“一个”及“该”意在包括复数形式。It should also be understood that the terms used in this application specification are only for the purpose of describing specific embodiments and are not intended to limit the application. As used in this application specification and the appended claims, unless the context clearly indicates otherwise, the singular forms "a", "an" and "the" are intended to include plural forms.
还应当进一步理解,在本申请说明书和所附权利要求书中使用的术语“和/或”是指相关联列出的项中的一个或多个的任何组合以及所有可能组合,并且包括这些组合。It should be further understood that the term “and/or” used in the specification and appended claims refers to any combination and all possible combinations of one or more of the associated listed items, and includes these combinations.
如在本说明书和所附权利要求书中所使用的那样,术语“如果”可以依据上下文被解释为“当...时”或“一旦”或“响应于确定”或“响应于检测到”。类似地,短语“如果确定”或“如果检测到[所描述条件或事件]”可以依据上下文被解释为意指“一旦确定”或“响应于确定”或“一旦检测到[所描述条件或事件]”或“响应于检测到[所描述条件或事件]”。As used in this specification and the appended claims, the term "if" may be interpreted as "when" or "upon" or "in response to determining" or "in response to detecting," depending on the context. Similarly, the phrases "if it is determined" or "if [described condition or event] is detected" may be interpreted as meaning "upon determination" or "in response to determining" or "upon detection of [described condition or event]" or "in response to detecting [described condition or event]," depending on the context.
另外,在本申请的描述中,术语“第一”、“第二”、“第三”等仅用于区分描述,而不能理解为指示或暗示相对重要性。In addition, in the description of the present application, the terms "first", "second", "third", etc. are only used to distinguish the description and cannot be understood as indicating or implying relative importance.
图1为一种气相沉积设备1,其具有一个反应腔100,在所述反应腔100中可对晶圆W进行处理。反应腔100包含腔室顶盖101和腔室主体102。所述腔室顶盖101覆盖所述腔室主体102,通过腔室顶盖101、腔室主体102共同围成气密性的内部处理空间。腔室顶盖101通常采用金属材料(例如不锈钢)。尽管图1中所示的腔室主体102为圆筒形的,其也可以是其它形状,例如方形、六角形、八角形或任意其他适当的形状。FIG. 1 is a vapor deposition device 1, which has a reaction chamber 100, in which a wafer W can be processed. The reaction chamber 100 includes a chamber cover 101 and a chamber body 102. The chamber cover 101 covers the chamber body 102, and the chamber cover 101 and the chamber body 102 together form an airtight internal processing space. The chamber cover 101 is usually made of metal material (such as stainless steel). Although the chamber body 102 shown in FIG. 1 is cylindrical, it can also be other shapes, such as square, hexagonal, octagonal or any other suitable shape.
如图1所示,进气装置107(通常采用耐腐蚀且具有良好导热率的不锈钢材料)的顶部穿设腔室顶盖位于反应腔100内。托盘109设置在进气装置107下方,并与进气装置107相对,托盘109的上表面为晶圆承载面1091。所述晶圆承载面1091与腔室顶盖101之间形成反应区域。进气装置107气路连通外部的工艺气体供应装置(图中未示出),用于向所述反应区域内输送工艺气体。工艺气体可包括载体气体(载气)和工艺气体,工艺气体可包括III族气体与V族气体。在典型的金属有机化学气相沉积过程中,载体气体可为氮气、氢气或氩气等气体。As shown in FIG1 , the top of the gas inlet device 107 (usually made of corrosion-resistant stainless steel with good thermal conductivity) is penetrated by a chamber top cover and is located in the reaction chamber 100. The tray 109 is arranged below the gas inlet device 107 and opposite to the gas inlet device 107, and the upper surface of the tray 109 is a wafer carrying surface 1091. A reaction area is formed between the wafer carrying surface 1091 and the chamber top cover 101. The gas path of the gas inlet device 107 is connected to an external process gas supply device (not shown in the figure) for conveying process gas into the reaction area. The process gas may include a carrier gas (carrier gas) and a process gas, and the process gas may include a group III gas and a group V gas. In a typical metal organic chemical vapor deposition process, the carrier gas may be a gas such as nitrogen, hydrogen or argon.
托盘109的材料通常为石墨,具有良好的导热性。托盘下方设有加热元件120,通过所述加热元件120加热托盘109,托盘109再将加热元件120提供的热能传递至晶圆W,工艺气体在特定温度下反应并沉积在晶圆W上形成所需材料的薄膜。The material of the tray 109 is usually graphite, which has good thermal conductivity. A heating element 120 is provided under the tray, and the tray 109 is heated by the heating element 120. The tray 109 then transfers the heat energy provided by the heating element 120 to the wafer W. The process gas reacts at a specific temperature and is deposited on the wafer W to form a thin film of the desired material.
托盘109底部固定连接一驱动轴104(可以由外部的电机或气缸驱动),该驱动轴104的底部竖直向下穿设腔室主体102的底壁并位于反应腔100的外部。通过所述驱动轴104驱动托盘109高速旋转,使到达托盘109上表面的不同种类工艺气体在高速旋转的托盘109驱动下达到充分混合。The bottom of the tray 109 is fixedly connected to a driving shaft 104 (which can be driven by an external motor or cylinder), and the bottom of the driving shaft 104 vertically passes through the bottom wall of the chamber body 102 and is located outside the reaction chamber 100. The driving shaft 104 drives the tray 109 to rotate at a high speed, so that different types of process gases reaching the upper surface of the tray 109 are fully mixed under the driving of the high-speed rotating tray 109.
所述排气装置103用于排放反应腔100内的气体,包括反应生成的废气,和未来得及参加反应的部分工艺气体。The exhaust device 103 is used to exhaust the gas in the reaction chamber 100, including the waste gas generated by the reaction and part of the process gas that does not have time to participate in the reaction.
上衬垫106设置在在腔室顶盖101的下方,用于隔离反应腔100内辐射到腔室顶盖101的热量,以及防止在腔室顶盖101上形成沉积物。上衬垫106的材料可以是石墨。上衬垫106的厚度一般大于2mm,以提供足够的刚度。图1中的腔室顶盖101和上衬垫106均具有平板型的结构,可以避免反应室腔100存在大规模垂直方向的扩散气流,保证反应腔100内的气流为平流状态,提高反应腔100内气流分布的均一性。The upper liner 106 is arranged below the chamber top cover 101, and is used to isolate the heat radiated from the reaction chamber 100 to the chamber top cover 101, and to prevent the formation of deposits on the chamber top cover 101. The material of the upper liner 106 can be graphite. The thickness of the upper liner 106 is generally greater than 2mm to provide sufficient rigidity. The chamber top cover 101 and the upper liner 106 in FIG. 1 both have a flat plate structure, which can avoid the existence of large-scale vertical diffusion airflow in the reaction chamber 100, ensure that the airflow in the reaction chamber 100 is in a horizontal flow state, and improve the uniformity of the airflow distribution in the reaction chamber 100.
由内而外,沿着托盘109的径向方向,工艺气体流动截面108的面积逐渐增大。所述流动截面108为反应腔100内与进气装置107同中心轴的筒形截面,所述筒形截面的顶部、底部分别落在上衬垫106、晶圆承载面1091上。如图1、图2所示,流动截面108与进气装置中心轴的水平距离为l时,该流动截面108的面积s=2π×l×h,h表示流动截面108的高度。当上衬垫106为平板型结构时,h为上衬垫106与晶圆承载面1091之间的竖直距离。From the inside to the outside, along the radial direction of the tray 109, the area of the process gas flow section 108 gradually increases. The flow section 108 is a cylindrical section with the same central axis as the gas inlet device 107 in the reaction chamber 100, and the top and bottom of the cylindrical section fall on the upper pad 106 and the wafer support surface 1091 respectively. As shown in Figures 1 and 2, when the horizontal distance between the flow section 108 and the central axis of the gas inlet device is l, the area of the flow section 108 is s=2π×l×h, where h represents the height of the flow section 108. When the upper pad 106 is a flat plate structure, h is the vertical distance between the upper pad 106 and the wafer support surface 1091.
自进气装置107流出的工艺气体朝着远离进气装置107的方向流动的过程中,流动截面108面积逐渐增大,因而工艺气体的密度逐渐降低,薄膜的沉积速度也越慢。为防止反应腔100内部的工艺气体在其流动方向上逐渐稀薄,则需要加大工艺气体的投放量,这就导致工艺气体的投放量会远大于实际反应所需求用量,造成了浪费。As the process gas flowing out of the gas inlet device 107 flows in a direction away from the gas inlet device 107, the flow cross section 108 gradually increases, so the density of the process gas gradually decreases, and the deposition speed of the film also becomes slower. In order to prevent the process gas inside the reaction chamber 100 from becoming gradually thinner in its flow direction, it is necessary to increase the amount of process gas added, which results in the amount of process gas added being much larger than the amount required for the actual reaction, resulting in waste.
另一方面,上衬垫106所受的热辐射较大,工艺气体容易在上衬垫106表面沉积。上衬垫106表面的沉积物剥落后,容易在反应腔100内形成颗粒污染物,大大降低了晶圆W的成品率。On the other hand, the upper liner 106 is subjected to greater heat radiation, and the process gas is easily deposited on the surface of the upper liner 106. After the deposits on the surface of the upper liner 106 are peeled off, particle contaminants are easily formed in the reaction chamber 100, which greatly reduces the yield of the wafer W.
本实用新型提供了一种气相沉积设备,该气相沉积设备的上衬垫由第二母线或第三母线绕进气装置107的中心轴旋转而成。第二母线、第三母线上各点与晶圆承载面1091之间的竖直距离、与进气装置中心轴之间的水平距离满足设定条件。本实用新型通过改变上衬垫106的形貌,大大提高了反应腔100内工艺气体的利用率以及晶圆表面薄膜的沉积速率,同时还兼顾了晶圆表面薄膜厚度的一致性。通过本实用新型的气相沉积设备能够在晶圆表面快速生长出高质量的薄膜。同时本实用新型还能够按区域调节上衬垫106的温度,快速导走上衬垫106热量的同时,还提高了上衬垫106温度的一致性,不仅大大减少了上衬垫106表面的沉积物,还能够避免上衬垫106因热应力发生变形而损坏。The utility model provides a vapor deposition device, the upper pad of which is formed by rotating the second busbar or the third busbar around the central axis of the air intake device 107. The vertical distance between each point on the second busbar and the third busbar and the wafer bearing surface 1091, and the horizontal distance between each point and the central axis of the air intake device meet the set conditions. The utility model greatly improves the utilization rate of the process gas in the reaction chamber 100 and the deposition rate of the thin film on the wafer surface by changing the morphology of the upper pad 106, while also taking into account the consistency of the thickness of the thin film on the wafer surface. The vapor deposition device of the utility model can quickly grow a high-quality thin film on the wafer surface. At the same time, the utility model can also adjust the temperature of the upper pad 106 according to the region, quickly conduct the heat of the upper pad 106, and also improve the consistency of the temperature of the upper pad 106, which not only greatly reduces the deposits on the surface of the upper pad 106, but also can avoid the deformation and damage of the upper pad 106 due to thermal stress.
实施例一Embodiment 1
本实用新型提供一种气相沉积设备2,如图3所示,其包含一反应腔200。所述反应腔200包含腔室顶盖201和腔室主体202。所述反应腔200内设有托盘209、进气装置207、上衬垫206、抽气环230、侧壁衬垫270,所述腔室顶盖201位于所述上衬垫206的上方。The utility model provides a vapor deposition device 2, as shown in FIG3, comprising a reaction chamber 200. The reaction chamber 200 comprises a chamber top cover 201 and a chamber body 202. The reaction chamber 200 is provided with a tray 209, an air inlet device 207, an upper liner 206, an exhaust ring 230, and a side wall liner 270, and the chamber top cover 201 is located above the upper liner 206.
所述托盘209设置在反应腔200内的下方,托盘209的上表面为晶圆承载面2091。上衬垫206与所述晶圆承载面2091相对,上衬垫206与晶圆承载面2091之间形成反应区域C。托盘209的下方设有加热装置220,通过托盘209将加热装置220提供的热能传递至晶圆W,工艺气体在特定温度下反应并沉积在晶圆W上形成所需材料的薄膜。The tray 209 is disposed at the bottom of the reaction chamber 200, and the upper surface of the tray 209 is a wafer carrying surface 2091. The upper pad 206 is opposite to the wafer carrying surface 2091, and a reaction area C is formed between the upper pad 206 and the wafer carrying surface 2091. A heating device 220 is disposed below the tray 209, and the heat energy provided by the heating device 220 is transferred to the wafer W through the tray 209, and the process gas reacts at a specific temperature and is deposited on the wafer W to form a thin film of a desired material.
本实施例中,如图3所示,沿托盘209的周向方向,在托盘209的上表面设有多个凹部,多个用于放置晶圆W的晶圆承载盘205分别设置在多个凹部内。凹部内设有特殊的气道(图中未示出),所述气道用于在晶圆承载盘205与托盘209之间通入一定压力的气体,使晶圆承载盘205可以被气压托起脱离托盘表面,以一定的高度悬浮起来后绕其中心自转。托盘209底部固定连接一驱动轴204,用于驱动托盘209带动晶圆承载盘205一同绕托盘中心高速旋转。通过驱动晶圆承载盘205自转与公转,使到达晶圆上表面的不同种类工艺气体以均匀的分布在晶圆W上沉积。In this embodiment, as shown in FIG3 , a plurality of recesses are provided on the upper surface of the tray 209 along the circumferential direction of the tray 209, and a plurality of wafer carriers 205 for placing wafers W are respectively arranged in the plurality of recesses. A special airway (not shown in the figure) is provided in the recess, and the airway is used to pass a gas of a certain pressure between the wafer carrier 205 and the tray 209, so that the wafer carrier 205 can be lifted up by the air pressure and separated from the surface of the tray, and then rotate around its center after being suspended at a certain height. A driving shaft 204 is fixedly connected to the bottom of the tray 209, which is used to drive the tray 209 to drive the wafer carrier 205 to rotate at high speed around the center of the tray. By driving the wafer carrier 205 to rotate and revolve, different types of process gases reaching the upper surface of the wafer are deposited on the wafer W in a uniform distribution.
如图4所示,进气装置207的内部具有多个进气管路2071。所述进气管路2071的进气端20711气路连通外部的工艺气体供应装置(图中未示出)。所述进气管路2071的出气端20712具有水平的一字形结构(其长度方向平行于托盘209的径向方向),用于横向地向所述反应区域C内注入工艺气体,使得工艺气体尽可能水平的通过晶圆表面,并在晶圆表面均匀分布,以提高晶圆表面沉积薄膜的均匀性。不同种类工艺气体的所述出气端20712具有不同的高度,因此能够在竖直方向上分层的向反应腔200内注入多种工艺气体,防止多种工艺气体在到达晶圆W表面之间提前反应。As shown in FIG4 , the air inlet device 207 has a plurality of air inlet pipelines 2071 inside. The air inlet end 20711 of the air inlet pipeline 2071 is connected to an external process gas supply device (not shown in the figure). The air outlet end 20712 of the air inlet pipeline 2071 has a horizontal straight-line structure (its length direction is parallel to the radial direction of the tray 209), which is used to inject process gas into the reaction area C laterally, so that the process gas passes through the wafer surface as horizontally as possible and is evenly distributed on the wafer surface to improve the uniformity of the thin film deposited on the wafer surface. The air outlet ends 20712 of different types of process gases have different heights, so that multiple process gases can be injected into the reaction chamber 200 in layers in the vertical direction to prevent the multiple process gases from reacting prematurely before reaching the surface of the wafer W.
如图3、图5所示,所述抽气环230围绕设置在所述托盘209的侧下方。抽气环230包含内环231、外环232以及连接所述内环和外环的环顶面233。如图5所示,沿抽气环230的周向方向,在所述环顶面233开有多个抽气孔235。反应腔200内的气体依序通过抽气环230、排气装置排放至反应腔200外部。As shown in FIG3 and FIG5, the exhaust ring 230 is disposed around the lower side of the tray 209. The exhaust ring 230 includes an inner ring 231, an outer ring 232, and a ring top surface 233 connecting the inner ring and the outer ring. As shown in FIG5, along the circumferential direction of the exhaust ring 230, a plurality of exhaust holes 235 are opened on the ring top surface 233. The gas in the reaction chamber 200 is discharged to the outside of the reaction chamber 200 through the exhaust ring 230 and the exhaust device in sequence.
如图3、图5所示,所述侧壁衬垫270围绕所述托盘209的外周设置,并位于上衬垫206和抽气环230之间,通过侧壁衬垫270防止工艺气体沉积在反应腔200的内侧壁。本实施例中,如图3所示,侧壁衬垫270具有向进气装置207方向延伸的气流引导部271。所述气流引导部271具有环形结构,从上至下,其内径逐渐增大。通过所述气流引导部271将工艺气体引流至抽气环230。As shown in FIG3 and FIG5, the side wall gasket 270 is arranged around the outer circumference of the tray 209 and is located between the upper gasket 206 and the pumping ring 230. The side wall gasket 270 prevents the process gas from being deposited on the inner side wall of the reaction chamber 200. In this embodiment, as shown in FIG3, the side wall gasket 270 has an airflow guide portion 271 extending toward the air inlet device 207. The airflow guide portion 271 has an annular structure, and its inner diameter gradually increases from top to bottom. The process gas is guided to the pumping ring 230 through the airflow guide portion 271.
本实施例中,上衬垫206由第一母线①绕进气装置207的中心轴旋转而成。如图6所示,所述第一母线①具有靠近所述中心轴的起始点和远离中心轴的终点O',所述起始点即上衬垫206的最靠近所述进气装置207的端点。点x、y为所述第一母线①上的任意两点,点x、y与晶圆承载面2091之间的竖直距离分别记为h1、h2,点x、y与进气装置中心轴之间的水平距离分别记为l1、l2,点x、y满足h1×l1=h2×l2。In this embodiment, the upper pad 206 is formed by rotating the first busbar ① around the central axis of the air inlet device 207. As shown in FIG6 , the first busbar ① has a starting point close to the central axis and an end point O' away from the central axis, and the starting point is the end point of the upper pad 206 closest to the air inlet device 207. Points x and y are any two points on the first busbar ①, and the vertical distances between points x and y and the wafer bearing surface 2091 are recorded as h 1 and h 2 , respectively, and the horizontal distances between points x and y and the central axis of the air inlet device are recorded as l 1 and l 2 , respectively, and points x and y satisfy h 1 ×l 1 =h 2 ×l 2 .
本实施例中,如图3所示,所述终点O'落在所述气流引导部271的顶面。沿着与托盘径向平行的方向,从所述终点O'向外水平延伸形成一水平段,所述水平段绕进气装置207的中心轴旋转形成一环形的上衬垫承载部2061。所述上衬垫承载部2061的底面贴合所述气流引导部271的顶面,由气流引导部271为上衬垫承载部2061提供支撑。值得一提的是,上衬垫承载部2061的底面和侧壁衬垫270的顶面可以不是水平面,只要能够保证两者能够贴合即可。In this embodiment, as shown in FIG. 3 , the end point O' falls on the top surface of the airflow guide portion 271. Along the direction parallel to the radial direction of the tray, a horizontal section is horizontally extended outward from the end point O', and the horizontal section rotates around the central axis of the air intake device 207 to form an annular upper pad bearing portion 2061. The bottom surface of the upper pad bearing portion 2061 fits the top surface of the airflow guide portion 271, and the airflow guide portion 271 provides support for the upper pad bearing portion 2061. It is worth mentioning that the bottom surface of the upper pad bearing portion 2061 and the top surface of the side wall pad 270 may not be horizontal planes, as long as the two can be guaranteed to fit each other.
如图3所示,工艺气体的流动截面208为反应腔200内与进气装置207同中心轴的筒形截面,流动截面208的顶部、底部分别落在上衬垫206、晶圆承载面2091上。易于理解的,与点x对应的流动截面208和与点y对应的流动截面208具有相同的面积S,S=2π×h1×l1。也即是说,通过本实用新型中由第一母线①生成的上衬垫206,使得在托盘209的径向方向上,工艺气体的流动截面面积处处相等。因而本实施例中,在远离进气装置207的方向上,工艺气体的浓度梯度较小(工艺气体浓度的降低主要由于工艺气体在流动过程中持续发生反应并沉积下来)。通过本实用新型极大地提高了工艺气体的利用率,减少了工艺气体的用量,显著降低了晶圆W加工的成本。As shown in FIG3 , the flow cross section 208 of the process gas is a cylindrical cross section in the reaction chamber 200 with the same central axis as the gas inlet device 207, and the top and bottom of the flow cross section 208 fall on the upper pad 206 and the wafer carrying surface 2091 respectively. It is easy to understand that the flow cross section 208 corresponding to point x and the flow cross section 208 corresponding to point y have the same area S, S=2π×h 1 ×l 1 . That is to say, through the upper pad 206 generated by the first busbar ① in the utility model, the flow cross section area of the process gas is equal everywhere in the radial direction of the tray 209. Therefore, in this embodiment, in the direction away from the gas inlet device 207, the concentration gradient of the process gas is small (the reduction in the concentration of the process gas is mainly due to the continuous reaction and deposition of the process gas during the flow process). The utility model greatly improves the utilization rate of the process gas, reduces the amount of process gas used, and significantly reduces the cost of wafer W processing.
在另一个实施例中,还可以使非活性气体由最接近上衬垫206的所述出气端20712流入所述反应区域C,使得在参与反应的工艺气体和上衬垫206之间形成分离层。这不仅有助于减少上衬垫206表面的沉积物,还能够迫使参与反应的工艺气体更靠近晶圆表面,以此提高工艺气体的利用率。In another embodiment, the inactive gas may be made to flow into the reaction region C from the gas outlet 20712 closest to the upper liner 206, so that a separation layer is formed between the process gas involved in the reaction and the upper liner 206. This not only helps to reduce the deposits on the surface of the upper liner 206, but also forces the process gas involved in the reaction to be closer to the wafer surface, thereby improving the utilization rate of the process gas.
晶圆表面化学反应的速率受到晶圆表面工艺气体浓度的影响。本实施例中,沿着远离进气装置207的方向,上衬垫206与晶圆承载面2091之间的距离逐渐减小,自进气装置207流出的工艺气体被上衬垫206强制流向晶圆承载面2091,原本沿水平方向输送的工艺气体获得竖直方向的速度分量,从而使得更多的工艺气体往晶圆表面输送以参与晶圆表面的化学反应。因此,通过本实用新型提高了晶圆表面薄膜的沉积速率。The rate of chemical reaction on the wafer surface is affected by the concentration of process gas on the wafer surface. In this embodiment, the distance between the upper pad 206 and the wafer bearing surface 2091 gradually decreases in the direction away from the air inlet device 207, and the process gas flowing out of the air inlet device 207 is forced by the upper pad 206 to flow toward the wafer bearing surface 2091. The process gas originally transported in the horizontal direction obtains a velocity component in the vertical direction, so that more process gas is transported to the wafer surface to participate in the chemical reaction on the wafer surface. Therefore, the deposition rate of the thin film on the wafer surface is improved by the utility model.
在一个实验中,通过采用平板型上衬垫106的气相沉积设备1和本实施例的气相沉积设备2(上衬垫206由第一母线①生成),在同样大小的晶圆W(晶圆W自转的同时还随托盘209公转)上沉积相同材料的薄膜。该实验中,气相沉积设备1和气相沉积设备2的反应腔200具有相同的直径,且均使用了相同大小的托盘。该实验中,晶圆直径约为150mm。气相沉积设备1中,上衬垫106与晶圆承载面2091之间的竖直距离与气相沉积设备2中上衬垫206的起始点O与晶圆承载面2091之间的竖直距离相同。需要强调的是,上述数据仅作为示例,不作为本实用新型的限制。In an experiment, a thin film of the same material is deposited on a wafer W of the same size (wafer W rotates while revolving with the tray 209) by using a vapor deposition device 1 with a flat upper pad 106 and a vapor deposition device 2 of this embodiment (the upper pad 206 is generated by the first busbar ①). In this experiment, the reaction chamber 200 of the vapor deposition device 1 and the vapor deposition device 2 have the same diameter, and both use trays of the same size. In this experiment, the wafer diameter is about 150 mm. In the vapor deposition device 1, the vertical distance between the upper pad 106 and the wafer bearing surface 2091 is the same as the vertical distance between the starting point O of the upper pad 206 in the vapor deposition device 2 and the wafer bearing surface 2091. It should be emphasized that the above data is only used as an example and is not intended to be a limitation of the present utility model.
如图7所示,可以将气相沉积设备1的平板型上衬垫106,看做由水平直线(base)绕进气装置107的中心轴旋转而成。当上衬垫106由水平直线旋转得来时,如图8所示,晶圆表面薄膜的平均长速为2.5896um/h,薄膜厚度一致性差异为3.16%。所述薄膜厚度一致性差异的计算公式为(GRmax-GRmin)/GRave/2,GRmax、GRmin分别为晶圆表面薄膜的最大、最小生长速度,GRave为晶圆表面薄膜的平均生长速度。在理想状态下,我们希望薄膜的平均长速尽可能高,且薄膜厚度一致性差异尽可能小。As shown in FIG7 , the flat upper pad 106 of the vapor deposition device 1 can be regarded as being formed by rotating a horizontal straight line (base) around the central axis of the air inlet device 107. When the upper pad 106 is rotated from a horizontal straight line, as shown in FIG8 , the average growth rate of the film on the wafer surface is 2.5896um/h, and the film thickness consistency difference is 3.16%. The calculation formula for the film thickness consistency difference is (GR max -GR min )/GR ave /2, where GR max and GR min are the maximum and minimum growth rates of the film on the wafer surface, respectively, and GR ave is the average growth rate of the film on the wafer surface. Ideally, we hope that the average growth rate of the film is as high as possible and the film thickness consistency difference is as small as possible.
在上述实验中,采用由第一母线①得来的上衬垫206进行CVD工艺时,如图8所示,晶圆表面薄膜的平均长速为3.0192um/h,薄膜厚度一致性差异为3.18%。如图9所示,晶圆径向方向上的各个位置处,第一母线①对应的薄膜生长速度始终高于水平直线base对应的薄膜生长速度。以上数据说明,本实施例的气相沉积设备2显著提高薄膜生长速度的同时,还兼顾了晶圆表面薄膜厚度的一致性。气相沉积设备2能够在晶圆表面快速生长出高质量的薄膜。In the above experiment, when the upper pad 206 obtained from the first busbar ① is used for the CVD process, as shown in Figure 8, the average growth rate of the film on the wafer surface is 3.0192um/h, and the film thickness consistency difference is 3.18%. As shown in Figure 9, at each position in the radial direction of the wafer, the film growth rate corresponding to the first busbar ① is always higher than the film growth rate corresponding to the horizontal straight line base. The above data show that the vapor deposition equipment 2 of this embodiment significantly improves the film growth rate while taking into account the consistency of the film thickness on the wafer surface. The vapor deposition equipment 2 can quickly grow high-quality films on the wafer surface.
本实用新型中,上衬垫206也可以由第二母线绕进气装置207的中心轴旋转而成。所述第二母线由第一母线①绕其起始点O在竖直方向上旋转设定的角度而成。定义:第一母线①绕其起始点O向靠近晶圆承载面2091的方向旋转时,所述角度为负值;第一母线①绕其起始点O向远离晶圆承载面2091的方向旋转时,所述角度为正值。本实用新型中,所述角度为[-2°,5°],包括-2°、(-2°,0°)、0°、(0°,5°)、5°,(-2°,5°)等。In the present invention, the upper pad 206 can also be formed by rotating the second busbar around the central axis of the air intake device 207. The second busbar is formed by rotating the first busbar ① around its starting point O in the vertical direction at a set angle. Definition: When the first busbar ① rotates around its starting point O in a direction close to the wafer bearing surface 2091, the angle is a negative value; when the first busbar ① rotates around its starting point O in a direction away from the wafer bearing surface 2091, the angle is a positive value. In the present invention, the angle is [-2°, 5°], including -2°, (-2°, 0°), 0°, (0°, 5°), 5°, (-2°, 5°), etc.
在另一个实施例中,如图6所示,第二母线②由第一母线①旋转-2°得来。该实施例中,沿着远离进气装置207的方向,流动截面208的面积逐渐减小(小于S),与由第一母线①生成的上衬垫206相比,该实施例的上衬垫206可以将更多的工艺气体往晶圆表面输送,不仅可以进一步减小工艺气体的投放量,同时还使得晶圆表面薄膜的平均长速进一步提高。In another embodiment, as shown in FIG6 , the second busbar ② is obtained by rotating the first busbar ① by -2°. In this embodiment, the area of the flow cross section 208 gradually decreases (less than S) along the direction away from the gas inlet device 207. Compared with the upper liner 206 generated by the first busbar ①, the upper liner 206 of this embodiment can transport more process gas to the wafer surface, which can not only further reduce the amount of process gas input, but also further increase the average growth rate of the film on the wafer surface.
如图9所示,晶圆径向方向上的各个位置处,第二母线②对应的薄膜生长速度始终高于第一母线①对应的薄膜生长速度。如图8所示,与第二母线②对应的晶圆表面薄膜平均长速为3.1660um/h,薄膜厚度一致性差异为4.13%。同时也可以看出,与第一母线①对应的薄膜厚度一致性差异(3.67%)相比,第二母线②对应的薄膜厚度一致性差异略有增大,但是在可以接受的范围内。As shown in Figure 9, at each position in the radial direction of the wafer, the film growth rate corresponding to the second busbar ② is always higher than the film growth rate corresponding to the first busbar ①. As shown in Figure 8, the average growth rate of the film on the wafer surface corresponding to the second busbar ② is 3.1660um/h, and the film thickness consistency difference is 4.13%. It can also be seen that compared with the film thickness consistency difference (3.67%) corresponding to the first busbar ①, the film thickness consistency difference corresponding to the second busbar ② is slightly increased, but within an acceptable range.
在另一个实施例中,如图6所示,第二母线③由第一母线①旋转5°得来。如图9所示,晶圆径向方向上的各个位置处,第二母线③对应的薄膜生长速度始终低于第一母线①对应的薄膜生长速度。该实施例中,虽然沿着远离进气装置207的方向,流动截面208的面积仍然逐渐增大,但与采用平板型的上衬垫106相比,仍可以减少工艺气体的投放量、提高工艺气体的源效。该实施例中,如图8所示,晶圆表面薄膜的平均长速为2.6786um/h,薄膜厚度一致性差异为2.37%。与采用平板型的上衬垫相比,该实施例不仅提高了晶圆表面薄膜的平均长速,还减小了薄膜厚度一致性差异,为较佳的实施例。In another embodiment, as shown in FIG6 , the second busbar ③ is obtained by rotating the first busbar ① by 5°. As shown in FIG9 , at each position in the radial direction of the wafer, the film growth rate corresponding to the second busbar ③ is always lower than the film growth rate corresponding to the first busbar ①. In this embodiment, although the area of the flow cross section 208 still gradually increases in the direction away from the air inlet device 207, compared with the use of a flat upper liner 106, the amount of process gas delivered can still be reduced and the source efficiency of the process gas can be improved. In this embodiment, as shown in FIG8 , the average growth rate of the film on the wafer surface is 2.6786um/h, and the film thickness consistency difference is 2.37%. Compared with the use of a flat upper liner, this embodiment not only improves the average growth rate of the film on the wafer surface, but also reduces the film thickness consistency difference, and is a preferred embodiment.
实施例二Embodiment 2
本实施例的上衬垫206由第三母线④绕进气装置207的中心轴旋转而成,如图6所示,所述第三母线④为直线,第三母线④与第一母线①共用所述起始点O和终点O',第三母线④位于第一母线①和第二母线③之间。The upper gasket 206 of this embodiment is formed by rotating the third busbar ④ around the central axis of the air intake device 207. As shown in Figure 6, the third busbar ④ is a straight line. The third busbar ④ shares the starting point O and the end point O' with the first busbar ①. The third busbar ④ is located between the first busbar ① and the second busbar ③.
如图9所示,晶圆径向方向上的各个位置处,第三母线④对应的薄膜生长速度低于第一母线①对应的薄膜生长速度、并高于第二母线③对应的薄膜生长速度。如图8所示,与第三母线④对应的薄膜平均长速为2.9127um/h,薄膜厚度一致性差异为3.67%。As shown in Figure 9, at various positions in the radial direction of the wafer, the film growth rate corresponding to the third busbar ④ is lower than the film growth rate corresponding to the first busbar ①, and higher than the film growth rate corresponding to the second busbar ③. As shown in Figure 8, the average film growth rate corresponding to the third busbar ④ is 2.9127um/h, and the film thickness consistency difference is 3.67%.
与平板型的上衬垫106相比,采用第三母线④生成的上衬垫206在增加工艺气体源效、提高晶圆表面薄膜沉积速度的同时,对晶圆表面薄膜厚度一致性的影响较小,可以忽略不计。Compared with the flat-type upper liner 106, the upper liner 206 generated by the third busbar ④ increases the process gas source efficiency and improves the film deposition rate on the wafer surface, while having a small and negligible impact on the consistency of the film thickness on the wafer surface.
实施例三Embodiment 3
本实施例中,如图3、图10所示,腔室顶盖201内设有冷却流体通道2011,由于腔室顶盖201与上衬垫206之间具有良好的热传递,通过所述冷却流体通道2011可以调节腔室顶盖201、上衬垫206的温度。理想状态下,希望上衬垫206的温度比托盘温度低大约100度至200度,一方面可以减少在上衬垫206表面的薄膜沉积,从而有效减少反应腔200内的颗粒污染物,达到提高晶圆W成品率、降低反应腔200的清洗频率的目的。另一方面,上衬垫206与反应腔200内的工艺气体也存在热传递,通过控制上衬垫206的温度,可以避免因上衬垫206的温度过低导致反应腔200内工艺气体的温度不能满足工艺需求。In this embodiment, as shown in FIG. 3 and FIG. 10 , a cooling fluid channel 2011 is provided in the chamber top cover 201. Since there is good heat transfer between the chamber top cover 201 and the upper liner 206, the temperature of the chamber top cover 201 and the upper liner 206 can be adjusted through the cooling fluid channel 2011. Ideally, it is hoped that the temperature of the upper liner 206 is about 100 to 200 degrees lower than the tray temperature. On the one hand, the film deposition on the surface of the upper liner 206 can be reduced, thereby effectively reducing the particle contaminants in the reaction chamber 200, thereby achieving the purpose of improving the yield of the wafer W and reducing the cleaning frequency of the reaction chamber 200. On the other hand, there is also heat transfer between the upper liner 206 and the process gas in the reaction chamber 200. By controlling the temperature of the upper liner 206, it can be avoided that the temperature of the process gas in the reaction chamber 200 cannot meet the process requirements due to the excessively low temperature of the upper liner 206.
由于气体流动导致的热传导以及腔体中存在冷却通道,不可避免的使得托盘209各区域的导热性差异较大。本实施例中,基于工艺过程中托盘209的温度分布,沿托盘209的径向方向,将托盘209虚拟划分为多个同心的环形温度带,相邻的所述环形温度带之间的温差超过设定的温差阈值。如图10所示,本实施例中将托盘划分为3个环形温度带D1、D2、D3,环形温度带的数量仅作为示例,不作为本实用新型的限制。Due to the heat conduction caused by the gas flow and the presence of the cooling channel in the cavity, it is inevitable that the thermal conductivity of each area of the tray 209 is greatly different. In this embodiment, based on the temperature distribution of the tray 209 during the process, the tray 209 is virtually divided into a plurality of concentric annular temperature zones along the radial direction of the tray 209, and the temperature difference between adjacent annular temperature zones exceeds the set temperature difference threshold. As shown in FIG. 10, in this embodiment, the tray is divided into three annular temperature zones D1 , D2 , and D3 . The number of annular temperature zones is only used as an example and is not a limitation of the present invention.
沿所述腔室顶盖201的径向方向,将所述腔室顶盖201虚拟划分为与所述多个环形温度带分别对应的多个环形调温区。各环形温度带向上衬垫对应的环形区域辐射的热量不同。环形调温区内的冷却流体通道2011与腔室顶盖201下表面之间的距离取决于对应的环形温度带的温度。如图10所示,本实施例中将腔室顶盖201划分为3个环形调温区G1、G2、G3。Along the radial direction of the chamber top cover 201, the chamber top cover 201 is virtually divided into a plurality of annular temperature adjustment zones corresponding to the plurality of annular temperature zones. Each annular temperature zone radiates different amounts of heat to the annular region corresponding to the upper liner. The distance between the cooling fluid channel 2011 in the annular temperature adjustment zone and the lower surface of the chamber top cover 201 depends on the temperature of the corresponding annular temperature zone. As shown in FIG10, in this embodiment, the chamber top cover 201 is divided into three annular temperature adjustment zones G1 , G2 , and G3 .
如图10所示,环形温度带D2的温度最高,对应环形调温区G2内冷却流体通道2011与腔室顶盖201下表面之间的距离最近。环形温度带D1的温度最低,对应环形调温区G1内冷却流体通道2011与腔室顶盖201下表面之间的距离最远。这样可以按区域调节上衬垫206的温度,有利于减小上衬垫206的温度梯度,避免上衬垫206因热应力发生变形。通过提高上衬垫206温度的一致性,还可以提高反应腔200内工艺气体温度的一致性,有益于在晶圆表面生长厚度均匀的薄膜。As shown in FIG10 , the temperature of the annular temperature zone D 2 is the highest, and the distance between the cooling fluid channel 2011 in the corresponding annular temperature adjustment zone G 2 and the lower surface of the chamber top cover 201 is the shortest. The temperature of the annular temperature zone D 1 is the lowest, and the distance between the cooling fluid channel 2011 in the corresponding annular temperature adjustment zone G 1 and the lower surface of the chamber top cover 201 is the farthest. In this way, the temperature of the upper liner 206 can be adjusted by region, which is conducive to reducing the temperature gradient of the upper liner 206 and avoiding deformation of the upper liner 206 due to thermal stress. By improving the consistency of the temperature of the upper liner 206, the consistency of the temperature of the process gas in the reaction chamber 200 can also be improved, which is beneficial to growing a thin film with uniform thickness on the surface of the wafer.
实施例四Embodiment 4
本实施例中,腔室顶盖201与上衬垫206之间设有调温机构,用于增强对上衬垫206的调温效果。如图3、图11所示,所述调温机构包括导热板261(铝材质或石英材质),导热板261的上表面贴合腔室顶盖201的下表面。In this embodiment, a temperature regulating mechanism is provided between the chamber top cover 201 and the upper liner 206 to enhance the temperature regulating effect on the upper liner 206. As shown in FIG3 and FIG11, the temperature regulating mechanism includes a heat conducting plate 261 (made of aluminum or quartz), and the upper surface of the heat conducting plate 261 is attached to the lower surface of the chamber top cover 201.
如图3、图11所示,所述调温机构还包括形成在导热板261与上衬垫206之间的间隙262。气相沉积设备还包括传热气体输入端2621,如图3、图11所示,所述传热气体输入端2621穿设腔室顶盖201和导热板261,用于向所述间隙262提供传热气体。As shown in FIGS. 3 and 11 , the temperature adjustment mechanism further includes a gap 262 formed between the heat conducting plate 261 and the upper liner 206. The vapor deposition apparatus further includes a heat transfer gas input end 2621, as shown in FIGS. 3 and 11 , the heat transfer gas input end 2621 penetrates the chamber top cover 201 and the heat conducting plate 261, and is used to provide heat transfer gas to the gap 262.
易于理解的,导热板261越厚、导热板261的表面发射率越大,导热板261的传热效果越好。基于托盘209的温度分布特点,本实施例中,如图11所示,沿着远离进气装置207的方向,导热板261的厚度先变厚后变薄和/或导热板261的表面发射率先变大后变小。由于沿腔室顶盖201与上衬垫206之间的间距处处一致,导热板261变厚/变薄,则间隙262就变小/变大。因此沿着远离进气装置207的方向,间隙262先变小后变大。It is easy to understand that the thicker the heat conducting plate 261 is and the greater the surface emissivity of the heat conducting plate 261 is, the better the heat transfer effect of the heat conducting plate 261 is. Based on the temperature distribution characteristics of the tray 209, in this embodiment, as shown in FIG11, along the direction away from the air inlet device 207, the thickness of the heat conducting plate 261 first becomes thicker and then becomes thinner and/or the surface emissivity of the heat conducting plate 261 first becomes larger and then becomes smaller. Since the spacing between the chamber top cover 201 and the upper liner 206 is consistent everywhere, the gap 262 becomes smaller/larger when the heat conducting plate 261 becomes thicker/thinner. Therefore, along the direction away from the air inlet device 207, the gap 262 first becomes smaller and then becomes larger.
本实施例中,导热板261的厚度、导热板261的表面发射率、间隙262大小随托盘209温度变化而变化,有助于按区域调节上衬垫206的温度,提高上衬垫206温度的一致性,避免上衬垫206的温度梯度过大而变形损坏。In this embodiment, the thickness of the heat conducting plate 261, the surface emissivity of the heat conducting plate 261, and the size of the gap 262 change with the temperature of the tray 209, which helps to adjust the temperature of the upper pad 206 by region, improve the temperature consistency of the upper pad 206, and avoid deformation and damage of the upper pad 206 due to excessive temperature gradient.
在另一个实施例中,所述传热气体的组分可调。例如,传热气体可以包括氮气、氩气,该两种气体具有不同的导热系数。通过调节氮气与氩气的流量比,可以调节传热气体的导热率,以此实时调节上衬垫206的温度。在不同材料的沉积工艺中,可以将上衬垫206调节至不同的温度,以此减少上衬垫206的沉积物。在一个实施例中,氮气与氩气的流量比范围为3:1至2:1(此仅作为示例,不作为本实用新型的限制)。In another embodiment, the composition of the heat transfer gas is adjustable. For example, the heat transfer gas may include nitrogen and argon, and the two gases have different thermal conductivities. By adjusting the flow ratio of nitrogen to argon, the thermal conductivity of the heat transfer gas can be adjusted, thereby adjusting the temperature of the upper pad 206 in real time. In the deposition process of different materials, the upper pad 206 can be adjusted to different temperatures to reduce the deposits on the upper pad 206. In one embodiment, the flow ratio of nitrogen to argon ranges from 3:1 to 2:1 (this is only an example and is not a limitation of the present invention).
应理解,上述实施例中各步骤的序号的大小并不意味着执行顺序的先后,各过程的执行顺序应以其功能和内在逻辑确定,而不应对本申请实施例的实施过程构成任何限定。It should be understood that the size of the serial numbers of the steps in the above embodiments does not mean the order of execution. The execution order of each process should be determined by its function and internal logic, and should not constitute any limitation on the implementation process of the embodiments of the present application.
以上所述,仅为本实用新型的具体实施方式,但本实用新型的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本实用新型揭露的技术范围内,可轻易想到各种等效的修改或替换,这些修改或替换都应涵盖在本实用新型的保护范围之内。因此,本实用新型的保护范围应以权利要求的保护范围为准。The above is only a specific implementation of the utility model, but the protection scope of the utility model is not limited thereto. Any technician familiar with the technical field can easily think of various equivalent modifications or replacements within the technical scope disclosed by the utility model, and these modifications or replacements should be included in the protection scope of the utility model. Therefore, the protection scope of the utility model should be based on the protection scope of the claims.
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